Synthesis and Characterization of H(3)PW(12)O(40) and H(3)PMo(12)O(40) Nanoparticles by a Simple Method

In this study H(3)PW(12)O(40)·9H(2)O and H(3)PMo(12)O(40)·6H(2)O (HPA) particles were changed into nano forms by heat-treatment in an autoclave as a simple, repaid, inexpensive and one step method. The particle size of these nanoparticles was around 25 nm. The as-synthesized nanostructures were char...

Descripción completa

Detalles Bibliográficos
Autores principales: Javidi, Jaber, Esmaeilpour, Mohsen, Rahiminezhad, Zahra, Dodeji, Fatemeh Nowroozi
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Springer US 2014
Materias:
Original Paper
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7189835/
https://www.ncbi.nlm.nih.gov/pubmed/32362736
http://dx.doi.org/10.1007/s10876-014-0745-x
_version_ 1783527573073952768
author Javidi, Jaber
Esmaeilpour, Mohsen
Rahiminezhad, Zahra
Dodeji, Fatemeh Nowroozi
author_facet Javidi, Jaber
Esmaeilpour, Mohsen
Rahiminezhad, Zahra
Dodeji, Fatemeh Nowroozi
author_sort Javidi, Jaber
collection PubMed
description In this study H(3)PW(12)O(40)·9H(2)O and H(3)PMo(12)O(40)·6H(2)O (HPA) particles were changed into nano forms by heat-treatment in an autoclave as a simple, repaid, inexpensive and one step method. The particle size of these nanoparticles was around 25 nm. The as-synthesized nanostructures were characterized by dynamic light scattering, X-ray powder diffraction, transmission electron microscopy, Fourier transform infrared spectroscopy and inductively coupled plasma analyzer. Thermal stability of nanoparticles was surveyed by thermal gravimeter analyse. Acidity of prepared nanoparticles was investigated by pyridine adsorption method. Results showed rising acidity by declining particle size of HPA.
format Online
Article
Text
id pubmed-7189835
institution National Center for Biotechnology Information
language English
publishDate 2014
publisher Springer US
record_format MEDLINE/PubMed
spelling pubmed-71898352020-04-29 Synthesis and Characterization of H(3)PW(12)O(40) and H(3)PMo(12)O(40) Nanoparticles by a Simple Method Javidi, Jaber Esmaeilpour, Mohsen Rahiminezhad, Zahra Dodeji, Fatemeh Nowroozi J Clust Sci Original Paper In this study H(3)PW(12)O(40)·9H(2)O and H(3)PMo(12)O(40)·6H(2)O (HPA) particles were changed into nano forms by heat-treatment in an autoclave as a simple, repaid, inexpensive and one step method. The particle size of these nanoparticles was around 25 nm. The as-synthesized nanostructures were characterized by dynamic light scattering, X-ray powder diffraction, transmission electron microscopy, Fourier transform infrared spectroscopy and inductively coupled plasma analyzer. Thermal stability of nanoparticles was surveyed by thermal gravimeter analyse. Acidity of prepared nanoparticles was investigated by pyridine adsorption method. Results showed rising acidity by declining particle size of HPA. Springer US 2014-06-18 2014 /pmc/articles/PMC7189835/ /pubmed/32362736 http://dx.doi.org/10.1007/s10876-014-0745-x Text en © Springer Science+Business Media New York 2014 This article is made available via the PMC Open Access Subset for unrestricted research re-use and secondary analysis in any form or by any means with acknowledgement of the original source. These permissions are granted for the duration of the World Health Organization (WHO) declaration of COVID-19 as a global pandemic.
spellingShingle Original Paper
Javidi, Jaber
Esmaeilpour, Mohsen
Rahiminezhad, Zahra
Dodeji, Fatemeh Nowroozi
Synthesis and Characterization of H(3)PW(12)O(40) and H(3)PMo(12)O(40) Nanoparticles by a Simple Method
title Synthesis and Characterization of H(3)PW(12)O(40) and H(3)PMo(12)O(40) Nanoparticles by a Simple Method
title_full Synthesis and Characterization of H(3)PW(12)O(40) and H(3)PMo(12)O(40) Nanoparticles by a Simple Method
title_fullStr Synthesis and Characterization of H(3)PW(12)O(40) and H(3)PMo(12)O(40) Nanoparticles by a Simple Method
title_full_unstemmed Synthesis and Characterization of H(3)PW(12)O(40) and H(3)PMo(12)O(40) Nanoparticles by a Simple Method
title_short Synthesis and Characterization of H(3)PW(12)O(40) and H(3)PMo(12)O(40) Nanoparticles by a Simple Method
title_sort synthesis and characterization of h(3)pw(12)o(40) and h(3)pmo(12)o(40) nanoparticles by a simple method
topic Original Paper
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7189835/
https://www.ncbi.nlm.nih.gov/pubmed/32362736
http://dx.doi.org/10.1007/s10876-014-0745-x
work_keys_str_mv AT javidijaber synthesisandcharacterizationofh3pw12o40andh3pmo12o40nanoparticlesbyasimplemethod
AT esmaeilpourmohsen synthesisandcharacterizationofh3pw12o40andh3pmo12o40nanoparticlesbyasimplemethod
AT rahiminezhadzahra synthesisandcharacterizationofh3pw12o40andh3pmo12o40nanoparticlesbyasimplemethod
AT dodejifatemehnowroozi synthesisandcharacterizationofh3pw12o40andh3pmo12o40nanoparticlesbyasimplemethod

Ejemplares similares