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Efficient Removal of Methylene Blue from Aqueous Solutions Using a High Specific Surface Area Porous Carbon Derived from Soybean Dreg

Porous carbon material with high specific surface area was prepared from soybean dreg by a simple and effective two-step method (high temperature pyrolysis and activation). The structural characteristics of the synthesized carbon were evaluated by Brunauer–Emmett–Teller (BET), N(2) adsorption/desorp...

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Autores principales: Ying, Zhiwei, Huang, Lu, Ji, Lili, Li, He, Liu, Xinqi, Zhang, Chi, Zhang, Jian, Yi, Guofu
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8038204/
https://www.ncbi.nlm.nih.gov/pubmed/33918336
http://dx.doi.org/10.3390/ma14071754
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author Ying, Zhiwei
Huang, Lu
Ji, Lili
Li, He
Liu, Xinqi
Zhang, Chi
Zhang, Jian
Yi, Guofu
author_facet Ying, Zhiwei
Huang, Lu
Ji, Lili
Li, He
Liu, Xinqi
Zhang, Chi
Zhang, Jian
Yi, Guofu
author_sort Ying, Zhiwei
collection PubMed
description Porous carbon material with high specific surface area was prepared from soybean dreg by a simple and effective two-step method (high temperature pyrolysis and activation). The structural characteristics of the synthesized carbon were evaluated by Brunauer–Emmett–Teller (BET), N(2) adsorption/desorption measurements/techniques, an elemental analyzer (EA), scanning electron microscopy equipped with energy dispersive X-ray spectroscopy (SEM-EDS), transmission electron microscopy (TEM), an X-ray diffractometer (XRD), Raman spectroscopy (Raman), a Fourier transform infrared spectrometer (FTIR), and X-ray photoelectron spectroscopy (XPS). The specific surface area of SDB-6-K was 2786 m(2) g(−1), the pore volume was 2.316 cm(3) g(−1), and the average pore size was 3.326 nm. The high specific surface area and effective functional groups of carbon material promoted the adsorption of methylene blue. The maximum adsorption capacity of SDB-6-K to methylene blue was 2636 mg g(−1) at 318 K. The adsorption kinetic and isotherm data were most suitable for pseudo-second-order and Langmuir equations. The results showed that the adsorbent had excellent adsorptive ability and had good practical application potential in the field of dye wastewater treatment in the future.
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spelling pubmed-80382042021-04-12 Efficient Removal of Methylene Blue from Aqueous Solutions Using a High Specific Surface Area Porous Carbon Derived from Soybean Dreg Ying, Zhiwei Huang, Lu Ji, Lili Li, He Liu, Xinqi Zhang, Chi Zhang, Jian Yi, Guofu Materials (Basel) Article Porous carbon material with high specific surface area was prepared from soybean dreg by a simple and effective two-step method (high temperature pyrolysis and activation). The structural characteristics of the synthesized carbon were evaluated by Brunauer–Emmett–Teller (BET), N(2) adsorption/desorption measurements/techniques, an elemental analyzer (EA), scanning electron microscopy equipped with energy dispersive X-ray spectroscopy (SEM-EDS), transmission electron microscopy (TEM), an X-ray diffractometer (XRD), Raman spectroscopy (Raman), a Fourier transform infrared spectrometer (FTIR), and X-ray photoelectron spectroscopy (XPS). The specific surface area of SDB-6-K was 2786 m(2) g(−1), the pore volume was 2.316 cm(3) g(−1), and the average pore size was 3.326 nm. The high specific surface area and effective functional groups of carbon material promoted the adsorption of methylene blue. The maximum adsorption capacity of SDB-6-K to methylene blue was 2636 mg g(−1) at 318 K. The adsorption kinetic and isotherm data were most suitable for pseudo-second-order and Langmuir equations. The results showed that the adsorbent had excellent adsorptive ability and had good practical application potential in the field of dye wastewater treatment in the future. MDPI 2021-04-02 /pmc/articles/PMC8038204/ /pubmed/33918336 http://dx.doi.org/10.3390/ma14071754 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Ying, Zhiwei
Huang, Lu
Ji, Lili
Li, He
Liu, Xinqi
Zhang, Chi
Zhang, Jian
Yi, Guofu
Efficient Removal of Methylene Blue from Aqueous Solutions Using a High Specific Surface Area Porous Carbon Derived from Soybean Dreg
title Efficient Removal of Methylene Blue from Aqueous Solutions Using a High Specific Surface Area Porous Carbon Derived from Soybean Dreg
title_full Efficient Removal of Methylene Blue from Aqueous Solutions Using a High Specific Surface Area Porous Carbon Derived from Soybean Dreg
title_fullStr Efficient Removal of Methylene Blue from Aqueous Solutions Using a High Specific Surface Area Porous Carbon Derived from Soybean Dreg
title_full_unstemmed Efficient Removal of Methylene Blue from Aqueous Solutions Using a High Specific Surface Area Porous Carbon Derived from Soybean Dreg
title_short Efficient Removal of Methylene Blue from Aqueous Solutions Using a High Specific Surface Area Porous Carbon Derived from Soybean Dreg
title_sort efficient removal of methylene blue from aqueous solutions using a high specific surface area porous carbon derived from soybean dreg
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8038204/
https://www.ncbi.nlm.nih.gov/pubmed/33918336
http://dx.doi.org/10.3390/ma14071754
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