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A portable on-axis laser-heating system for near-90° X-ray spectroscopy: application to ferropericlase and iron silicide

A portable IR fiber laser-heating system, optimized for X-ray emission spectroscopy (XES) and nuclear inelastic scattering (NIS) spectroscopy with signal collection through the radial opening of diamond anvil cells near 90°with respect to the incident X-ray beam, is presented. The system offers doub...

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Autores principales: Spiekermann, Georg, Kupenko, Ilya, Petitgirard, Sylvain, Harder, Manuel, Nyrow, Alexander, Weis, Christopher, Albers, Christian, Biedermann, Nicole, Libon, Lélia, Sahle, Christoph J., Cerantola, Valerio, Glazyrin, Konstantin, Konôpková, Zuzana, Sinmyo, Ryosuke, Morgenroth, Wolfgang, Sergueev, Ilya, Yavaş, Hasan, Dubrovinsky, Leonid, Tolan, Metin, Sternemann, Christian, Wilke, Max
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2020
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7064108/
https://www.ncbi.nlm.nih.gov/pubmed/32153280
http://dx.doi.org/10.1107/S1600577519017041
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author Spiekermann, Georg
Kupenko, Ilya
Petitgirard, Sylvain
Harder, Manuel
Nyrow, Alexander
Weis, Christopher
Albers, Christian
Biedermann, Nicole
Libon, Lélia
Sahle, Christoph J.
Cerantola, Valerio
Glazyrin, Konstantin
Konôpková, Zuzana
Sinmyo, Ryosuke
Morgenroth, Wolfgang
Sergueev, Ilya
Yavaş, Hasan
Dubrovinsky, Leonid
Tolan, Metin
Sternemann, Christian
Wilke, Max
author_facet Spiekermann, Georg
Kupenko, Ilya
Petitgirard, Sylvain
Harder, Manuel
Nyrow, Alexander
Weis, Christopher
Albers, Christian
Biedermann, Nicole
Libon, Lélia
Sahle, Christoph J.
Cerantola, Valerio
Glazyrin, Konstantin
Konôpková, Zuzana
Sinmyo, Ryosuke
Morgenroth, Wolfgang
Sergueev, Ilya
Yavaş, Hasan
Dubrovinsky, Leonid
Tolan, Metin
Sternemann, Christian
Wilke, Max
author_sort Spiekermann, Georg
collection PubMed
description A portable IR fiber laser-heating system, optimized for X-ray emission spectroscopy (XES) and nuclear inelastic scattering (NIS) spectroscopy with signal collection through the radial opening of diamond anvil cells near 90°with respect to the incident X-ray beam, is presented. The system offers double-sided on-axis heating by a single laser source and zero attenuation of incoming X-rays other than by the high-pressure environment. A description of the system, which has been tested for pressures above 100 GPa and temperatures up to 3000 K, is given. The XES spectra of laser-heated Mg(0.67)Fe(0.33)O demonstrate the potential to map the iron spin state in the pressure–temperature range of the Earth’s lower mantle, and the NIS spectra of laser-heated FeSi give access to the sound velocity of this candidate of a phase inside the Earth’s core. This portable system represents one of the few bridges across the gap between laser heating and high-resolution X-ray spectroscopies with signal collection near 90°.
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spelling pubmed-70641082020-03-13 A portable on-axis laser-heating system for near-90° X-ray spectroscopy: application to ferropericlase and iron silicide Spiekermann, Georg Kupenko, Ilya Petitgirard, Sylvain Harder, Manuel Nyrow, Alexander Weis, Christopher Albers, Christian Biedermann, Nicole Libon, Lélia Sahle, Christoph J. Cerantola, Valerio Glazyrin, Konstantin Konôpková, Zuzana Sinmyo, Ryosuke Morgenroth, Wolfgang Sergueev, Ilya Yavaş, Hasan Dubrovinsky, Leonid Tolan, Metin Sternemann, Christian Wilke, Max J Synchrotron Radiat Research Papers A portable IR fiber laser-heating system, optimized for X-ray emission spectroscopy (XES) and nuclear inelastic scattering (NIS) spectroscopy with signal collection through the radial opening of diamond anvil cells near 90°with respect to the incident X-ray beam, is presented. The system offers double-sided on-axis heating by a single laser source and zero attenuation of incoming X-rays other than by the high-pressure environment. A description of the system, which has been tested for pressures above 100 GPa and temperatures up to 3000 K, is given. The XES spectra of laser-heated Mg(0.67)Fe(0.33)O demonstrate the potential to map the iron spin state in the pressure–temperature range of the Earth’s lower mantle, and the NIS spectra of laser-heated FeSi give access to the sound velocity of this candidate of a phase inside the Earth’s core. This portable system represents one of the few bridges across the gap between laser heating and high-resolution X-ray spectroscopies with signal collection near 90°. International Union of Crystallography 2020-02-13 /pmc/articles/PMC7064108/ /pubmed/32153280 http://dx.doi.org/10.1107/S1600577519017041 Text en © Spiekermann et al. 2020 http://creativecommons.org/licenses/by/4.0/ This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.http://creativecommons.org/licenses/by/4.0/
spellingShingle Research Papers
Spiekermann, Georg
Kupenko, Ilya
Petitgirard, Sylvain
Harder, Manuel
Nyrow, Alexander
Weis, Christopher
Albers, Christian
Biedermann, Nicole
Libon, Lélia
Sahle, Christoph J.
Cerantola, Valerio
Glazyrin, Konstantin
Konôpková, Zuzana
Sinmyo, Ryosuke
Morgenroth, Wolfgang
Sergueev, Ilya
Yavaş, Hasan
Dubrovinsky, Leonid
Tolan, Metin
Sternemann, Christian
Wilke, Max
A portable on-axis laser-heating system for near-90° X-ray spectroscopy: application to ferropericlase and iron silicide
title A portable on-axis laser-heating system for near-90° X-ray spectroscopy: application to ferropericlase and iron silicide
title_full A portable on-axis laser-heating system for near-90° X-ray spectroscopy: application to ferropericlase and iron silicide
title_fullStr A portable on-axis laser-heating system for near-90° X-ray spectroscopy: application to ferropericlase and iron silicide
title_full_unstemmed A portable on-axis laser-heating system for near-90° X-ray spectroscopy: application to ferropericlase and iron silicide
title_short A portable on-axis laser-heating system for near-90° X-ray spectroscopy: application to ferropericlase and iron silicide
title_sort portable on-axis laser-heating system for near-90° x-ray spectroscopy: application to ferropericlase and iron silicide
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7064108/
https://www.ncbi.nlm.nih.gov/pubmed/32153280
http://dx.doi.org/10.1107/S1600577519017041
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