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Microwave-assisted synthesis of 2-substituted 4,5,6,7-tetrahydro-1,3-thiazepines from 4-aminobutanol

A general procedure for the synthesis of 2-substituted tetrahydro-1,3-thiazepines by MW-assisted cyclization of 4-thioamidobutanols is presented. The acyclic precursors were prepared in high overall yields by an expeditious three-step diacylation/thionation/deprotection sequence from 4-aminobutanol....

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Detalles Bibliográficos
Autores principales:	Mollo, María C, Kilimciler, Natalia B, Bisceglia, Juan A, Orelli, Liliana R
Formato:	Online Artículo Texto
Lenguaje:	English
Publicado:	Beilstein-Institut 2020
Materias:	Full Research Paper
Acceso en línea:	https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6964664/ https://www.ncbi.nlm.nih.gov/pubmed/31976014 http://dx.doi.org/10.3762/bjoc.16.5

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