Microwave-assisted synthesis of rhodamine derivatives

The microwave synthesis of 12 rhodamine-derived imines is described. The present work involves condensation of rhodamine hydrazide with various aromatic aldehydes in ethanol under microwave irradiation. The results obtained indicate that, unlike classical heating, microwave irradiation results in hi...

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Autores principales: Abebe, Fasil, Sutton, Treshaun, Perkins, Pierce, Makins-Dennis, Khalil, Winstead, Angela
Formato: Online Artículo Texto
Lenguaje:English
Publicado: 2018
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7082095/
https://www.ncbi.nlm.nih.gov/pubmed/32194653
http://dx.doi.org/10.1080/17518253.2018.1472814
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author Abebe, Fasil
Sutton, Treshaun
Perkins, Pierce
Makins-Dennis, Khalil
Winstead, Angela
author_facet Abebe, Fasil
Sutton, Treshaun
Perkins, Pierce
Makins-Dennis, Khalil
Winstead, Angela
author_sort Abebe, Fasil
collection PubMed
description The microwave synthesis of 12 rhodamine-derived imines is described. The present work involves condensation of rhodamine hydrazide with various aromatic aldehydes in ethanol under microwave irradiation. The results obtained indicate that, unlike classical heating, microwave irradiation results in higher yields, shorter reaction time, mild reaction condition and simple work-up procedure. The structures of synthesized compounds were confirmed by (1)H-NMR, (13)C-NMR, FT-IR and high-resolution mass spectra data.
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spelling pubmed-70820952020-03-19 Microwave-assisted synthesis of rhodamine derivatives Abebe, Fasil Sutton, Treshaun Perkins, Pierce Makins-Dennis, Khalil Winstead, Angela Green Chem Lett Rev Article The microwave synthesis of 12 rhodamine-derived imines is described. The present work involves condensation of rhodamine hydrazide with various aromatic aldehydes in ethanol under microwave irradiation. The results obtained indicate that, unlike classical heating, microwave irradiation results in higher yields, shorter reaction time, mild reaction condition and simple work-up procedure. The structures of synthesized compounds were confirmed by (1)H-NMR, (13)C-NMR, FT-IR and high-resolution mass spectra data. 2018-05-14 2018 /pmc/articles/PMC7082095/ /pubmed/32194653 http://dx.doi.org/10.1080/17518253.2018.1472814 Text en This is an Open Access article distributed under the terms of the Creative Commons Attribution License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
spellingShingle Article
Abebe, Fasil
Sutton, Treshaun
Perkins, Pierce
Makins-Dennis, Khalil
Winstead, Angela
Microwave-assisted synthesis of rhodamine derivatives
title Microwave-assisted synthesis of rhodamine derivatives
title_full Microwave-assisted synthesis of rhodamine derivatives
title_fullStr Microwave-assisted synthesis of rhodamine derivatives
title_full_unstemmed Microwave-assisted synthesis of rhodamine derivatives
title_short Microwave-assisted synthesis of rhodamine derivatives
title_sort microwave-assisted synthesis of rhodamine derivatives
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7082095/
https://www.ncbi.nlm.nih.gov/pubmed/32194653
http://dx.doi.org/10.1080/17518253.2018.1472814
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