Crystal structure of ethyl 2-(5-amino-1-benzene­sulfonyl-3-oxo-2,3-di­hydro-1H-pyrazol-2-yl)acetate

In the title compound, C(13)H(15)N(3)O(5)S, the two rings face each other in a ‘V′ form at the S atom, with one N—H⋯O=S and one C—H⋯O=S contact from the pyrazolyl substituents to the sulfonyl group. Two classical hydrogen bonds from the amine group, one of the form N—H⋯O=S and one N—H⋯O=C(oxo), link...

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Autores principales: Metwally, Nadia H., Elgemeie, Galal H., Jones, Peter G.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2020
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7133039/
https://www.ncbi.nlm.nih.gov/pubmed/32280488
http://dx.doi.org/10.1107/S2056989020002674
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author Metwally, Nadia H.
Elgemeie, Galal H.
Jones, Peter G.
author_facet Metwally, Nadia H.
Elgemeie, Galal H.
Jones, Peter G.
author_sort Metwally, Nadia H.
collection PubMed
description In the title compound, C(13)H(15)N(3)O(5)S, the two rings face each other in a ‘V′ form at the S atom, with one N—H⋯O=S and one C—H⋯O=S contact from the pyrazolyl substituents to the sulfonyl group. Two classical hydrogen bonds from the amine group, one of the form N—H⋯O=S and one N—H⋯O=C(oxo), link the mol­ecules to form layers parallel to the bc plane.
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spelling pubmed-71330392020-04-10 Crystal structure of ethyl 2-(5-amino-1-benzene­sulfonyl-3-oxo-2,3-di­hydro-1H-pyrazol-2-yl)acetate Metwally, Nadia H. Elgemeie, Galal H. Jones, Peter G. Acta Crystallogr E Crystallogr Commun Research Communications In the title compound, C(13)H(15)N(3)O(5)S, the two rings face each other in a ‘V′ form at the S atom, with one N—H⋯O=S and one C—H⋯O=S contact from the pyrazolyl substituents to the sulfonyl group. Two classical hydrogen bonds from the amine group, one of the form N—H⋯O=S and one N—H⋯O=C(oxo), link the mol­ecules to form layers parallel to the bc plane. International Union of Crystallography 2020-03-03 /pmc/articles/PMC7133039/ /pubmed/32280488 http://dx.doi.org/10.1107/S2056989020002674 Text en © Metwally et al. 2020 http://creativecommons.org/licenses/by/4.0/ This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.http://creativecommons.org/licenses/by/4.0/
spellingShingle Research Communications
Metwally, Nadia H.
Elgemeie, Galal H.
Jones, Peter G.
Crystal structure of ethyl 2-(5-amino-1-benzene­sulfonyl-3-oxo-2,3-di­hydro-1H-pyrazol-2-yl)acetate
title Crystal structure of ethyl 2-(5-amino-1-benzene­sulfonyl-3-oxo-2,3-di­hydro-1H-pyrazol-2-yl)acetate
title_full Crystal structure of ethyl 2-(5-amino-1-benzene­sulfonyl-3-oxo-2,3-di­hydro-1H-pyrazol-2-yl)acetate
title_fullStr Crystal structure of ethyl 2-(5-amino-1-benzene­sulfonyl-3-oxo-2,3-di­hydro-1H-pyrazol-2-yl)acetate
title_full_unstemmed Crystal structure of ethyl 2-(5-amino-1-benzene­sulfonyl-3-oxo-2,3-di­hydro-1H-pyrazol-2-yl)acetate
title_short Crystal structure of ethyl 2-(5-amino-1-benzene­sulfonyl-3-oxo-2,3-di­hydro-1H-pyrazol-2-yl)acetate
title_sort crystal structure of ethyl 2-(5-amino-1-benzene­sulfonyl-3-oxo-2,3-di­hydro-1h-pyrazol-2-yl)acetate
topic Research Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7133039/
https://www.ncbi.nlm.nih.gov/pubmed/32280488
http://dx.doi.org/10.1107/S2056989020002674
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