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Optimized synthesis of aminooxy-peptides as glycoprobe precursors for surface-based sugar–protein interaction studies
An improved procedure for solid phase coupling of Boc-aminooxyacetic acid to peptides is described. By avoiding base-containing activation mixtures which cause over-acylation, it practically suppresses this unwanted side reaction and leads to near quantitative yields of Aoa-peptides, useful as glyco...
| Autores principales: | , , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
Elsevier Ltd.
2007
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7126385/ https://www.ncbi.nlm.nih.gov/pubmed/17629701 http://dx.doi.org/10.1016/j.bmcl.2007.06.090 |