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New Grain Formation by Constitutional Undercooling Due to Remelting of Segregated Microstructures during Powder Bed Fusion

A microstructure has significant influence on the mechanical properties of parts. For isotropic properties, the formation of equiaxed microstructures by the nucleation of new grains during solidification is necessary. For conventional solidification processes, nucleation is well-understood. Regardin...

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Autores principales: Rausch, Alexander M., Gotterbarm, Martin R., Pistor, Julian, Markl, Matthias, Körner, Carolin
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2020
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7731160/
https://www.ncbi.nlm.nih.gov/pubmed/33287217
http://dx.doi.org/10.3390/ma13235517
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author Rausch, Alexander M.
Gotterbarm, Martin R.
Pistor, Julian
Markl, Matthias
Körner, Carolin
author_facet Rausch, Alexander M.
Gotterbarm, Martin R.
Pistor, Julian
Markl, Matthias
Körner, Carolin
author_sort Rausch, Alexander M.
collection PubMed
description A microstructure has significant influence on the mechanical properties of parts. For isotropic properties, the formation of equiaxed microstructures by the nucleation of new grains during solidification is necessary. For conventional solidification processes, nucleation is well-understood. Regarding powder bed fusion, the repeated remelting of previous layers can cause nucleation under some conditions that are not explainable with classical theories. Here, we investigate this nucleation mechanism with an unprecedented level of detail. In the first step, we built samples with single crystalline microstructures from Ni-base superalloy IN718 by selective electron beam melting. In the second step, single lines with different parameters were molten on top of these samples. We observed a huge number of new grains by nucleation at the melt-pool border of these single lines. However, new grains can only prevail if the alignment of their crystallographic orientation with respect to the local temperature gradient is superior to that of the base material. The current hypothesis is that nucleation at the melt-pool border happens due to remelting microsegregations from former solidification processes leading to constitutional undercooling directly at the onset of solidification. This study offers the opportunity to understand and exploit this mechanism for different manufacturing processes.
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spelling pubmed-77311602020-12-12 New Grain Formation by Constitutional Undercooling Due to Remelting of Segregated Microstructures during Powder Bed Fusion Rausch, Alexander M. Gotterbarm, Martin R. Pistor, Julian Markl, Matthias Körner, Carolin Materials (Basel) Article A microstructure has significant influence on the mechanical properties of parts. For isotropic properties, the formation of equiaxed microstructures by the nucleation of new grains during solidification is necessary. For conventional solidification processes, nucleation is well-understood. Regarding powder bed fusion, the repeated remelting of previous layers can cause nucleation under some conditions that are not explainable with classical theories. Here, we investigate this nucleation mechanism with an unprecedented level of detail. In the first step, we built samples with single crystalline microstructures from Ni-base superalloy IN718 by selective electron beam melting. In the second step, single lines with different parameters were molten on top of these samples. We observed a huge number of new grains by nucleation at the melt-pool border of these single lines. However, new grains can only prevail if the alignment of their crystallographic orientation with respect to the local temperature gradient is superior to that of the base material. The current hypothesis is that nucleation at the melt-pool border happens due to remelting microsegregations from former solidification processes leading to constitutional undercooling directly at the onset of solidification. This study offers the opportunity to understand and exploit this mechanism for different manufacturing processes. MDPI 2020-12-03 /pmc/articles/PMC7731160/ /pubmed/33287217 http://dx.doi.org/10.3390/ma13235517 Text en © 2020 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Rausch, Alexander M.
Gotterbarm, Martin R.
Pistor, Julian
Markl, Matthias
Körner, Carolin
New Grain Formation by Constitutional Undercooling Due to Remelting of Segregated Microstructures during Powder Bed Fusion
title New Grain Formation by Constitutional Undercooling Due to Remelting of Segregated Microstructures during Powder Bed Fusion
title_full New Grain Formation by Constitutional Undercooling Due to Remelting of Segregated Microstructures during Powder Bed Fusion
title_fullStr New Grain Formation by Constitutional Undercooling Due to Remelting of Segregated Microstructures during Powder Bed Fusion
title_full_unstemmed New Grain Formation by Constitutional Undercooling Due to Remelting of Segregated Microstructures during Powder Bed Fusion
title_short New Grain Formation by Constitutional Undercooling Due to Remelting of Segregated Microstructures during Powder Bed Fusion
title_sort new grain formation by constitutional undercooling due to remelting of segregated microstructures during powder bed fusion
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7731160/
https://www.ncbi.nlm.nih.gov/pubmed/33287217
http://dx.doi.org/10.3390/ma13235517
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