Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)

The high-precision X-ray diffraction setup for work with diamond anvil cells (DACs) in interaction chamber 2 (IC2) of the High Energy Density instrument of the European X-ray Free-Electron Laser is described. This includes beamline optics, sample positioning and detector systems located in the multi...

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Autores principales: Liermann, H. P., Konôpková, Z., Appel, K., Prescher, C., Schropp, A., Cerantola, V., Husband, R. J., McHardy, J. D., McMahon, M. I., McWilliams, R. S., Pépin, C. M., Mainberger, J., Roeper, M., Berghäuser, A., Damker, H., Talkovski, P., Foese, M., Kujala, N., Ball, O. B., Baron, M. A., Briggs, R., Bykov, M., Bykova, E., Chantel, J., Coleman, A. L., Cynn, H., Dattelbaum, D., Dresselhaus-Marais, L. E., Eggert, J. H., Ehm, L., Evans, W. J., Fiquet, G., Frost, M., Glazyrin, K., Goncharov, A. F., Hwang, H., Jenei, Zs., Kim, J.-Y., Langenhorst, F., Lee, Y., Makita, M., Marquardt, H., McBride, E. E., Merkel, S., Morard, G., O’Bannon, E. F., Otzen, C., Pace, E. J., Pelka, A., Pigott, J. S., Prakapenka, V. B., Redmer, R., Sanchez-Valle, C., Schoelmerich, M., Speziale, S., Spiekermann, G., Sturtevant, B. T., Toleikis, S., Velisavljevic, N., Wilke, M., Yoo, C.-S., Baehtz, C., Zastrau, U., Strohm, C.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2021
Materias:
Research Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8127375/
https://www.ncbi.nlm.nih.gov/pubmed/33949979
http://dx.doi.org/10.1107/S1600577521002551
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author Liermann, H. P.
Konôpková, Z.
Appel, K.
Prescher, C.
Schropp, A.
Cerantola, V.
Husband, R. J.
McHardy, J. D.
McMahon, M. I.
McWilliams, R. S.
Pépin, C. M.
Mainberger, J.
Roeper, M.
Berghäuser, A.
Damker, H.
Talkovski, P.
Foese, M.
Kujala, N.
Ball, O. B.
Baron, M. A.
Briggs, R.
Bykov, M.
Bykova, E.
Chantel, J.
Coleman, A. L.
Cynn, H.
Dattelbaum, D.
Dresselhaus-Marais, L. E.
Eggert, J. H.
Ehm, L.
Evans, W. J.
Fiquet, G.
Frost, M.
Glazyrin, K.
Goncharov, A. F.
Hwang, H.
Jenei, Zs.
Kim, J.-Y.
Langenhorst, F.
Lee, Y.
Makita, M.
Marquardt, H.
McBride, E. E.
Merkel, S.
Morard, G.
O’Bannon, E. F.
Otzen, C.
Pace, E. J.
Pelka, A.
Pigott, J. S.
Prakapenka, V. B.
Redmer, R.
Sanchez-Valle, C.
Schoelmerich, M.
Speziale, S.
Spiekermann, G.
Sturtevant, B. T.
Toleikis, S.
Velisavljevic, N.
Wilke, M.
Yoo, C.-S.
Baehtz, C.
Zastrau, U.
Strohm, C.
author_facet Liermann, H. P.
Konôpková, Z.
Appel, K.
Prescher, C.
Schropp, A.
Cerantola, V.
Husband, R. J.
McHardy, J. D.
McMahon, M. I.
McWilliams, R. S.
Pépin, C. M.
Mainberger, J.
Roeper, M.
Berghäuser, A.
Damker, H.
Talkovski, P.
Foese, M.
Kujala, N.
Ball, O. B.
Baron, M. A.
Briggs, R.
Bykov, M.
Bykova, E.
Chantel, J.
Coleman, A. L.
Cynn, H.
Dattelbaum, D.
Dresselhaus-Marais, L. E.
Eggert, J. H.
Ehm, L.
Evans, W. J.
Fiquet, G.
Frost, M.
Glazyrin, K.
Goncharov, A. F.
Hwang, H.
Jenei, Zs.
Kim, J.-Y.
Langenhorst, F.
Lee, Y.
Makita, M.
Marquardt, H.
McBride, E. E.
Merkel, S.
Morard, G.
O’Bannon, E. F.
Otzen, C.
Pace, E. J.
Pelka, A.
Pigott, J. S.
Prakapenka, V. B.
Redmer, R.
Sanchez-Valle, C.
Schoelmerich, M.
Speziale, S.
Spiekermann, G.
Sturtevant, B. T.
Toleikis, S.
Velisavljevic, N.
Wilke, M.
Yoo, C.-S.
Baehtz, C.
Zastrau, U.
Strohm, C.
author_sort Liermann, H. P.
collection PubMed
description The high-precision X-ray diffraction setup for work with diamond anvil cells (DACs) in interaction chamber 2 (IC2) of the High Energy Density instrument of the European X-ray Free-Electron Laser is described. This includes beamline optics, sample positioning and detector systems located in the multipurpose vacuum chamber. Concepts for pump–probe X-ray diffraction experiments in the DAC are described and their implementation demonstrated during the First User Community Assisted Commissioning experiment. X-ray heating and diffraction of Bi under pressure, obtained using 20 fs X-ray pulses at 17.8 keV and 2.2 MHz repetition, is illustrated through splitting of diffraction peaks, and interpreted employing finite element modeling of the sample chamber in the DAC.
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spelling pubmed-81273752021-06-14 Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL) Liermann, H. P. Konôpková, Z. Appel, K. Prescher, C. Schropp, A. Cerantola, V. Husband, R. J. McHardy, J. D. McMahon, M. I. McWilliams, R. S. Pépin, C. M. Mainberger, J. Roeper, M. Berghäuser, A. Damker, H. Talkovski, P. Foese, M. Kujala, N. Ball, O. B. Baron, M. A. Briggs, R. Bykov, M. Bykova, E. Chantel, J. Coleman, A. L. Cynn, H. Dattelbaum, D. Dresselhaus-Marais, L. E. Eggert, J. H. Ehm, L. Evans, W. J. Fiquet, G. Frost, M. Glazyrin, K. Goncharov, A. F. Hwang, H. Jenei, Zs. Kim, J.-Y. Langenhorst, F. Lee, Y. Makita, M. Marquardt, H. McBride, E. E. Merkel, S. Morard, G. O’Bannon, E. F. Otzen, C. Pace, E. J. Pelka, A. Pigott, J. S. Prakapenka, V. B. Redmer, R. Sanchez-Valle, C. Schoelmerich, M. Speziale, S. Spiekermann, G. Sturtevant, B. T. Toleikis, S. Velisavljevic, N. Wilke, M. Yoo, C.-S. Baehtz, C. Zastrau, U. Strohm, C. J Synchrotron Radiat Research Papers The high-precision X-ray diffraction setup for work with diamond anvil cells (DACs) in interaction chamber 2 (IC2) of the High Energy Density instrument of the European X-ray Free-Electron Laser is described. This includes beamline optics, sample positioning and detector systems located in the multipurpose vacuum chamber. Concepts for pump–probe X-ray diffraction experiments in the DAC are described and their implementation demonstrated during the First User Community Assisted Commissioning experiment. X-ray heating and diffraction of Bi under pressure, obtained using 20 fs X-ray pulses at 17.8 keV and 2.2 MHz repetition, is illustrated through splitting of diffraction peaks, and interpreted employing finite element modeling of the sample chamber in the DAC. International Union of Crystallography 2021-04-14 /pmc/articles/PMC8127375/ /pubmed/33949979 http://dx.doi.org/10.1107/S1600577521002551 Text en © H. P. Liermann et al. 2021 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Papers
Liermann, H. P.
Konôpková, Z.
Appel, K.
Prescher, C.
Schropp, A.
Cerantola, V.
Husband, R. J.
McHardy, J. D.
McMahon, M. I.
McWilliams, R. S.
Pépin, C. M.
Mainberger, J.
Roeper, M.
Berghäuser, A.
Damker, H.
Talkovski, P.
Foese, M.
Kujala, N.
Ball, O. B.
Baron, M. A.
Briggs, R.
Bykov, M.
Bykova, E.
Chantel, J.
Coleman, A. L.
Cynn, H.
Dattelbaum, D.
Dresselhaus-Marais, L. E.
Eggert, J. H.
Ehm, L.
Evans, W. J.
Fiquet, G.
Frost, M.
Glazyrin, K.
Goncharov, A. F.
Hwang, H.
Jenei, Zs.
Kim, J.-Y.
Langenhorst, F.
Lee, Y.
Makita, M.
Marquardt, H.
McBride, E. E.
Merkel, S.
Morard, G.
O’Bannon, E. F.
Otzen, C.
Pace, E. J.
Pelka, A.
Pigott, J. S.
Prakapenka, V. B.
Redmer, R.
Sanchez-Valle, C.
Schoelmerich, M.
Speziale, S.
Spiekermann, G.
Sturtevant, B. T.
Toleikis, S.
Velisavljevic, N.
Wilke, M.
Yoo, C.-S.
Baehtz, C.
Zastrau, U.
Strohm, C.
Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)
title Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)
title_full Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)
title_fullStr Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)
title_full_unstemmed Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)
title_short Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)
title_sort novel experimental setup for megahertz x-ray diffraction in a diamond anvil cell at the high energy density (hed) instrument of the european x-ray free-electron laser (euxfel)
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8127375/
https://www.ncbi.nlm.nih.gov/pubmed/33949979
http://dx.doi.org/10.1107/S1600577521002551
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