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Methods of investigation transformation kinetics of yttrium carbonate hydroxide in citric acid solution into yttrium citrate dihydrate

A method of synthesis crystalline yttrium citrate dihydrate was proposed as a result of the transformation of the freshly precipitated basic yttrium carbonate phase in a citric acid solution. The synthesis time was determined on the basis of composition analysis, structure and thermogravimetric stud...

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Detalles Bibliográficos
Autores principales: Janusz, W., Skwarek, E., Sternik, D., Pikus, S., Pawlak, D., Parus, J.L., Mikołajczak, R.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2020
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7725940/
https://www.ncbi.nlm.nih.gov/pubmed/33318957
http://dx.doi.org/10.1016/j.mex.2020.101153
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author Janusz, W.
Skwarek, E.
Sternik, D.
Pikus, S.
Pawlak, D.
Parus, J.L.
Mikołajczak, R.
author_facet Janusz, W.
Skwarek, E.
Sternik, D.
Pikus, S.
Pawlak, D.
Parus, J.L.
Mikołajczak, R.
author_sort Janusz, W.
collection PubMed
description A method of synthesis crystalline yttrium citrate dihydrate was proposed as a result of the transformation of the freshly precipitated basic yttrium carbonate phase in a citric acid solution. The synthesis time was determined on the basis of composition analysis, structure and thermogravimetric studies of samples taken during the synthesis. The research methods used have shown that in the initial stage of the synthesis, the processes of citric acid sorption on basic yttrium carbonate and transformation of amorphous yttrium carbonate hydroxide into crystalline yttrium hydroxide occurs. It is only after 72 h of synthesis that the crystalline yttrium citrate dihydrate is formed. • Synthesis crystalline yttrium citrate dehydrate. • The synthesis time 72 h. • Synthesis components: the freshly precipitated basic yttrium carbonate phase in a citric acid solution.
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spelling pubmed-77259402020-12-13 Methods of investigation transformation kinetics of yttrium carbonate hydroxide in citric acid solution into yttrium citrate dihydrate Janusz, W. Skwarek, E. Sternik, D. Pikus, S. Pawlak, D. Parus, J.L. Mikołajczak, R. MethodsX Method Article A method of synthesis crystalline yttrium citrate dihydrate was proposed as a result of the transformation of the freshly precipitated basic yttrium carbonate phase in a citric acid solution. The synthesis time was determined on the basis of composition analysis, structure and thermogravimetric studies of samples taken during the synthesis. The research methods used have shown that in the initial stage of the synthesis, the processes of citric acid sorption on basic yttrium carbonate and transformation of amorphous yttrium carbonate hydroxide into crystalline yttrium hydroxide occurs. It is only after 72 h of synthesis that the crystalline yttrium citrate dihydrate is formed. • Synthesis crystalline yttrium citrate dehydrate. • The synthesis time 72 h. • Synthesis components: the freshly precipitated basic yttrium carbonate phase in a citric acid solution. Elsevier 2020-11-27 /pmc/articles/PMC7725940/ /pubmed/33318957 http://dx.doi.org/10.1016/j.mex.2020.101153 Text en © 2020 The Author(s) http://creativecommons.org/licenses/by/4.0/ This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Method Article
Janusz, W.
Skwarek, E.
Sternik, D.
Pikus, S.
Pawlak, D.
Parus, J.L.
Mikołajczak, R.
Methods of investigation transformation kinetics of yttrium carbonate hydroxide in citric acid solution into yttrium citrate dihydrate
title Methods of investigation transformation kinetics of yttrium carbonate hydroxide in citric acid solution into yttrium citrate dihydrate
title_full Methods of investigation transformation kinetics of yttrium carbonate hydroxide in citric acid solution into yttrium citrate dihydrate
title_fullStr Methods of investigation transformation kinetics of yttrium carbonate hydroxide in citric acid solution into yttrium citrate dihydrate
title_full_unstemmed Methods of investigation transformation kinetics of yttrium carbonate hydroxide in citric acid solution into yttrium citrate dihydrate
title_short Methods of investigation transformation kinetics of yttrium carbonate hydroxide in citric acid solution into yttrium citrate dihydrate
title_sort methods of investigation transformation kinetics of yttrium carbonate hydroxide in citric acid solution into yttrium citrate dihydrate
topic Method Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7725940/
https://www.ncbi.nlm.nih.gov/pubmed/33318957
http://dx.doi.org/10.1016/j.mex.2020.101153
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