Synthesis and Crystal Structure of Dimorphic Dibenzo[cde,opq]rubicene

Dibenzo[cde,opq]rubicene has been synthesized by an eight‐step reaction sequence including an iron‐mediated [2+2+1] cycloaddition and a flash vacuum pyrolysis as key steps. Two crystal modifications of the S‐shaped, planar polycyclic aromatic hydrocarbon have been obtained and characterized by X‐ray...

Descripción completa

Detalles Bibliográficos
Autores principales: Suresh, Joghee R., Whitener, Glenn, Theumer, Gabriele, Bröcher, Dirk J., Bauer, Ingmar, Massa, Werner, Knölker, Hans‐Joachim
Formato: Online Artículo Texto
Lenguaje:English
Publicado: John Wiley and Sons Inc. 2019
Materias:
Full Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6899531/
https://www.ncbi.nlm.nih.gov/pubmed/31339614
http://dx.doi.org/10.1002/chem.201902915
_version_ 1783477150479810560
author Suresh, Joghee R.
Whitener, Glenn
Theumer, Gabriele
Bröcher, Dirk J.
Bauer, Ingmar
Massa, Werner
Knölker, Hans‐Joachim
author_facet Suresh, Joghee R.
Whitener, Glenn
Theumer, Gabriele
Bröcher, Dirk J.
Bauer, Ingmar
Massa, Werner
Knölker, Hans‐Joachim
author_sort Suresh, Joghee R.
collection PubMed
description Dibenzo[cde,opq]rubicene has been synthesized by an eight‐step reaction sequence including an iron‐mediated [2+2+1] cycloaddition and a flash vacuum pyrolysis as key steps. Two crystal modifications of the S‐shaped, planar polycyclic aromatic hydrocarbon have been obtained and characterized by X‐ray diffractometry.
format Online
Article
Text
id pubmed-6899531
institution National Center for Biotechnology Information
language English
publishDate 2019
publisher John Wiley and Sons Inc.
record_format MEDLINE/PubMed
spelling pubmed-68995312019-12-19 Synthesis and Crystal Structure of Dimorphic Dibenzo[cde,opq]rubicene Suresh, Joghee R. Whitener, Glenn Theumer, Gabriele Bröcher, Dirk J. Bauer, Ingmar Massa, Werner Knölker, Hans‐Joachim Chemistry Full Papers Dibenzo[cde,opq]rubicene has been synthesized by an eight‐step reaction sequence including an iron‐mediated [2+2+1] cycloaddition and a flash vacuum pyrolysis as key steps. Two crystal modifications of the S‐shaped, planar polycyclic aromatic hydrocarbon have been obtained and characterized by X‐ray diffractometry. John Wiley and Sons Inc. 2019-09-24 2019-10-28 /pmc/articles/PMC6899531/ /pubmed/31339614 http://dx.doi.org/10.1002/chem.201902915 Text en © 2019 The Authors. Published by Wiley-VCH Verlag GmbH & Co. KGaA. This is an open access article under the terms of the http://creativecommons.org/licenses/by-nc-nd/4.0/ License, which permits use and distribution in any medium, provided the original work is properly cited, the use is non‐commercial and no modifications or adaptations are made.
spellingShingle Full Papers
Suresh, Joghee R.
Whitener, Glenn
Theumer, Gabriele
Bröcher, Dirk J.
Bauer, Ingmar
Massa, Werner
Knölker, Hans‐Joachim
Synthesis and Crystal Structure of Dimorphic Dibenzo[cde,opq]rubicene
title Synthesis and Crystal Structure of Dimorphic Dibenzo[cde,opq]rubicene
title_full Synthesis and Crystal Structure of Dimorphic Dibenzo[cde,opq]rubicene
title_fullStr Synthesis and Crystal Structure of Dimorphic Dibenzo[cde,opq]rubicene
title_full_unstemmed Synthesis and Crystal Structure of Dimorphic Dibenzo[cde,opq]rubicene
title_short Synthesis and Crystal Structure of Dimorphic Dibenzo[cde,opq]rubicene
title_sort synthesis and crystal structure of dimorphic dibenzo[cde,opq]rubicene
topic Full Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6899531/
https://www.ncbi.nlm.nih.gov/pubmed/31339614
http://dx.doi.org/10.1002/chem.201902915
work_keys_str_mv AT sureshjogheer synthesisandcrystalstructureofdimorphicdibenzocdeopqrubicene
AT whitenerglenn synthesisandcrystalstructureofdimorphicdibenzocdeopqrubicene
AT theumergabriele synthesisandcrystalstructureofdimorphicdibenzocdeopqrubicene
AT brocherdirkj synthesisandcrystalstructureofdimorphicdibenzocdeopqrubicene
AT baueringmar synthesisandcrystalstructureofdimorphicdibenzocdeopqrubicene
AT massawerner synthesisandcrystalstructureofdimorphicdibenzocdeopqrubicene
AT knolkerhansjoachim synthesisandcrystalstructureofdimorphicdibenzocdeopqrubicene

Ejemplares similares