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Structural, vibrational and optical studies on semiorganic crystals of boric acid potassium acetate
A semiorganic crystal of Boricacid potassium acetate has been grown by low temperature solution growth technique at room temperature using deionized water as a solvent. The crystalline nature of the compound was confirmed by the sharp and well defined peaks observed from the powder X-ray diffraction...
Autores principales: | , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Elsevier
2020
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7002783/ https://www.ncbi.nlm.nih.gov/pubmed/32042942 http://dx.doi.org/10.1016/j.heliyon.2019.e03133 |
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author | Kayalvizhi, C. Anand, S. Durga, R. Ebinezer, B. Samuel Sundararajan, R.S. |
author_facet | Kayalvizhi, C. Anand, S. Durga, R. Ebinezer, B. Samuel Sundararajan, R.S. |
author_sort | Kayalvizhi, C. |
collection | PubMed |
description | A semiorganic crystal of Boricacid potassium acetate has been grown by low temperature solution growth technique at room temperature using deionized water as a solvent. The crystalline nature of the compound was confirmed by the sharp and well defined peaks observed from the powder X-ray diffraction pattern. By single crystal X-ray diffraction method, the structure of the grown crystal has been studied. The Boric acid Potassium Acetate (BAPA) crystal has good optical transmittance in the entire UV visible region. FT-IR and FT-Raman spectral studies were performed to identify the vibrations of functional groups. The mechanical strength of the grown crystal was determined by Vicker's micro hardness test. Photoluminescence study was carried out on the crystal. The SHG study represents the nonlinear optical efficiency of the crystal. |
format | Online Article Text |
id | pubmed-7002783 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2020 |
publisher | Elsevier |
record_format | MEDLINE/PubMed |
spelling | pubmed-70027832020-02-10 Structural, vibrational and optical studies on semiorganic crystals of boric acid potassium acetate Kayalvizhi, C. Anand, S. Durga, R. Ebinezer, B. Samuel Sundararajan, R.S. Heliyon Article A semiorganic crystal of Boricacid potassium acetate has been grown by low temperature solution growth technique at room temperature using deionized water as a solvent. The crystalline nature of the compound was confirmed by the sharp and well defined peaks observed from the powder X-ray diffraction pattern. By single crystal X-ray diffraction method, the structure of the grown crystal has been studied. The Boric acid Potassium Acetate (BAPA) crystal has good optical transmittance in the entire UV visible region. FT-IR and FT-Raman spectral studies were performed to identify the vibrations of functional groups. The mechanical strength of the grown crystal was determined by Vicker's micro hardness test. Photoluminescence study was carried out on the crystal. The SHG study represents the nonlinear optical efficiency of the crystal. Elsevier 2020-01-06 /pmc/articles/PMC7002783/ /pubmed/32042942 http://dx.doi.org/10.1016/j.heliyon.2019.e03133 Text en © 2020 The Authors http://creativecommons.org/licenses/by-nc-nd/4.0/ This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/). |
spellingShingle | Article Kayalvizhi, C. Anand, S. Durga, R. Ebinezer, B. Samuel Sundararajan, R.S. Structural, vibrational and optical studies on semiorganic crystals of boric acid potassium acetate |
title | Structural, vibrational and optical studies on semiorganic crystals of boric acid potassium acetate |
title_full | Structural, vibrational and optical studies on semiorganic crystals of boric acid potassium acetate |
title_fullStr | Structural, vibrational and optical studies on semiorganic crystals of boric acid potassium acetate |
title_full_unstemmed | Structural, vibrational and optical studies on semiorganic crystals of boric acid potassium acetate |
title_short | Structural, vibrational and optical studies on semiorganic crystals of boric acid potassium acetate |
title_sort | structural, vibrational and optical studies on semiorganic crystals of boric acid potassium acetate |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7002783/ https://www.ncbi.nlm.nih.gov/pubmed/32042942 http://dx.doi.org/10.1016/j.heliyon.2019.e03133 |
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