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3D-Printed Hermetic Alumina Housings

Ceramics are repeatedly investigated as packaging materials because of their gas tightness, e.g., as hermetic implantable housing. Recent advances also make it possible to print the established aluminum oxide in a Fused Filament Fabrication process, creating new possibilities for manufacturing perso...

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Autores principales: Eickenscheidt, Max, Langenmair, Michael, Dbouk, Ahmad, Nötzel, Dorit, Hanemann, Thomas, Stieglitz, Thomas
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7795362/
https://www.ncbi.nlm.nih.gov/pubmed/33401644
http://dx.doi.org/10.3390/ma14010200
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author Eickenscheidt, Max
Langenmair, Michael
Dbouk, Ahmad
Nötzel, Dorit
Hanemann, Thomas
Stieglitz, Thomas
author_facet Eickenscheidt, Max
Langenmair, Michael
Dbouk, Ahmad
Nötzel, Dorit
Hanemann, Thomas
Stieglitz, Thomas
author_sort Eickenscheidt, Max
collection PubMed
description Ceramics are repeatedly investigated as packaging materials because of their gas tightness, e.g., as hermetic implantable housing. Recent advances also make it possible to print the established aluminum oxide in a Fused Filament Fabrication process, creating new possibilities for manufacturing personalized devices with complex shapes. This study was able to achieve integration of channels with a diameter of 500 µm (pre-sintered) with a nozzle size of 250 µm (layer thickness 100 µm) and even closed hemispheres were printed without support structures. During sintering, the weight-bearing feedstock shrinks by 16.7%, resulting in a relative material density of 96.6%. The well-known challenges of the technology such as surface roughness (Ra = 15–20 µm) and integrated cavities remain. However, it could be shown that the hollow structures in bulk do not represent a mechanical weak point and that the material can be gas-tight (<10(−12) mbar s(−1)). For verification, a volume-free helium leak test device was developed and validated. Finally, platinum coatings with high adhesion examined the functionalization of the ceramic. All the prerequisites for hermetic housings with integrated metal structures are given, with a new level of complexity of ceramic shapes available.
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spelling pubmed-77953622021-01-10 3D-Printed Hermetic Alumina Housings Eickenscheidt, Max Langenmair, Michael Dbouk, Ahmad Nötzel, Dorit Hanemann, Thomas Stieglitz, Thomas Materials (Basel) Article Ceramics are repeatedly investigated as packaging materials because of their gas tightness, e.g., as hermetic implantable housing. Recent advances also make it possible to print the established aluminum oxide in a Fused Filament Fabrication process, creating new possibilities for manufacturing personalized devices with complex shapes. This study was able to achieve integration of channels with a diameter of 500 µm (pre-sintered) with a nozzle size of 250 µm (layer thickness 100 µm) and even closed hemispheres were printed without support structures. During sintering, the weight-bearing feedstock shrinks by 16.7%, resulting in a relative material density of 96.6%. The well-known challenges of the technology such as surface roughness (Ra = 15–20 µm) and integrated cavities remain. However, it could be shown that the hollow structures in bulk do not represent a mechanical weak point and that the material can be gas-tight (<10(−12) mbar s(−1)). For verification, a volume-free helium leak test device was developed and validated. Finally, platinum coatings with high adhesion examined the functionalization of the ceramic. All the prerequisites for hermetic housings with integrated metal structures are given, with a new level of complexity of ceramic shapes available. MDPI 2021-01-03 /pmc/articles/PMC7795362/ /pubmed/33401644 http://dx.doi.org/10.3390/ma14010200 Text en © 2021 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Eickenscheidt, Max
Langenmair, Michael
Dbouk, Ahmad
Nötzel, Dorit
Hanemann, Thomas
Stieglitz, Thomas
3D-Printed Hermetic Alumina Housings
title 3D-Printed Hermetic Alumina Housings
title_full 3D-Printed Hermetic Alumina Housings
title_fullStr 3D-Printed Hermetic Alumina Housings
title_full_unstemmed 3D-Printed Hermetic Alumina Housings
title_short 3D-Printed Hermetic Alumina Housings
title_sort 3d-printed hermetic alumina housings
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7795362/
https://www.ncbi.nlm.nih.gov/pubmed/33401644
http://dx.doi.org/10.3390/ma14010200
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