Cargando…

Synthesis and crystal structures of a bis(3-hydroxy-cyclohex-2-en-1-one) and two hexahydroquinoline derivatives

The title compound I, 2,2′-[(2-nitrophenyl)methylene]bis(3-hydroxy-5,5-dimethylcyclohex-2-enone), C(23)H(27)NO(6), features a 1,3-ketone–enol conformation which is stabilized by two intramolecular hydrogen bonds. The most prominent intermolecular interactions in compound I are C—H⋯O hydro...

Descripción completa

Detalles Bibliográficos
Autores principales:	Steiger, Scott A., Li, Chun, Gates, Christina, Natale, Nicholas R.
Formato:	Online Artículo Texto
Lenguaje:	English
Publicado:	International Union of Crystallography 2020
Materias:	Research Communications
Acceso en línea:	https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7001840/ https://www.ncbi.nlm.nih.gov/pubmed/32071733 http://dx.doi.org/10.1107/S2056989019017018

Ejemplares similares

Synthesis, crystal structures, and Hirshfeld analysis of three hexahydroquinoline derivatives
por: Steiger, Scott A., et al.
Publicado: (2022)

3-Hydroxy-2-[(2E)-1-(2-hydroxy-6-oxocyclohex-1-en-1-yl)-3-(2-methoxyphenyl)prop-2-en-1-yl]cyclohex-2-en-1-one
por: Cha, Joo Hwan, et al.
Publicado: (2011)

(E)-3-Hydroxy-5,5-dimethyl-2-(3-phenylprop-2-en-1-yl)cyclohex-2-en-1-one
por: Zonouzi, Afsaneh, et al.
Publicado: (2011)

(6Z)-3,5-Bis(4-fluorophenyl)-6-(1-hydroxyethylidene)cyclohex-2-en-1-one
por: Jasinski, Jerry P., et al.
Publicado: (2012)

Dimethyl 2-(3-chlorophenyl)-6-hydroxy-6-methyl-4-(methylamino)cyclohex-3-ene-1,3-dicarboxylate
por: Amirthaganesan, S., et al.
Publicado: (2011)

3-Hydroxy-2-[(4-hydroxy-3,5-dimethoxyphenyl)(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-en-1-yl)methyl]-5,5-dimethylcyclohex-2-en-1-one
por: Yang, Xiao-Hui, et al.
Publicado: (2011)

3-Hydroxy-5,5-dimethyl-2-(2-oxopropyl)cyclohex-2-enone
por: Martínez, Roberto, et al.
Publicado: (2009)

Crystal structure of 3-hydroxy-2-(4-hydroxy-3-methoxyphenylmethyl)-5,5-dimethylcyclohex-2-enone
por: Stikute, Agnese, et al.
Publicado: (2018)

2,2′-[(3-Bromo-4-hydroxy-5-methoxyphenyl)methylidene]bis(3-hydroxy-5,5-dimethylcyclohex-2-en-1-one)
por: Sughanya, V., et al.
Publicado: (2012)

trans-Cyclohex-2-ene-1,4-diyl bis(4-nitrophenyl) dicarbonate
por: Nawazish Ali, Syed, et al.
Publicado: (2007)

Di-tert-butyl cyclohex-2-ene-1,4-diyl dicarbonate
por: Ali, Syed Nawazish, et al.
Publicado: (2009)

3-Methyl-5-(4-methylphenyl)cyclohex-2-enone
por: Mohan, R. T. Sabapathy, et al.
Publicado: (2008)

3-Methyl-5-(3-phenoxyphenyl)cyclohex-2-enone
por: Mohan, R. T. Sabapathy, et al.
Publicado: (2008)

Ethyl 4-(5-bromo-2-hydroxyphenyl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate
por: Kurbanova, Malahat M., et al.
Publicado: (2013)

7-Hydroxy-1,2,3,4-tetrahydroquinolin-2-one dihydrate
por: Zong, Qian-Shou, et al.
Publicado: (2012)

8-Hydroxy-5-(hydroxymethyl)quinolin-1-ium chloride
por: Fathi, Majda, et al.
Publicado: (2012)

3-Hydroxy-2-[(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-en-1-yl)(3-nitrophenyl)methyl]-5,5-dimethylcyclohex-2-en-1-one
por: Palakshi Reddy, B., et al.
Publicado: (2010)

Crystal structure of ethyl 4-[4-(dimethylamino)phenyl]-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate
por: Steiger, Scott A., et al.
Publicado: (2018)

3-[(1-Hydroxy-1-phenylpropan-2-yl)amino]-5,5-dimethylcyclohex-2-enone
por: Ghorab, Mostafa M., et al.
Publicado: (2012)

(E)-(2,4-Dichlorophenyl)[2-hydroxy-6-(methoxyimino)cyclohex-1-enyl]methanone
por: Huang, Guang-Dong, et al.
Publicado: (2009)

rac-Diethyl 6-hydroxy-4-[(2-hydroxyethyl)amino]-6-methyl-2-phenylcyclohex-3-ene-1,3-dicarboxylate
por: Maharramov, Abel M., et al.
Publicado: (2010)

N′-[(E)-2-Hydroxy-3,5-diiodobenzylidene]cyclohexane-1-carbohydrazide
por: Thirugnanasundar, A., et al.
Publicado: (2011)

(2E,6E)-2,6-Bis(4-methylbenzylidene)cyclohex-3-en-1-one
por: Abaee, M. Saeed, et al.
Publicado: (2012)

2,2′-[(4-Ethoxyphenyl)methylene]bis(3-hydroxy-5,5-dimethylcyclohex-2-en-1-one)
por: Sureshbabu, N., et al.
Publicado: (2012)

catena-Poly[[trimethyltin(IV)]-μ-cyclohex-3-ene-1-carboxylato]
por: Ren, Yun, et al.
Publicado: (2009)

2,5-Dimethyl-3-[4-(trifluoromethoxy)anilino]cyclohex-2-enone
por: North, Henry, et al.
Publicado: (2011)

12-(2-Hydroxy-6-oxocyclohex-1-enyl)-9,10-dihydro-8H-benzo[a]xanthen-11(12H)-one
por: Akkurt, Mehmet, et al.
Publicado: (2013)

Synthesis, characterization, crystal structure and Hirshfeld surface analysis of a hexahydroquinoline derivative: tert-butyl 4-([1,1′-biphenyl]-4-yl)-2,6,6-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate
por: Yıldırım, Sema Öztürk, et al.
Publicado: (2022)

1,3-Bis(3-tert-butyl-2-hydroxy-5-methoxybenzyl)hexahydropyrimidin-5-ol monohydrate
por: Rivera, Augusto, et al.
Publicado: (2014)

(5-Bromo-2-hydroxyphenyl)(4-propylcyclohexyl)methanone
por: Meng, Kang, et al.
Publicado: (2012)

Ethyl 4-(3-hydroxyphenyl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate
por: Mookiah, P., et al.
Publicado: (2009)

Crystal structure and DFT study of 8-hydroxy-1,2,3,5,6,7-hexahydropyrido[3,2,1-ij]quinoline-9-carbaldehyde
por: Faizi, Md. Serajul Haque, et al.
Publicado: (2017)

1-[(Z)-2-Butyltellanyl-1-chloroethenyl]cyclohex-1-ene
por: Zukerman-Schpector, Julio, et al.
Publicado: (2012)

4-Dichloromethyl-4-methyl-5-(nitromethyl)cyclohex-2-enone
por: Novaković, Sladjana B., et al.
Publicado: (2013)

(E)-4-(2-Chloro-1-hydroxy-2,6,6-trimethylcyclohexyl)but-3-en-2-one
por: Liu, Shan, et al.
Publicado: (2012)

3-Hydroxy-2,2-bis(1H-pyrazol-1-yl)cyclopentanone
por: Rybakov, Victor B., et al.
Publicado: (2012)

Bis(3-hydroxymethylanilinium) hexachloridostannate(IV)
por: Bouacida, Sofiane, et al.
Publicado: (2011)

Crystal structure of {[2-hydroxy-2-(3-methoxyphenyl)cyclohexyl]methyl}dimethylammonium benzoate
por: Sheshadri, S. N., et al.
Publicado: (2015)

4-(4-Chlorophenyl)-8-methyl-2-oxo-1,2,5,6,7,8-hexahydroquinoline-3-carbonitrile
por: Asiri, Abdullah M., et al.
Publicado: (2011)

8-Methyl-2-oxo-4-(thiophen-2-yl)-1,2,5,6,7,8-hexahydroquinoline-3-carbonitrile
por: Asiri, Abdullah M., et al.
Publicado: (2012)

Cannot write session to /tmp/vufind_sessions/sess_cn3nl4ud05p9gmt1ackqj3hq4o