Combined X-ray and neutron single-crystal diffraction in diamond anvil cells

It is shown that it is possible to perform combined X-ray and neutron single-crystal studies in the same diamond anvil cell (DAC). A modified Merrill–Bassett DAC equipped with an inflatable membrane filled with He gas has been developed. It can be used on laboratory X-ray and synchrotron diffractome...

Descripción completa

Detalles Bibliográficos
Autores principales: Grzechnik, Andrzej, Meven, Martin, Paulmann, Carsten, Friese, Karen
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2020
Materias:
Research Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6998780/
https://www.ncbi.nlm.nih.gov/pubmed/32047402
http://dx.doi.org/10.1107/S1600576719014201
_version_ 1783493895888306176
author Grzechnik, Andrzej
Meven, Martin
Paulmann, Carsten
Friese, Karen
author_facet Grzechnik, Andrzej
Meven, Martin
Paulmann, Carsten
Friese, Karen
author_sort Grzechnik, Andrzej
collection PubMed
description It is shown that it is possible to perform combined X-ray and neutron single-crystal studies in the same diamond anvil cell (DAC). A modified Merrill–Bassett DAC equipped with an inflatable membrane filled with He gas has been developed. It can be used on laboratory X-ray and synchrotron diffractometers as well as on neutron instruments. The data processing procedures and a joint structural refinement of the high-pressure synchrotron and neutron single-crystal data are presented and discussed for the first time.
format Online
Article
Text
id pubmed-6998780
institution National Center for Biotechnology Information
language English
publishDate 2020
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-69987802020-02-11 Combined X-ray and neutron single-crystal diffraction in diamond anvil cells Grzechnik, Andrzej Meven, Martin Paulmann, Carsten Friese, Karen J Appl Crystallogr Research Papers It is shown that it is possible to perform combined X-ray and neutron single-crystal studies in the same diamond anvil cell (DAC). A modified Merrill–Bassett DAC equipped with an inflatable membrane filled with He gas has been developed. It can be used on laboratory X-ray and synchrotron diffractometers as well as on neutron instruments. The data processing procedures and a joint structural refinement of the high-pressure synchrotron and neutron single-crystal data are presented and discussed for the first time. International Union of Crystallography 2020-02-01 /pmc/articles/PMC6998780/ /pubmed/32047402 http://dx.doi.org/10.1107/S1600576719014201 Text en © Andrzej Grzechnik et al. 2020 http://creativecommons.org/licenses/by/4.0/ This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.http://creativecommons.org/licenses/by/4.0/
spellingShingle Research Papers
Grzechnik, Andrzej
Meven, Martin
Paulmann, Carsten
Friese, Karen
Combined X-ray and neutron single-crystal diffraction in diamond anvil cells
title Combined X-ray and neutron single-crystal diffraction in diamond anvil cells
title_full Combined X-ray and neutron single-crystal diffraction in diamond anvil cells
title_fullStr Combined X-ray and neutron single-crystal diffraction in diamond anvil cells
title_full_unstemmed Combined X-ray and neutron single-crystal diffraction in diamond anvil cells
title_short Combined X-ray and neutron single-crystal diffraction in diamond anvil cells
title_sort combined x-ray and neutron single-crystal diffraction in diamond anvil cells
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6998780/
https://www.ncbi.nlm.nih.gov/pubmed/32047402
http://dx.doi.org/10.1107/S1600576719014201
work_keys_str_mv AT grzechnikandrzej combinedxrayandneutronsinglecrystaldiffractionindiamondanvilcells
AT mevenmartin combinedxrayandneutronsinglecrystaldiffractionindiamondanvilcells
AT paulmanncarsten combinedxrayandneutronsinglecrystaldiffractionindiamondanvilcells
AT friesekaren combinedxrayandneutronsinglecrystaldiffractionindiamondanvilcells

Ejemplares similares