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Dry Cold Forging of Pure Titanium Wire to Thin Plate with Use of β-SiC Coating Dies
Dense β-SiC coating with 3C-structure was utilized as a dry cold forging punch and core-die. Pure titanium T328H wires of industrial grade II were employed as a work material. No adhesion or galling of metallic titanium was detected on the contact interface between this β-SiC die and titanium work,...
Autores principales: | , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2020
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7504516/ https://www.ncbi.nlm.nih.gov/pubmed/32867120 http://dx.doi.org/10.3390/ma13173780 |
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author | Aizawa, Tatsuhiko Yoshino, Tomoaki Fukuda, Tatsuya Shiratori, Tomomi |
author_facet | Aizawa, Tatsuhiko Yoshino, Tomoaki Fukuda, Tatsuya Shiratori, Tomomi |
author_sort | Aizawa, Tatsuhiko |
collection | PubMed |
description | Dense β-SiC coating with 3C-structure was utilized as a dry cold forging punch and core-die. Pure titanium T328H wires of industrial grade II were employed as a work material. No adhesion or galling of metallic titanium was detected on the contact interface between this β-SiC die and titanium work, even after this continuous forging process, up to a reduction in thickness by 70%. SEM (Scanning Electron Microscopy) and EDX (Electron Dispersive X-ray spectroscopy) were utilized to analyze this contact interface. A very thin titanium oxide layer was in situ formed in the radial direction from the center of the contact interface. Isolated carbon from β-SiC agglomerated and distributed in dots at the center of the initial contact interface. Raman spectroscopy was utilized, yielding the discovery that this carbon is unbound as a free carbon or not bound in SiC or TiC and that intermediate titanium oxides are formed with TiO(2) as a tribofilm. |
format | Online Article Text |
id | pubmed-7504516 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2020 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-75045162020-09-24 Dry Cold Forging of Pure Titanium Wire to Thin Plate with Use of β-SiC Coating Dies Aizawa, Tatsuhiko Yoshino, Tomoaki Fukuda, Tatsuya Shiratori, Tomomi Materials (Basel) Article Dense β-SiC coating with 3C-structure was utilized as a dry cold forging punch and core-die. Pure titanium T328H wires of industrial grade II were employed as a work material. No adhesion or galling of metallic titanium was detected on the contact interface between this β-SiC die and titanium work, even after this continuous forging process, up to a reduction in thickness by 70%. SEM (Scanning Electron Microscopy) and EDX (Electron Dispersive X-ray spectroscopy) were utilized to analyze this contact interface. A very thin titanium oxide layer was in situ formed in the radial direction from the center of the contact interface. Isolated carbon from β-SiC agglomerated and distributed in dots at the center of the initial contact interface. Raman spectroscopy was utilized, yielding the discovery that this carbon is unbound as a free carbon or not bound in SiC or TiC and that intermediate titanium oxides are formed with TiO(2) as a tribofilm. MDPI 2020-08-27 /pmc/articles/PMC7504516/ /pubmed/32867120 http://dx.doi.org/10.3390/ma13173780 Text en © 2020 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Aizawa, Tatsuhiko Yoshino, Tomoaki Fukuda, Tatsuya Shiratori, Tomomi Dry Cold Forging of Pure Titanium Wire to Thin Plate with Use of β-SiC Coating Dies |
title | Dry Cold Forging of Pure Titanium Wire to Thin Plate with Use of β-SiC Coating Dies |
title_full | Dry Cold Forging of Pure Titanium Wire to Thin Plate with Use of β-SiC Coating Dies |
title_fullStr | Dry Cold Forging of Pure Titanium Wire to Thin Plate with Use of β-SiC Coating Dies |
title_full_unstemmed | Dry Cold Forging of Pure Titanium Wire to Thin Plate with Use of β-SiC Coating Dies |
title_short | Dry Cold Forging of Pure Titanium Wire to Thin Plate with Use of β-SiC Coating Dies |
title_sort | dry cold forging of pure titanium wire to thin plate with use of β-sic coating dies |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7504516/ https://www.ncbi.nlm.nih.gov/pubmed/32867120 http://dx.doi.org/10.3390/ma13173780 |
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