Research on the effects of hydrothermal synthesis conditions on the crystal habit of MIL-121

The investigation of the influence of hydrothermal synthesis conditions such as synthetic temperature, the amount of solvent, addition of additives including sodium hydroxide, lithium chloride and 2-methylimidazole on the morphology and size of MIL-121 was carried out. The experimental results indic...

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Detalles Bibliográficos
Autores principales: Wang, Fei, Zhu, Liang, Wei, Qingyan, Wang, Yanfei
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The Royal Society 2020
Materias:
Chemistry
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7735355/
https://www.ncbi.nlm.nih.gov/pubmed/33391802
http://dx.doi.org/10.1098/rsos.201212
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author Wang, Fei
Zhu, Liang
Wei, Qingyan
Wang, Yanfei
author_facet Wang, Fei
Zhu, Liang
Wei, Qingyan
Wang, Yanfei
author_sort Wang, Fei
collection PubMed
description The investigation of the influence of hydrothermal synthesis conditions such as synthetic temperature, the amount of solvent, addition of additives including sodium hydroxide, lithium chloride and 2-methylimidazole on the morphology and size of MIL-121 was carried out. The experimental results indicated the significant impact of hydrothermal synthesis conditions on the morphologies and sizes of MIL-121 crystals. The synthesis temperature has little effect on the morphology, which is mainly reflected in the change of the aspect ratio, but the effect on the size is significant under low-temperature conditions. Additives have an important influence on the morphology and size of MIL-121. Our study provides a potential for the improvement of MIL-121 adsorption performance.
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spelling pubmed-77353552020-12-31 Research on the effects of hydrothermal synthesis conditions on the crystal habit of MIL-121 Wang, Fei Zhu, Liang Wei, Qingyan Wang, Yanfei R Soc Open Sci Chemistry The investigation of the influence of hydrothermal synthesis conditions such as synthetic temperature, the amount of solvent, addition of additives including sodium hydroxide, lithium chloride and 2-methylimidazole on the morphology and size of MIL-121 was carried out. The experimental results indicated the significant impact of hydrothermal synthesis conditions on the morphologies and sizes of MIL-121 crystals. The synthesis temperature has little effect on the morphology, which is mainly reflected in the change of the aspect ratio, but the effect on the size is significant under low-temperature conditions. Additives have an important influence on the morphology and size of MIL-121. Our study provides a potential for the improvement of MIL-121 adsorption performance. The Royal Society 2020-11-18 /pmc/articles/PMC7735355/ /pubmed/33391802 http://dx.doi.org/10.1098/rsos.201212 Text en © 2020 The Authors. http://creativecommons.org/licenses/by/4.0/ http://creativecommons.org/licenses/by/4.0/http://creativecommons.org/licenses/by/4.0/Published by the Royal Society under the terms of the Creative Commons Attribution License http://creativecommons.org/licenses/by/4.0/, which permits unrestricted use, provided the original author and source are credited.
spellingShingle Chemistry
Wang, Fei
Zhu, Liang
Wei, Qingyan
Wang, Yanfei
Research on the effects of hydrothermal synthesis conditions on the crystal habit of MIL-121
title Research on the effects of hydrothermal synthesis conditions on the crystal habit of MIL-121
title_full Research on the effects of hydrothermal synthesis conditions on the crystal habit of MIL-121
title_fullStr Research on the effects of hydrothermal synthesis conditions on the crystal habit of MIL-121
title_full_unstemmed Research on the effects of hydrothermal synthesis conditions on the crystal habit of MIL-121
title_short Research on the effects of hydrothermal synthesis conditions on the crystal habit of MIL-121
title_sort research on the effects of hydrothermal synthesis conditions on the crystal habit of mil-121
topic Chemistry
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7735355/
https://www.ncbi.nlm.nih.gov/pubmed/33391802
http://dx.doi.org/10.1098/rsos.201212
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