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Low-Cost Benzene Toluene Xylene Measurement Gas System Based on the Mini Chromatographic Cartridge

Benzene, toluene and xylene (BTX) are an important part of the volatile organic compounds (VOCs) to be detected and monitored in the air, due to their toxicity towards human health. One of the most reliable technique used in BTX detection is gas chromatography (GC), which presents a high sensitivity...

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Autores principales: Zampetti, Emiliano, Papa, Paolo, Avossa, Joshua, Bearzotti, Andrea, Balducci, Catia, Tranfo, Giovanna, Macagnano, Antonella
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2020
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7796067/
https://www.ncbi.nlm.nih.gov/pubmed/33379142
http://dx.doi.org/10.3390/s21010125
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author Zampetti, Emiliano
Papa, Paolo
Avossa, Joshua
Bearzotti, Andrea
Balducci, Catia
Tranfo, Giovanna
Macagnano, Antonella
author_facet Zampetti, Emiliano
Papa, Paolo
Avossa, Joshua
Bearzotti, Andrea
Balducci, Catia
Tranfo, Giovanna
Macagnano, Antonella
author_sort Zampetti, Emiliano
collection PubMed
description Benzene, toluene and xylene (BTX) are an important part of the volatile organic compounds (VOCs) to be detected and monitored in the air, due to their toxicity towards human health. One of the most reliable technique used in BTX detection is gas chromatography (GC), which presents a high sensitivity. On the other hand, it has important drawbacks, such as high costs, the need for qualified personnel and frequent maintenance. To overcome these drawbacks, this work reports the development of a low cost and portable BTX gas detection system based on a mini chromatographic cartridge, a photo ionization detector (PID), a simple control unit (based on Arduino architecture) and a mini pump. In order to separate the BTX components, we propose the use of a cartridge 80 mm in length, composed of several commercial chromatographic column sections. To test the system performances, we have injected different amounts (from about 0.3 to 5.3 µg) of benzene, toluene and xylene and two of the most frequent possible interferents (ethanol, acetone). Experimental results have shown different retention time values (i.e., 25 ± 0.5 s, 51 ± 1.2 s and 117 ± 4 s, respectively) for benzene, toluene and xylene.
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spelling pubmed-77960672021-01-10 Low-Cost Benzene Toluene Xylene Measurement Gas System Based on the Mini Chromatographic Cartridge Zampetti, Emiliano Papa, Paolo Avossa, Joshua Bearzotti, Andrea Balducci, Catia Tranfo, Giovanna Macagnano, Antonella Sensors (Basel) Letter Benzene, toluene and xylene (BTX) are an important part of the volatile organic compounds (VOCs) to be detected and monitored in the air, due to their toxicity towards human health. One of the most reliable technique used in BTX detection is gas chromatography (GC), which presents a high sensitivity. On the other hand, it has important drawbacks, such as high costs, the need for qualified personnel and frequent maintenance. To overcome these drawbacks, this work reports the development of a low cost and portable BTX gas detection system based on a mini chromatographic cartridge, a photo ionization detector (PID), a simple control unit (based on Arduino architecture) and a mini pump. In order to separate the BTX components, we propose the use of a cartridge 80 mm in length, composed of several commercial chromatographic column sections. To test the system performances, we have injected different amounts (from about 0.3 to 5.3 µg) of benzene, toluene and xylene and two of the most frequent possible interferents (ethanol, acetone). Experimental results have shown different retention time values (i.e., 25 ± 0.5 s, 51 ± 1.2 s and 117 ± 4 s, respectively) for benzene, toluene and xylene. MDPI 2020-12-28 /pmc/articles/PMC7796067/ /pubmed/33379142 http://dx.doi.org/10.3390/s21010125 Text en © 2020 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Letter
Zampetti, Emiliano
Papa, Paolo
Avossa, Joshua
Bearzotti, Andrea
Balducci, Catia
Tranfo, Giovanna
Macagnano, Antonella
Low-Cost Benzene Toluene Xylene Measurement Gas System Based on the Mini Chromatographic Cartridge
title Low-Cost Benzene Toluene Xylene Measurement Gas System Based on the Mini Chromatographic Cartridge
title_full Low-Cost Benzene Toluene Xylene Measurement Gas System Based on the Mini Chromatographic Cartridge
title_fullStr Low-Cost Benzene Toluene Xylene Measurement Gas System Based on the Mini Chromatographic Cartridge
title_full_unstemmed Low-Cost Benzene Toluene Xylene Measurement Gas System Based on the Mini Chromatographic Cartridge
title_short Low-Cost Benzene Toluene Xylene Measurement Gas System Based on the Mini Chromatographic Cartridge
title_sort low-cost benzene toluene xylene measurement gas system based on the mini chromatographic cartridge
topic Letter
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7796067/
https://www.ncbi.nlm.nih.gov/pubmed/33379142
http://dx.doi.org/10.3390/s21010125
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