Cargando…

The In-Situ Observation of Grain Rotation and Microstructure Evolution Induced by Electromigration in Sn-3.0Ag-0.5Cu Solder Joints

The in-situ observation of Sn-3.0Ag-0.5Cu solder joints under electromigration was conducted to investigate the microstructure and grain orientation evolution. It was observed that there was a grain rotation phenomenon during current stressing by in-situ electron backscattered diffraction (EBSD). Th...

Descripción completa

Detalles Bibliográficos
Autores principales: Fu, Xing, Liu, Min, Xu, KeXin, Chen, Si, Shi, YiJun, Fu, ZhiWei, Huang, Yun, Chen, HongTao, Yao, RuoHe
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2020
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7730036/
https://www.ncbi.nlm.nih.gov/pubmed/33276575
http://dx.doi.org/10.3390/ma13235497
_version_ 1783621592450859008
author Fu, Xing
Liu, Min
Xu, KeXin
Chen, Si
Shi, YiJun
Fu, ZhiWei
Huang, Yun
Chen, HongTao
Yao, RuoHe
author_facet Fu, Xing
Liu, Min
Xu, KeXin
Chen, Si
Shi, YiJun
Fu, ZhiWei
Huang, Yun
Chen, HongTao
Yao, RuoHe
author_sort Fu, Xing
collection PubMed
description The in-situ observation of Sn-3.0Ag-0.5Cu solder joints under electromigration was conducted to investigate the microstructure and grain orientation evolution. It was observed that there was a grain rotation phenomenon during current stressing by in-situ electron backscattered diffraction (EBSD). The rotation angle was calculated, which indicated that the grain reorientation led to the decrease of the resistance of solder joints. On the other hand, the orientation of β-Sn played a critical role in determining the migration of Cu atoms in solder joints under current stressing migration. When the angle between the electron flow direction and the c-axis of Sn (defined as α) was close to 0°, massive Cu(6)Sn(5) intermetallic compounds were observed in the solder bulk; however, when α was close to 90°, the migration of the intermetallic compound (IMC) was blocked but many Sn hillocks grew in the anode. Moreover, the low angle boundaries were the fast diffusion channel of Cu atoms while the high grain boundaries in the range of 55°–65° were not favorable to the fast diffusion of Cu atoms.
format Online
Article
Text
id pubmed-7730036
institution National Center for Biotechnology Information
language English
publishDate 2020
publisher MDPI
record_format MEDLINE/PubMed
spelling pubmed-77300362020-12-12 The In-Situ Observation of Grain Rotation and Microstructure Evolution Induced by Electromigration in Sn-3.0Ag-0.5Cu Solder Joints Fu, Xing Liu, Min Xu, KeXin Chen, Si Shi, YiJun Fu, ZhiWei Huang, Yun Chen, HongTao Yao, RuoHe Materials (Basel) Article The in-situ observation of Sn-3.0Ag-0.5Cu solder joints under electromigration was conducted to investigate the microstructure and grain orientation evolution. It was observed that there was a grain rotation phenomenon during current stressing by in-situ electron backscattered diffraction (EBSD). The rotation angle was calculated, which indicated that the grain reorientation led to the decrease of the resistance of solder joints. On the other hand, the orientation of β-Sn played a critical role in determining the migration of Cu atoms in solder joints under current stressing migration. When the angle between the electron flow direction and the c-axis of Sn (defined as α) was close to 0°, massive Cu(6)Sn(5) intermetallic compounds were observed in the solder bulk; however, when α was close to 90°, the migration of the intermetallic compound (IMC) was blocked but many Sn hillocks grew in the anode. Moreover, the low angle boundaries were the fast diffusion channel of Cu atoms while the high grain boundaries in the range of 55°–65° were not favorable to the fast diffusion of Cu atoms. MDPI 2020-12-02 /pmc/articles/PMC7730036/ /pubmed/33276575 http://dx.doi.org/10.3390/ma13235497 Text en © 2020 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Fu, Xing
Liu, Min
Xu, KeXin
Chen, Si
Shi, YiJun
Fu, ZhiWei
Huang, Yun
Chen, HongTao
Yao, RuoHe
The In-Situ Observation of Grain Rotation and Microstructure Evolution Induced by Electromigration in Sn-3.0Ag-0.5Cu Solder Joints
title The In-Situ Observation of Grain Rotation and Microstructure Evolution Induced by Electromigration in Sn-3.0Ag-0.5Cu Solder Joints
title_full The In-Situ Observation of Grain Rotation and Microstructure Evolution Induced by Electromigration in Sn-3.0Ag-0.5Cu Solder Joints
title_fullStr The In-Situ Observation of Grain Rotation and Microstructure Evolution Induced by Electromigration in Sn-3.0Ag-0.5Cu Solder Joints
title_full_unstemmed The In-Situ Observation of Grain Rotation and Microstructure Evolution Induced by Electromigration in Sn-3.0Ag-0.5Cu Solder Joints
title_short The In-Situ Observation of Grain Rotation and Microstructure Evolution Induced by Electromigration in Sn-3.0Ag-0.5Cu Solder Joints
title_sort in-situ observation of grain rotation and microstructure evolution induced by electromigration in sn-3.0ag-0.5cu solder joints
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7730036/
https://www.ncbi.nlm.nih.gov/pubmed/33276575
http://dx.doi.org/10.3390/ma13235497
work_keys_str_mv AT fuxing theinsituobservationofgrainrotationandmicrostructureevolutioninducedbyelectromigrationinsn30ag05cusolderjoints
AT liumin theinsituobservationofgrainrotationandmicrostructureevolutioninducedbyelectromigrationinsn30ag05cusolderjoints
AT xukexin theinsituobservationofgrainrotationandmicrostructureevolutioninducedbyelectromigrationinsn30ag05cusolderjoints
AT chensi theinsituobservationofgrainrotationandmicrostructureevolutioninducedbyelectromigrationinsn30ag05cusolderjoints
AT shiyijun theinsituobservationofgrainrotationandmicrostructureevolutioninducedbyelectromigrationinsn30ag05cusolderjoints
AT fuzhiwei theinsituobservationofgrainrotationandmicrostructureevolutioninducedbyelectromigrationinsn30ag05cusolderjoints
AT huangyun theinsituobservationofgrainrotationandmicrostructureevolutioninducedbyelectromigrationinsn30ag05cusolderjoints
AT chenhongtao theinsituobservationofgrainrotationandmicrostructureevolutioninducedbyelectromigrationinsn30ag05cusolderjoints
AT yaoruohe theinsituobservationofgrainrotationandmicrostructureevolutioninducedbyelectromigrationinsn30ag05cusolderjoints
AT fuxing insituobservationofgrainrotationandmicrostructureevolutioninducedbyelectromigrationinsn30ag05cusolderjoints
AT liumin insituobservationofgrainrotationandmicrostructureevolutioninducedbyelectromigrationinsn30ag05cusolderjoints
AT xukexin insituobservationofgrainrotationandmicrostructureevolutioninducedbyelectromigrationinsn30ag05cusolderjoints
AT chensi insituobservationofgrainrotationandmicrostructureevolutioninducedbyelectromigrationinsn30ag05cusolderjoints
AT shiyijun insituobservationofgrainrotationandmicrostructureevolutioninducedbyelectromigrationinsn30ag05cusolderjoints
AT fuzhiwei insituobservationofgrainrotationandmicrostructureevolutioninducedbyelectromigrationinsn30ag05cusolderjoints
AT huangyun insituobservationofgrainrotationandmicrostructureevolutioninducedbyelectromigrationinsn30ag05cusolderjoints
AT chenhongtao insituobservationofgrainrotationandmicrostructureevolutioninducedbyelectromigrationinsn30ag05cusolderjoints
AT yaoruohe insituobservationofgrainrotationandmicrostructureevolutioninducedbyelectromigrationinsn30ag05cusolderjoints