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The Hard X-ray Nanoprobe beamline at Diamond Light Source
The Hard X-ray Nanoprobe beamline, I14, at Diamond Light Source is a new facility for nanoscale microscopy. The beamline was designed with an emphasis on multi-modal analysis, providing elemental mapping, speciation mapping by XANES, structural phase mapping using nano-XRD and imaging through differ...
Autores principales: | , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2021
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8127369/ https://www.ncbi.nlm.nih.gov/pubmed/33950009 http://dx.doi.org/10.1107/S1600577521002502 |
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author | Quinn, Paul D. Alianelli, Lucia Gomez-Gonzalez, Miguel Mahoney, David Cacho-Nerin, Fernando Peach, Andrew Parker, Julia E. |
author_facet | Quinn, Paul D. Alianelli, Lucia Gomez-Gonzalez, Miguel Mahoney, David Cacho-Nerin, Fernando Peach, Andrew Parker, Julia E. |
author_sort | Quinn, Paul D. |
collection | PubMed |
description | The Hard X-ray Nanoprobe beamline, I14, at Diamond Light Source is a new facility for nanoscale microscopy. The beamline was designed with an emphasis on multi-modal analysis, providing elemental mapping, speciation mapping by XANES, structural phase mapping using nano-XRD and imaging through differential phase contrast and ptychography. The 185 m-long beamline operates over a 5 keV to 23 keV energy range providing a ≤50 nm beam size for routine user experiments and a flexible scanning system allowing fast acquisition. The beamline achieves robust and stable operation by imaging the source in the vertical direction and implementing horizontally deflecting primary optics and an overfilled secondary source in the horizontal direction. This paper describes the design considerations, optical layout, aspects of the hardware engineering and scanning system in operation as well as some examples illustrating the beamline performance. |
format | Online Article Text |
id | pubmed-8127369 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2021 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-81273692021-06-14 The Hard X-ray Nanoprobe beamline at Diamond Light Source Quinn, Paul D. Alianelli, Lucia Gomez-Gonzalez, Miguel Mahoney, David Cacho-Nerin, Fernando Peach, Andrew Parker, Julia E. J Synchrotron Radiat Beamlines The Hard X-ray Nanoprobe beamline, I14, at Diamond Light Source is a new facility for nanoscale microscopy. The beamline was designed with an emphasis on multi-modal analysis, providing elemental mapping, speciation mapping by XANES, structural phase mapping using nano-XRD and imaging through differential phase contrast and ptychography. The 185 m-long beamline operates over a 5 keV to 23 keV energy range providing a ≤50 nm beam size for routine user experiments and a flexible scanning system allowing fast acquisition. The beamline achieves robust and stable operation by imaging the source in the vertical direction and implementing horizontally deflecting primary optics and an overfilled secondary source in the horizontal direction. This paper describes the design considerations, optical layout, aspects of the hardware engineering and scanning system in operation as well as some examples illustrating the beamline performance. International Union of Crystallography 2021-04-09 /pmc/articles/PMC8127369/ /pubmed/33950009 http://dx.doi.org/10.1107/S1600577521002502 Text en © Quinn et al. 2021 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Beamlines Quinn, Paul D. Alianelli, Lucia Gomez-Gonzalez, Miguel Mahoney, David Cacho-Nerin, Fernando Peach, Andrew Parker, Julia E. The Hard X-ray Nanoprobe beamline at Diamond Light Source |
title | The Hard X-ray Nanoprobe beamline at Diamond Light Source |
title_full | The Hard X-ray Nanoprobe beamline at Diamond Light Source |
title_fullStr | The Hard X-ray Nanoprobe beamline at Diamond Light Source |
title_full_unstemmed | The Hard X-ray Nanoprobe beamline at Diamond Light Source |
title_short | The Hard X-ray Nanoprobe beamline at Diamond Light Source |
title_sort | hard x-ray nanoprobe beamline at diamond light source |
topic | Beamlines |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8127369/ https://www.ncbi.nlm.nih.gov/pubmed/33950009 http://dx.doi.org/10.1107/S1600577521002502 |
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