Cargando…

Synthesis and Properties of Energetic Hydrazinium 5-Nitro-3-dinitromethyl-2H-pyrazole by Unexpected Isomerization of N-Nitropyrazole

[Image: see text] A new energetic salt, hydrazinium 5-nitro-3-dinitromethyl-2H-pyrazole, was synthesized using 1-nitro-3-trinitromethylpyrazole and hydrazine as raw materials and fully characterized by IR and NMR spectroscopy, elemental analysis, and X-ray crystallography. The isomerization of N-nit...

Descripción completa

Detalles Bibliográficos
Autores principales:	Zhang, Yiying, Li, Yanan, Yu, Tao, Liu, Yingzhe, Chen, Sanping, Ge, Zhongxue, Sun, Chenghui, Pang, Siping
Formato:	Online Artículo Texto
Lenguaje:	English
Publicado:	American Chemical Society 2019
Acceso en línea:	https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6868590/ https://www.ncbi.nlm.nih.gov/pubmed/31763523 http://dx.doi.org/10.1021/acsomega.9b01910

Ejemplares similares

Theoretical design and prediction of properties for dinitromethyl, fluorodinitromethyl, and (difluoroamino)dinitromethyl derivatives of triazole and tetrazole
por: Fei, Teng, et al.
Publicado: (2018)

4-Nitrophenylhydrazinium picrate monohydrate
por: Cai, Hong-lan, et al.
Publicado: (2013)

Coordinative Combination of Nitroamine and Gem-Dinitromethyl with Fused Ring for Enhanced Oxygen Balances and Detonation Properties
por: Zhang, Xun, et al.
Publicado: (2022)

Energetic Di- and Trinitromethylpyridines: Synthesis and Characterization
por: Zhang, Yiying, et al.
Publicado: (2017)

Redetermination of phenylhydrazinium chloride
por: de Lima, Geraldo M., et al.
Publicado: (2007)

1-Methylhydrazinium picrate
por: Mu, Xiao-Gang, et al.
Publicado: (2011)

Hydrazinium 2-amino-4-nitrobenzoate dihydrate: crystal structure and Hirshfeld surface analysis
por: Wardell, James L., et al.
Publicado: (2017)

3-Methyl-1,2,3-triazolium-1N-dinitromethylylide and the strategy of zwitterionic dinitromethyl groups in energetic materials design
por: Wozniak, Dominique R., et al.
Publicado: (2021)

Synthesis and Characterization of Azido- and Nitratoalkyl Nitropyrazoles as Potential Melt-Cast Explosives
por: Reinhardt, Elena, et al.
Publicado: (2023)

(Methoxycarbonyl)hydrazinium chloride monohydrate
por: Xie, Jian-Wu, et al.
Publicado: (2008)

Polymorphism, phase transformation and energetic properties of 3-nitro-1,2,4-triazole
por: Zhang, Pengcheng, et al.
Publicado: (2018)

Multimolecular Complexes of CL-20 with Nitropyrazole Derivatives: Geometric, Electronic Structure, and Stability
por: Zhu, Shuang-fei, et al.
Publicado: (2019)

Isostructural rubidium and caesium 4-(3,5-dinitropyrazol-4-yl)-3,5-dinitropyrazolates: crystal engineering with polynitro energetic species
por: Domasevitch, Kostiantyn V., et al.
Publicado: (2021)

Crystal structure of 2,2-diphenylhydrazinium chloride
por: Paul, Amit Kumal, et al.
Publicado: (2014)

Synthesis and Characterization of 5-Nitro-2-nitratomethyl-1,2,3,4-tetrazole: A High Nitrogen Energetic Compound with Good Oxygen Balance
por: Li, Yuchuan, et al.
Publicado: (2012)

Insensitive High-Energy Density Materials Based on Azazole-Rich Rings: 1,2,4-Triazole N-Oxide Derivatives Containing Isomerized Nitro and Amino Groups
por: Yang, Xinbo, et al.
Publicado: (2023)

Unexpected Isomerization of Oxetane-Carboxylic Acids
por: Chalyk, Bohdan, et al.
Publicado: (2022)

Unexpected Isomerization of Hexa‐tert‐butyl‐octaphosphane
por: Grell, Toni, et al.
Publicado: (2019)

From N–H Nitration to Controllable Aromatic Mononitration and Dinitration—The Discovery of a Versatile and Powerful N-Nitropyrazole Nitrating Reagent
por: Yang, Tao, et al.
Publicado: (2022)

2-(4-Chlorobenzoyl)-1-(diaminomethylene)hydrazinium chloride monohydrate
por: Chernyshev, V. M., et al.
Publicado: (2010)

Tri-explosophoric groups driven fused energetic heterocycles featuring superior energetic and safety performances outperforms HMX
por: Li, Jie, et al.
Publicado: (2022)

Recent Advances in Synthesis and Properties of Nitrated-Pyrazoles Based Energetic Compounds
por: Zhang, Shijie, et al.
Publicado: (2020)

Enhanced Energetic Performance via the Combination of Furoxan and Oxa-[5,5]bicyclic Structures
por: Zhang, Qi, et al.
Publicado: (2023)

Nitration of Chitin Monomer: From Glucosamine to Energetic Compound
por: Dou, Hui, et al.
Publicado: (2021)

Identification and characterization of an unexpected isomerization motif in CDRH2 that affects antibody activity
por: Yi, Meiqi, et al.
Publicado: (2023)

Amination of Nitroazoles — A Comparative Study of Structural and Energetic Properties
por: Zhao, Xiuxiu, et al.
Publicado: (2014)

N-Functionalization of 5-Aminotetrazoles: Balancing Energetic Performance and Molecular Stability by Introducing ADNP
por: Xiong, Jin, et al.
Publicado: (2022)

Boosting the Energetic Performance of Trinitromethyl-1,2,4-oxadiazole Moiety by Increasing Nitrogen-Oxygen in the Bridge
por: Chen, Peng, et al.
Publicado: (2022)

Progress of Artificial Intelligence in Drug Synthesis and Prospect of Its Application in Nitrification of Energetic Materials
por: Tan, Bojun, et al.
Publicado: (2023)

Size-matched hydrogen bonded hydroxylammonium frameworks for regulation of energetic materials
por: Lai, Qi, et al.
Publicado: (2022)

Energetic Butterfly: Heat-Resistant Diaminodinitro trans-Bimane
por: Zhang, Pengcheng, et al.
Publicado: (2019)

Asymmetrical Methylene-Bridge Linked Fully Iodinated Azoles as Energetic Biocidal Materials with Improved Thermal Stability
por: Zhao, Xinyuan, et al.
Publicado: (2023)

3,5-Dimethyl-1-(4-nitrophenyl)-1H-pyrazole
por: Tiekink, Edward R. T., et al.
Publicado: (2012)

Crystal structures of the two isomeric hydrogen-bonded cocrystals 2-chloro-4-nitrobenzoic acid–5-nitroquinoline (1/1) and 5-chloro-2-nitrobenzoic acid–5-nitroquinoline (1/1)
por: Gotoh, Kazuma, et al.
Publicado: (2019)

Sensitive Energetics from the N‐Amination of 4‐Nitro‐1,2,3‐Triazole
por: Wozniak, Dominique R., et al.
Publicado: (2020)

Theoretical investigation on the ground state properties of the hexaamminecobalt(iii) and nitro–nitrito linkage isomerism in pentaamminecobalt(iii) in vacuo
por: Muya, Jules Tshishimbi, et al.
Publicado: (2018)

5-Amino-1-(4-nitrophenyl)-1H-pyrazole-3-carbonitrile
por: Jiang, Qiang-Hua, et al.
Publicado: (2011)

Fluoropolymer/Glycidyl Azide Polymer (GAP) Block Copolyurethane as New Energetic Binders: Synthesis, Mechanical Properties, and Thermal Performance
por: Xu, Minghui, et al.
Publicado: (2021)

Full-nitro-nitroamino cooperative action: Climbing the energy peak of benzenes with enhanced chemical stability
por: Sun, Qi, et al.
Publicado: (2022)

Energetic Materials Based on N-substituted 4(5)-nitro-1,2,3-triazoles
por: Sukhanov, Gennady T., et al.
Publicado: (2022)

Cannot write session to /tmp/vufind_sessions/sess_o5o62qb3thmo3asecg2ovi7fj3