Crystal structure of 2,6-bis­(3-hy­droxy-3-methyl­but-1-yn-1-yl)pyridine monohydrate

In the title pyridine derivative, C(15)H(17)NO(2)·H(2)O, the two OH groups are oriented in directions opposite to each other with respect to the plane of the pyridine ring. In the crystal, hydrogen bonds between the pyridine mol­ecule and the water mol­ecule, viz. O(hy­droxy)—H⋯O(water), O(hy­droxy)...

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Detalles Bibliográficos
Autores principales: Koizumi, Take-aki, Takata, Toshikazu
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2020
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7643226/
https://www.ncbi.nlm.nih.gov/pubmed/33209344
http://dx.doi.org/10.1107/S2056989020013304
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author Koizumi, Take-aki
Takata, Toshikazu
author_facet Koizumi, Take-aki
Takata, Toshikazu
author_sort Koizumi, Take-aki
collection PubMed
description In the title pyridine derivative, C(15)H(17)NO(2)·H(2)O, the two OH groups are oriented in directions opposite to each other with respect to the plane of the pyridine ring. In the crystal, hydrogen bonds between the pyridine mol­ecule and the water mol­ecule, viz. O(hy­droxy)—H⋯O(water), O(hy­droxy)—H⋯O(hy­droxy), O(water)—H⋯O(hy­droxy) and O(water)—H···N(pyridine), result in the formation of a ribbon-like structure running along [011].
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spelling pubmed-76432262020-11-17 Crystal structure of 2,6-bis­(3-hy­droxy-3-methyl­but-1-yn-1-yl)pyridine monohydrate Koizumi, Take-aki Takata, Toshikazu Acta Crystallogr E Crystallogr Commun Research Communications In the title pyridine derivative, C(15)H(17)NO(2)·H(2)O, the two OH groups are oriented in directions opposite to each other with respect to the plane of the pyridine ring. In the crystal, hydrogen bonds between the pyridine mol­ecule and the water mol­ecule, viz. O(hy­droxy)—H⋯O(water), O(hy­droxy)—H⋯O(hy­droxy), O(water)—H⋯O(hy­droxy) and O(water)—H···N(pyridine), result in the formation of a ribbon-like structure running along [011]. International Union of Crystallography 2020-10-09 /pmc/articles/PMC7643226/ /pubmed/33209344 http://dx.doi.org/10.1107/S2056989020013304 Text en © Koizumi and Takata 2020 http://creativecommons.org/licenses/by/4.0/ This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.http://creativecommons.org/licenses/by/4.0/
spellingShingle Research Communications
Koizumi, Take-aki
Takata, Toshikazu
Crystal structure of 2,6-bis­(3-hy­droxy-3-methyl­but-1-yn-1-yl)pyridine monohydrate
title Crystal structure of 2,6-bis­(3-hy­droxy-3-methyl­but-1-yn-1-yl)pyridine monohydrate
title_full Crystal structure of 2,6-bis­(3-hy­droxy-3-methyl­but-1-yn-1-yl)pyridine monohydrate
title_fullStr Crystal structure of 2,6-bis­(3-hy­droxy-3-methyl­but-1-yn-1-yl)pyridine monohydrate
title_full_unstemmed Crystal structure of 2,6-bis­(3-hy­droxy-3-methyl­but-1-yn-1-yl)pyridine monohydrate
title_short Crystal structure of 2,6-bis­(3-hy­droxy-3-methyl­but-1-yn-1-yl)pyridine monohydrate
title_sort crystal structure of 2,6-bis­(3-hy­droxy-3-methyl­but-1-yn-1-yl)pyridine monohydrate
topic Research Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7643226/
https://www.ncbi.nlm.nih.gov/pubmed/33209344
http://dx.doi.org/10.1107/S2056989020013304
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AT takatatoshikazu crystalstructureof26bis3hydroxy3methylbut1yn1ylpyridinemonohydrate

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