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Preparation and Characterisation of Activated Carbon from Palm Mixed Waste Treated with Trona Ore

This study explores the use of a novel activating agent and demonstrates the production and characterisation of activated carbon (AC) from a combine palm waste (CPW) in 3:2:1 proportion by weight of empty fruit bunch, mesocarp fibre and palm kernel shell. The resulting biomass was processed by a mic...

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Detalles Bibliográficos
Autores principales: Ukanwa, Kalu Samuel, Patchigolla, Kumar, Sakrabani, Ruben, Anthony, Edward
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2020
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7663104/
https://www.ncbi.nlm.nih.gov/pubmed/33138276
http://dx.doi.org/10.3390/molecules25215028
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author Ukanwa, Kalu Samuel
Patchigolla, Kumar
Sakrabani, Ruben
Anthony, Edward
author_facet Ukanwa, Kalu Samuel
Patchigolla, Kumar
Sakrabani, Ruben
Anthony, Edward
author_sort Ukanwa, Kalu Samuel
collection PubMed
description This study explores the use of a novel activating agent and demonstrates the production and characterisation of activated carbon (AC) from a combine palm waste (CPW) in 3:2:1 proportion by weight of empty fruit bunch, mesocarp fibre and palm kernel shell. The resulting biomass was processed by a microwave-assisted method using trona and compared with material produced by conventional routes. These results demonstrate the potential of trona ore as an activating agent and the effectiveness of using a combined palm waste for a single stream activation process. It also assesses the effectiveness of trona ore in the elimination of alcohol, acids and aldehydes; with a focus on increasing the hydrophilicity of the resultant AC. The optimum results for the conventional production technique at 800 °C yielded a material with S(BET) 920 m(2)/g, V(total) 0.840 cm(3)/g, a mean pore diameter of 2.2 nm and an AC yield 40%. The optimum outcome of the microwave assisted technique for CPW was achieved at 600 W, S(BET) is 980 m(2)/g; V(total) 0.865 cm(3)/g; a mean pore diameter 2.2 nm and an AC yield of 42%. Fourier transform infrared spectrometry analyses showed that palm waste can be combined to produce AC and that trona ore has the capacity to significantly enhance biomass activation.
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spelling pubmed-76631042020-11-14 Preparation and Characterisation of Activated Carbon from Palm Mixed Waste Treated with Trona Ore Ukanwa, Kalu Samuel Patchigolla, Kumar Sakrabani, Ruben Anthony, Edward Molecules Article This study explores the use of a novel activating agent and demonstrates the production and characterisation of activated carbon (AC) from a combine palm waste (CPW) in 3:2:1 proportion by weight of empty fruit bunch, mesocarp fibre and palm kernel shell. The resulting biomass was processed by a microwave-assisted method using trona and compared with material produced by conventional routes. These results demonstrate the potential of trona ore as an activating agent and the effectiveness of using a combined palm waste for a single stream activation process. It also assesses the effectiveness of trona ore in the elimination of alcohol, acids and aldehydes; with a focus on increasing the hydrophilicity of the resultant AC. The optimum results for the conventional production technique at 800 °C yielded a material with S(BET) 920 m(2)/g, V(total) 0.840 cm(3)/g, a mean pore diameter of 2.2 nm and an AC yield 40%. The optimum outcome of the microwave assisted technique for CPW was achieved at 600 W, S(BET) is 980 m(2)/g; V(total) 0.865 cm(3)/g; a mean pore diameter 2.2 nm and an AC yield of 42%. Fourier transform infrared spectrometry analyses showed that palm waste can be combined to produce AC and that trona ore has the capacity to significantly enhance biomass activation. MDPI 2020-10-29 /pmc/articles/PMC7663104/ /pubmed/33138276 http://dx.doi.org/10.3390/molecules25215028 Text en © 2020 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Ukanwa, Kalu Samuel
Patchigolla, Kumar
Sakrabani, Ruben
Anthony, Edward
Preparation and Characterisation of Activated Carbon from Palm Mixed Waste Treated with Trona Ore
title Preparation and Characterisation of Activated Carbon from Palm Mixed Waste Treated with Trona Ore
title_full Preparation and Characterisation of Activated Carbon from Palm Mixed Waste Treated with Trona Ore
title_fullStr Preparation and Characterisation of Activated Carbon from Palm Mixed Waste Treated with Trona Ore
title_full_unstemmed Preparation and Characterisation of Activated Carbon from Palm Mixed Waste Treated with Trona Ore
title_short Preparation and Characterisation of Activated Carbon from Palm Mixed Waste Treated with Trona Ore
title_sort preparation and characterisation of activated carbon from palm mixed waste treated with trona ore
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7663104/
https://www.ncbi.nlm.nih.gov/pubmed/33138276
http://dx.doi.org/10.3390/molecules25215028
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