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Threefold helical assembly via hydroxy hydrogen bonds: the 2:1 co-crystal of bicyclo[3.3.0]octane-endo-3,endo-7-diol and bicyclo[3.3.0]octane-endo-3,exo-7-diol
Reduction of bicyclo[3.3.0]octane-3,7-dione yields a mixture of the endo-3,endo-7-diol and endo-3, exo-7-diol (C(8)H(14)O(2)) isomers (5 and 6). These form (5)(2)·(6) co-crystals in the monoclinic P2(1)/n space group (with Z = 6, Z′ = 1.5) rather than undergoing separation by means of fractional r...
| Autores principales: | , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2021
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8061109/ https://www.ncbi.nlm.nih.gov/pubmed/33953950 http://dx.doi.org/10.1107/S2056989021001730 |