Cargando…

Dry Cold Forging of Pure Titanium Wire to Thin Plate with Use of β-SiC Coating Dies

Dense β-SiC coating with 3C-structure was utilized as a dry cold forging punch and core-die. Pure titanium T328H wires of industrial grade II were employed as a work material. No adhesion or galling of metallic titanium was detected on the contact interface between this β-SiC die and titanium work,...

Descripción completa

Detalles Bibliográficos
Autores principales: Aizawa, Tatsuhiko, Yoshino, Tomoaki, Fukuda, Tatsuya, Shiratori, Tomomi
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2020
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7504516/
https://www.ncbi.nlm.nih.gov/pubmed/32867120
http://dx.doi.org/10.3390/ma13173780
_version_ 1783584642878668800
author Aizawa, Tatsuhiko
Yoshino, Tomoaki
Fukuda, Tatsuya
Shiratori, Tomomi
author_facet Aizawa, Tatsuhiko
Yoshino, Tomoaki
Fukuda, Tatsuya
Shiratori, Tomomi
author_sort Aizawa, Tatsuhiko
collection PubMed
description Dense β-SiC coating with 3C-structure was utilized as a dry cold forging punch and core-die. Pure titanium T328H wires of industrial grade II were employed as a work material. No adhesion or galling of metallic titanium was detected on the contact interface between this β-SiC die and titanium work, even after this continuous forging process, up to a reduction in thickness by 70%. SEM (Scanning Electron Microscopy) and EDX (Electron Dispersive X-ray spectroscopy) were utilized to analyze this contact interface. A very thin titanium oxide layer was in situ formed in the radial direction from the center of the contact interface. Isolated carbon from β-SiC agglomerated and distributed in dots at the center of the initial contact interface. Raman spectroscopy was utilized, yielding the discovery that this carbon is unbound as a free carbon or not bound in SiC or TiC and that intermediate titanium oxides are formed with TiO(2) as a tribofilm.
format Online
Article
Text
id pubmed-7504516
institution National Center for Biotechnology Information
language English
publishDate 2020
publisher MDPI
record_format MEDLINE/PubMed
spelling pubmed-75045162020-09-24 Dry Cold Forging of Pure Titanium Wire to Thin Plate with Use of β-SiC Coating Dies Aizawa, Tatsuhiko Yoshino, Tomoaki Fukuda, Tatsuya Shiratori, Tomomi Materials (Basel) Article Dense β-SiC coating with 3C-structure was utilized as a dry cold forging punch and core-die. Pure titanium T328H wires of industrial grade II were employed as a work material. No adhesion or galling of metallic titanium was detected on the contact interface between this β-SiC die and titanium work, even after this continuous forging process, up to a reduction in thickness by 70%. SEM (Scanning Electron Microscopy) and EDX (Electron Dispersive X-ray spectroscopy) were utilized to analyze this contact interface. A very thin titanium oxide layer was in situ formed in the radial direction from the center of the contact interface. Isolated carbon from β-SiC agglomerated and distributed in dots at the center of the initial contact interface. Raman spectroscopy was utilized, yielding the discovery that this carbon is unbound as a free carbon or not bound in SiC or TiC and that intermediate titanium oxides are formed with TiO(2) as a tribofilm. MDPI 2020-08-27 /pmc/articles/PMC7504516/ /pubmed/32867120 http://dx.doi.org/10.3390/ma13173780 Text en © 2020 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Aizawa, Tatsuhiko
Yoshino, Tomoaki
Fukuda, Tatsuya
Shiratori, Tomomi
Dry Cold Forging of Pure Titanium Wire to Thin Plate with Use of β-SiC Coating Dies
title Dry Cold Forging of Pure Titanium Wire to Thin Plate with Use of β-SiC Coating Dies
title_full Dry Cold Forging of Pure Titanium Wire to Thin Plate with Use of β-SiC Coating Dies
title_fullStr Dry Cold Forging of Pure Titanium Wire to Thin Plate with Use of β-SiC Coating Dies
title_full_unstemmed Dry Cold Forging of Pure Titanium Wire to Thin Plate with Use of β-SiC Coating Dies
title_short Dry Cold Forging of Pure Titanium Wire to Thin Plate with Use of β-SiC Coating Dies
title_sort dry cold forging of pure titanium wire to thin plate with use of β-sic coating dies
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7504516/
https://www.ncbi.nlm.nih.gov/pubmed/32867120
http://dx.doi.org/10.3390/ma13173780
work_keys_str_mv AT aizawatatsuhiko drycoldforgingofpuretitaniumwiretothinplatewithuseofbsiccoatingdies
AT yoshinotomoaki drycoldforgingofpuretitaniumwiretothinplatewithuseofbsiccoatingdies
AT fukudatatsuya drycoldforgingofpuretitaniumwiretothinplatewithuseofbsiccoatingdies
AT shiratoritomomi drycoldforgingofpuretitaniumwiretothinplatewithuseofbsiccoatingdies