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Methods of investigation transformation kinetics of yttrium carbonate hydroxide in citric acid solution into yttrium citrate dihydrate
A method of synthesis crystalline yttrium citrate dihydrate was proposed as a result of the transformation of the freshly precipitated basic yttrium carbonate phase in a citric acid solution. The synthesis time was determined on the basis of composition analysis, structure and thermogravimetric stud...
Autores principales: | , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Elsevier
2020
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7725940/ https://www.ncbi.nlm.nih.gov/pubmed/33318957 http://dx.doi.org/10.1016/j.mex.2020.101153 |
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author | Janusz, W. Skwarek, E. Sternik, D. Pikus, S. Pawlak, D. Parus, J.L. Mikołajczak, R. |
author_facet | Janusz, W. Skwarek, E. Sternik, D. Pikus, S. Pawlak, D. Parus, J.L. Mikołajczak, R. |
author_sort | Janusz, W. |
collection | PubMed |
description | A method of synthesis crystalline yttrium citrate dihydrate was proposed as a result of the transformation of the freshly precipitated basic yttrium carbonate phase in a citric acid solution. The synthesis time was determined on the basis of composition analysis, structure and thermogravimetric studies of samples taken during the synthesis. The research methods used have shown that in the initial stage of the synthesis, the processes of citric acid sorption on basic yttrium carbonate and transformation of amorphous yttrium carbonate hydroxide into crystalline yttrium hydroxide occurs. It is only after 72 h of synthesis that the crystalline yttrium citrate dihydrate is formed. • Synthesis crystalline yttrium citrate dehydrate. • The synthesis time 72 h. • Synthesis components: the freshly precipitated basic yttrium carbonate phase in a citric acid solution. |
format | Online Article Text |
id | pubmed-7725940 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2020 |
publisher | Elsevier |
record_format | MEDLINE/PubMed |
spelling | pubmed-77259402020-12-13 Methods of investigation transformation kinetics of yttrium carbonate hydroxide in citric acid solution into yttrium citrate dihydrate Janusz, W. Skwarek, E. Sternik, D. Pikus, S. Pawlak, D. Parus, J.L. Mikołajczak, R. MethodsX Method Article A method of synthesis crystalline yttrium citrate dihydrate was proposed as a result of the transformation of the freshly precipitated basic yttrium carbonate phase in a citric acid solution. The synthesis time was determined on the basis of composition analysis, structure and thermogravimetric studies of samples taken during the synthesis. The research methods used have shown that in the initial stage of the synthesis, the processes of citric acid sorption on basic yttrium carbonate and transformation of amorphous yttrium carbonate hydroxide into crystalline yttrium hydroxide occurs. It is only after 72 h of synthesis that the crystalline yttrium citrate dihydrate is formed. • Synthesis crystalline yttrium citrate dehydrate. • The synthesis time 72 h. • Synthesis components: the freshly precipitated basic yttrium carbonate phase in a citric acid solution. Elsevier 2020-11-27 /pmc/articles/PMC7725940/ /pubmed/33318957 http://dx.doi.org/10.1016/j.mex.2020.101153 Text en © 2020 The Author(s) http://creativecommons.org/licenses/by/4.0/ This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Method Article Janusz, W. Skwarek, E. Sternik, D. Pikus, S. Pawlak, D. Parus, J.L. Mikołajczak, R. Methods of investigation transformation kinetics of yttrium carbonate hydroxide in citric acid solution into yttrium citrate dihydrate |
title | Methods of investigation transformation kinetics of yttrium carbonate hydroxide in citric acid solution into yttrium citrate dihydrate |
title_full | Methods of investigation transformation kinetics of yttrium carbonate hydroxide in citric acid solution into yttrium citrate dihydrate |
title_fullStr | Methods of investigation transformation kinetics of yttrium carbonate hydroxide in citric acid solution into yttrium citrate dihydrate |
title_full_unstemmed | Methods of investigation transformation kinetics of yttrium carbonate hydroxide in citric acid solution into yttrium citrate dihydrate |
title_short | Methods of investigation transformation kinetics of yttrium carbonate hydroxide in citric acid solution into yttrium citrate dihydrate |
title_sort | methods of investigation transformation kinetics of yttrium carbonate hydroxide in citric acid solution into yttrium citrate dihydrate |
topic | Method Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7725940/ https://www.ncbi.nlm.nih.gov/pubmed/33318957 http://dx.doi.org/10.1016/j.mex.2020.101153 |
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