Cargando…

Production of Oil-in-Water Emulsions with Varying Dispersed-Phase Content using Confined Impinging Jet Mixers

[Image: see text] This work reports for the first time on the use of Confined Impinging Jet Mixers (CIJM) for the production of emulsions with dispersed-phase content up to 80 wt %, in both the surfactant-poor and -rich regimes, following the exposure to varying CIJM hydrodynamic conditions. It was...

Descripción completa

Detalles Bibliográficos
Autores principales: Tripodi, Ernesto, Lazidis, Aristodimos, Norton, Ian T., Spyropoulos, Fotis
Formato: Online Artículo Texto
Lenguaje:English
Publicado: American Chemical Society 2019
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7011702/
https://www.ncbi.nlm.nih.gov/pubmed/32063670
http://dx.doi.org/10.1021/acs.iecr.9b00634
_version_ 1783496114205360128
author Tripodi, Ernesto
Lazidis, Aristodimos
Norton, Ian T.
Spyropoulos, Fotis
author_facet Tripodi, Ernesto
Lazidis, Aristodimos
Norton, Ian T.
Spyropoulos, Fotis
author_sort Tripodi, Ernesto
collection PubMed
description [Image: see text] This work reports for the first time on the use of Confined Impinging Jet Mixers (CIJM) for the production of emulsions with dispersed-phase content up to 80 wt %, in both the surfactant-poor and -rich regimes, following the exposure to varying CIJM hydrodynamic conditions. It was observed computationally and experimentally that the CIJM capacity resulted strictly dependent on the mass jet flow rate (W(jet) > 176 g/min) and the pre-emulsion droplet size (>10 μm). CIJM emulsification performance remained (almost) unaffected by the variation in the oil mass fraction. All systems showed the lowest droplet size (∼8 μm) and similar droplet size distributions under the highest W(jet). Conditionally onto the Tween20 availability, the emulsion d(3,2) was primarily determined by formulation characteristics in the surfactant poor-regime and by the CIJM energy dissipation rate in the surfactant-rich regime. In conclusion, this study offers further insights into the CIJM suitability as a realistic alternative to already-established emulsification methods.
format Online
Article
Text
id pubmed-7011702
institution National Center for Biotechnology Information
language English
publishDate 2019
publisher American Chemical Society
record_format MEDLINE/PubMed
spelling pubmed-70117022020-02-12 Production of Oil-in-Water Emulsions with Varying Dispersed-Phase Content using Confined Impinging Jet Mixers Tripodi, Ernesto Lazidis, Aristodimos Norton, Ian T. Spyropoulos, Fotis Ind Eng Chem Res [Image: see text] This work reports for the first time on the use of Confined Impinging Jet Mixers (CIJM) for the production of emulsions with dispersed-phase content up to 80 wt %, in both the surfactant-poor and -rich regimes, following the exposure to varying CIJM hydrodynamic conditions. It was observed computationally and experimentally that the CIJM capacity resulted strictly dependent on the mass jet flow rate (W(jet) > 176 g/min) and the pre-emulsion droplet size (>10 μm). CIJM emulsification performance remained (almost) unaffected by the variation in the oil mass fraction. All systems showed the lowest droplet size (∼8 μm) and similar droplet size distributions under the highest W(jet). Conditionally onto the Tween20 availability, the emulsion d(3,2) was primarily determined by formulation characteristics in the surfactant poor-regime and by the CIJM energy dissipation rate in the surfactant-rich regime. In conclusion, this study offers further insights into the CIJM suitability as a realistic alternative to already-established emulsification methods. American Chemical Society 2019-07-08 2019-08-14 /pmc/articles/PMC7011702/ /pubmed/32063670 http://dx.doi.org/10.1021/acs.iecr.9b00634 Text en Copyright © 2019 American Chemical Society This is an open access article published under a Creative Commons Attribution (CC-BY) License (http://pubs.acs.org/page/policy/authorchoice_ccby_termsofuse.html) , which permits unrestricted use, distribution and reproduction in any medium, provided the author and source are cited.
spellingShingle Tripodi, Ernesto
Lazidis, Aristodimos
Norton, Ian T.
Spyropoulos, Fotis
Production of Oil-in-Water Emulsions with Varying Dispersed-Phase Content using Confined Impinging Jet Mixers
title Production of Oil-in-Water Emulsions with Varying Dispersed-Phase Content using Confined Impinging Jet Mixers
title_full Production of Oil-in-Water Emulsions with Varying Dispersed-Phase Content using Confined Impinging Jet Mixers
title_fullStr Production of Oil-in-Water Emulsions with Varying Dispersed-Phase Content using Confined Impinging Jet Mixers
title_full_unstemmed Production of Oil-in-Water Emulsions with Varying Dispersed-Phase Content using Confined Impinging Jet Mixers
title_short Production of Oil-in-Water Emulsions with Varying Dispersed-Phase Content using Confined Impinging Jet Mixers
title_sort production of oil-in-water emulsions with varying dispersed-phase content using confined impinging jet mixers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7011702/
https://www.ncbi.nlm.nih.gov/pubmed/32063670
http://dx.doi.org/10.1021/acs.iecr.9b00634
work_keys_str_mv AT tripodiernesto productionofoilinwateremulsionswithvaryingdispersedphasecontentusingconfinedimpingingjetmixers
AT lazidisaristodimos productionofoilinwateremulsionswithvaryingdispersedphasecontentusingconfinedimpingingjetmixers
AT nortoniant productionofoilinwateremulsionswithvaryingdispersedphasecontentusingconfinedimpingingjetmixers
AT spyropoulosfotis productionofoilinwateremulsionswithvaryingdispersedphasecontentusingconfinedimpingingjetmixers