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The Hard X-ray Nanoprobe beamline at Diamond Light Source

The Hard X-ray Nanoprobe beamline, I14, at Diamond Light Source is a new facility for nanoscale microscopy. The beamline was designed with an emphasis on multi-modal analysis, providing elemental mapping, speciation mapping by XANES, structural phase mapping using nano-XRD and imaging through differ...

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Autores principales: Quinn, Paul D., Alianelli, Lucia, Gomez-Gonzalez, Miguel, Mahoney, David, Cacho-Nerin, Fernando, Peach, Andrew, Parker, Julia E.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8127369/
https://www.ncbi.nlm.nih.gov/pubmed/33950009
http://dx.doi.org/10.1107/S1600577521002502
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author Quinn, Paul D.
Alianelli, Lucia
Gomez-Gonzalez, Miguel
Mahoney, David
Cacho-Nerin, Fernando
Peach, Andrew
Parker, Julia E.
author_facet Quinn, Paul D.
Alianelli, Lucia
Gomez-Gonzalez, Miguel
Mahoney, David
Cacho-Nerin, Fernando
Peach, Andrew
Parker, Julia E.
author_sort Quinn, Paul D.
collection PubMed
description The Hard X-ray Nanoprobe beamline, I14, at Diamond Light Source is a new facility for nanoscale microscopy. The beamline was designed with an emphasis on multi-modal analysis, providing elemental mapping, speciation mapping by XANES, structural phase mapping using nano-XRD and imaging through differential phase contrast and ptychography. The 185 m-long beamline operates over a 5 keV to 23 keV energy range providing a ≤50 nm beam size for routine user experiments and a flexible scanning system allowing fast acquisition. The beamline achieves robust and stable operation by imaging the source in the vertical direction and implementing horizontally deflecting primary optics and an overfilled secondary source in the horizontal direction. This paper describes the design considerations, optical layout, aspects of the hardware engineering and scanning system in operation as well as some examples illustrating the beamline performance.
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spelling pubmed-81273692021-06-14 The Hard X-ray Nanoprobe beamline at Diamond Light Source Quinn, Paul D. Alianelli, Lucia Gomez-Gonzalez, Miguel Mahoney, David Cacho-Nerin, Fernando Peach, Andrew Parker, Julia E. J Synchrotron Radiat Beamlines The Hard X-ray Nanoprobe beamline, I14, at Diamond Light Source is a new facility for nanoscale microscopy. The beamline was designed with an emphasis on multi-modal analysis, providing elemental mapping, speciation mapping by XANES, structural phase mapping using nano-XRD and imaging through differential phase contrast and ptychography. The 185 m-long beamline operates over a 5 keV to 23 keV energy range providing a ≤50 nm beam size for routine user experiments and a flexible scanning system allowing fast acquisition. The beamline achieves robust and stable operation by imaging the source in the vertical direction and implementing horizontally deflecting primary optics and an overfilled secondary source in the horizontal direction. This paper describes the design considerations, optical layout, aspects of the hardware engineering and scanning system in operation as well as some examples illustrating the beamline performance. International Union of Crystallography 2021-04-09 /pmc/articles/PMC8127369/ /pubmed/33950009 http://dx.doi.org/10.1107/S1600577521002502 Text en © Quinn et al. 2021 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Beamlines
Quinn, Paul D.
Alianelli, Lucia
Gomez-Gonzalez, Miguel
Mahoney, David
Cacho-Nerin, Fernando
Peach, Andrew
Parker, Julia E.
The Hard X-ray Nanoprobe beamline at Diamond Light Source
title The Hard X-ray Nanoprobe beamline at Diamond Light Source
title_full The Hard X-ray Nanoprobe beamline at Diamond Light Source
title_fullStr The Hard X-ray Nanoprobe beamline at Diamond Light Source
title_full_unstemmed The Hard X-ray Nanoprobe beamline at Diamond Light Source
title_short The Hard X-ray Nanoprobe beamline at Diamond Light Source
title_sort hard x-ray nanoprobe beamline at diamond light source
topic Beamlines
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8127369/
https://www.ncbi.nlm.nih.gov/pubmed/33950009
http://dx.doi.org/10.1107/S1600577521002502
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