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Scanning transmission imaging in the helium ion microscope using a microchannel plate with a delay line detector

A detection system based on a microchannel plate with a delay line readout structure has been developed to perform scanning transmission ion microscopy (STIM) in the helium ion microscope (HIM). This system is an improvement over other existing approaches since it combines the information of the sca...

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Autores principales: Serralta, Eduardo, Klingner, Nico, De Castro, Olivier, Mousley, Michael, Eswara, Santhana, Duarte Pinto, Serge, Wirtz, Tom, Hlawacek, Gregor
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Beilstein-Institut 2020
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7736698/
https://www.ncbi.nlm.nih.gov/pubmed/33364144
http://dx.doi.org/10.3762/bjnano.11.167
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author Serralta, Eduardo
Klingner, Nico
De Castro, Olivier
Mousley, Michael
Eswara, Santhana
Duarte Pinto, Serge
Wirtz, Tom
Hlawacek, Gregor
author_facet Serralta, Eduardo
Klingner, Nico
De Castro, Olivier
Mousley, Michael
Eswara, Santhana
Duarte Pinto, Serge
Wirtz, Tom
Hlawacek, Gregor
author_sort Serralta, Eduardo
collection PubMed
description A detection system based on a microchannel plate with a delay line readout structure has been developed to perform scanning transmission ion microscopy (STIM) in the helium ion microscope (HIM). This system is an improvement over other existing approaches since it combines the information of the scanning beam position on the sample with the position (scattering angle) and time of the transmission events. Various imaging modes, such as bright field and dark field or the direct image of the transmitted signal, can be created by post-processing the collected STIM data. Furthermore, the detector has high spatial and temporal resolution, is sensitive to both ions and neutral particles over a wide energy range, and shows robustness against ion beam-induced damage. A special in-vacuum movable support gives the possibility of moving the detector vertically, placing the detector closer to the sample for the detection of high-angle scattering events, or moving it down to increase the angular resolution and distance for time-of-flight measurements. With this new system, we show composition-dependent contrast for amorphous materials and the contrast difference between small-angle and high-angle scattering signals. We also detect channeling-related contrast on polycrystalline silicon, thallium chloride nanocrystals, and single-crystalline silicon by comparing the signal transmitted at different directions for the same data set.
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spelling pubmed-77366982020-12-23 Scanning transmission imaging in the helium ion microscope using a microchannel plate with a delay line detector Serralta, Eduardo Klingner, Nico De Castro, Olivier Mousley, Michael Eswara, Santhana Duarte Pinto, Serge Wirtz, Tom Hlawacek, Gregor Beilstein J Nanotechnol Full Research Paper A detection system based on a microchannel plate with a delay line readout structure has been developed to perform scanning transmission ion microscopy (STIM) in the helium ion microscope (HIM). This system is an improvement over other existing approaches since it combines the information of the scanning beam position on the sample with the position (scattering angle) and time of the transmission events. Various imaging modes, such as bright field and dark field or the direct image of the transmitted signal, can be created by post-processing the collected STIM data. Furthermore, the detector has high spatial and temporal resolution, is sensitive to both ions and neutral particles over a wide energy range, and shows robustness against ion beam-induced damage. A special in-vacuum movable support gives the possibility of moving the detector vertically, placing the detector closer to the sample for the detection of high-angle scattering events, or moving it down to increase the angular resolution and distance for time-of-flight measurements. With this new system, we show composition-dependent contrast for amorphous materials and the contrast difference between small-angle and high-angle scattering signals. We also detect channeling-related contrast on polycrystalline silicon, thallium chloride nanocrystals, and single-crystalline silicon by comparing the signal transmitted at different directions for the same data set. Beilstein-Institut 2020-12-11 /pmc/articles/PMC7736698/ /pubmed/33364144 http://dx.doi.org/10.3762/bjnano.11.167 Text en Copyright © 2020, Serralta et al. https://creativecommons.org/licenses/by/4.0https://www.beilstein-journals.org/bjnano/terms/termsThis is an Open Access article under the terms of the Creative Commons Attribution License (https://creativecommons.org/licenses/by/4.0). Please note that the reuse, redistribution and reproduction in particular requires that the author(s) and source are credited and that individual graphics may be subject to special legal provisions. The license is subject to the Beilstein Journal of Nanotechnology terms and conditions: (https://www.beilstein-journals.org/bjnano/terms/terms)
spellingShingle Full Research Paper
Serralta, Eduardo
Klingner, Nico
De Castro, Olivier
Mousley, Michael
Eswara, Santhana
Duarte Pinto, Serge
Wirtz, Tom
Hlawacek, Gregor
Scanning transmission imaging in the helium ion microscope using a microchannel plate with a delay line detector
title Scanning transmission imaging in the helium ion microscope using a microchannel plate with a delay line detector
title_full Scanning transmission imaging in the helium ion microscope using a microchannel plate with a delay line detector
title_fullStr Scanning transmission imaging in the helium ion microscope using a microchannel plate with a delay line detector
title_full_unstemmed Scanning transmission imaging in the helium ion microscope using a microchannel plate with a delay line detector
title_short Scanning transmission imaging in the helium ion microscope using a microchannel plate with a delay line detector
title_sort scanning transmission imaging in the helium ion microscope using a microchannel plate with a delay line detector
topic Full Research Paper
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7736698/
https://www.ncbi.nlm.nih.gov/pubmed/33364144
http://dx.doi.org/10.3762/bjnano.11.167
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