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Influence of Sintering Process on Microstructure and Mechanical Properties of Ti(C,N)-Based Cermet

In this study, a Ti(C,N)-based cermet material was prepared through vacuum sintering. The research also investigates how holding time and maximum sintering temperature influence the material microstructure and mechanical properties. X-ray diffraction (XRD), energy dispersive spectroscopy (EDS) were...

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Detalles Bibliográficos
Autores principales: Ji, Kaixun, Meng, Yanxin, Wang, Fuzeng, Li, Yousheng
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2020
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7559298/
https://www.ncbi.nlm.nih.gov/pubmed/32899590
http://dx.doi.org/10.3390/ma13183938
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author Ji, Kaixun
Meng, Yanxin
Wang, Fuzeng
Li, Yousheng
author_facet Ji, Kaixun
Meng, Yanxin
Wang, Fuzeng
Li, Yousheng
author_sort Ji, Kaixun
collection PubMed
description In this study, a Ti(C,N)-based cermet material was prepared through vacuum sintering. The research also investigates how holding time and maximum sintering temperature influence the material microstructure and mechanical properties. X-ray diffraction (XRD), energy dispersive spectroscopy (EDS) were used to analyze the composition of the cermet. The microstructure of the cermet was analyzed and examined using a scanning electron microscope (SEM). A Vickers hardness tester was used to test the mechanical properties of the materials. As indicated by testing results, the hardness of the material decreases as the temperature of sintering increases, and its fracture toughness increases gradually as holding time increases. Ti(C,N)-based cermet manifested the optimal mechanical properties when sintering was conducted under 1400 °C with 80 min of holding time. Moreover, the material microstructure is significantly affected by the sintering process. The grain size of Ti(C,N) cermets increases as the sintering temperature increases. The microstructure tends to be uniform and the complete core-rim structures are established as the holding time increases.
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spelling pubmed-75592982020-10-29 Influence of Sintering Process on Microstructure and Mechanical Properties of Ti(C,N)-Based Cermet Ji, Kaixun Meng, Yanxin Wang, Fuzeng Li, Yousheng Materials (Basel) Article In this study, a Ti(C,N)-based cermet material was prepared through vacuum sintering. The research also investigates how holding time and maximum sintering temperature influence the material microstructure and mechanical properties. X-ray diffraction (XRD), energy dispersive spectroscopy (EDS) were used to analyze the composition of the cermet. The microstructure of the cermet was analyzed and examined using a scanning electron microscope (SEM). A Vickers hardness tester was used to test the mechanical properties of the materials. As indicated by testing results, the hardness of the material decreases as the temperature of sintering increases, and its fracture toughness increases gradually as holding time increases. Ti(C,N)-based cermet manifested the optimal mechanical properties when sintering was conducted under 1400 °C with 80 min of holding time. Moreover, the material microstructure is significantly affected by the sintering process. The grain size of Ti(C,N) cermets increases as the sintering temperature increases. The microstructure tends to be uniform and the complete core-rim structures are established as the holding time increases. MDPI 2020-09-05 /pmc/articles/PMC7559298/ /pubmed/32899590 http://dx.doi.org/10.3390/ma13183938 Text en © 2020 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Ji, Kaixun
Meng, Yanxin
Wang, Fuzeng
Li, Yousheng
Influence of Sintering Process on Microstructure and Mechanical Properties of Ti(C,N)-Based Cermet
title Influence of Sintering Process on Microstructure and Mechanical Properties of Ti(C,N)-Based Cermet
title_full Influence of Sintering Process on Microstructure and Mechanical Properties of Ti(C,N)-Based Cermet
title_fullStr Influence of Sintering Process on Microstructure and Mechanical Properties of Ti(C,N)-Based Cermet
title_full_unstemmed Influence of Sintering Process on Microstructure and Mechanical Properties of Ti(C,N)-Based Cermet
title_short Influence of Sintering Process on Microstructure and Mechanical Properties of Ti(C,N)-Based Cermet
title_sort influence of sintering process on microstructure and mechanical properties of ti(c,n)-based cermet
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7559298/
https://www.ncbi.nlm.nih.gov/pubmed/32899590
http://dx.doi.org/10.3390/ma13183938
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AT liyousheng influenceofsinteringprocessonmicrostructureandmechanicalpropertiesofticnbasedcermet