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Optimisation of Urine Sample Preparation for Headspace-Solid Phase Microextraction Gas Chromatography-Mass Spectrometry: Altering Sample pH, Sulphuric Acid Concentration and Phase Ratio
Headspace-solid phase microextraction gas chromatography-mass spectrometry (HS-SPME-GC-MS) can be used to measure volatile organic compounds (VOCs) in human urine. However, there is no widely adopted standardised protocol for the preparation of urine samples for analysis resulting in an inability to...
Autores principales: | Aggarwal, Prashant, Baker, James, Boyd, Mark T., Coyle, Séamus, Probert, Chris, Chapman, Elinor A. |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2020
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7760603/ https://www.ncbi.nlm.nih.gov/pubmed/33255680 http://dx.doi.org/10.3390/metabo10120482 |
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