Supporting dataset on the optimization and validation of a QuEChERS-based method for the determination of 218 pesticide residues in clay loam soil

The dataset presented in this article supports “Optimization and validation of a method for the simultaneous environmental monitoring of 218 pesticide residues in clay loam soil” [1]. A method based on QuEChERS (Quick, Easy, Cheap, Effective, Rugged & Safe) for the extraction of pesticide and so...

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Detalles Bibliográficos
Autores principales: Acosta-Dacal, Andrea, Rial-Berriel, Cristian, Díaz-Díaz, Ricardo, Bernal Suárez, Mª del Mar, Zumbado, Manuel, Henríquez-Hernández, Luis Alberto, Luzardo, Octavio P.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2020
Materias:
Data Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7596106/
https://www.ncbi.nlm.nih.gov/pubmed/33145377
http://dx.doi.org/10.1016/j.dib.2020.106393
Descripción
Sumario:The dataset presented in this article supports “Optimization and validation of a method for the simultaneous environmental monitoring of 218 pesticide residues in clay loam soil” [1]. A method based on QuEChERS (Quick, Easy, Cheap, Effective, Rugged & Safe) for the extraction of pesticide and some metabolites residues was developed. The quantification of the chemicals was performed by a combination of two complementary LC-MS/MS and GC–MS/MS analyses. Detailed optimization data of the QuEChERS extraction method is provided, including (1) salt combination, (2) acidification of the solvent (3) the amount of the selected acid (Formic Acid, FA) and (4) moisturization of the soil samples prior to extraction. In addition, all the validation data are presented, including the matrix effect, which was evaluated for each analyte using the recommended procedure.

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