A novel method for in situ TEM measurements of adhesion at the diamond–metal interface

The procedure for in situ TEM measurements of bonding strength (adhesion) between diamond and the metal matrix using a Hysitron PI 95 TEM Picoindenter holder for mechanical tests and Push-to-Pull devices was proposed. For tensile tests, dog-bone shaped lamellae 280–330 nm thick and ~ 2.5 µm long wer...

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Autores principales: Loginov, P. A., Sidorenko, D. A., Orekhov, A. S., Levashov, E. A.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2021
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8139953/
https://www.ncbi.nlm.nih.gov/pubmed/34021180
http://dx.doi.org/10.1038/s41598-021-89536-2
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author Loginov, P. A.
Sidorenko, D. A.
Orekhov, A. S.
Levashov, E. A.
author_facet Loginov, P. A.
Sidorenko, D. A.
Orekhov, A. S.
Levashov, E. A.
author_sort Loginov, P. A.
collection PubMed
description The procedure for in situ TEM measurements of bonding strength (adhesion) between diamond and the metal matrix using a Hysitron PI 95 TEM Picoindenter holder for mechanical tests and Push-to-Pull devices was proposed. For tensile tests, dog-bone shaped lamellae 280–330 nm thick and ~ 2.5 µm long were used as objects of study. The lamellae were manufactured using the focused ion beam technology from the metal–diamond interface of diamond-containing composite material with a single-phase binder made of Fe–Co–Ni alloy. The experimentally determined bonding strength was 110 MPa.
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spelling pubmed-81399532021-05-25 A novel method for in situ TEM measurements of adhesion at the diamond–metal interface Loginov, P. A. Sidorenko, D. A. Orekhov, A. S. Levashov, E. A. Sci Rep Article The procedure for in situ TEM measurements of bonding strength (adhesion) between diamond and the metal matrix using a Hysitron PI 95 TEM Picoindenter holder for mechanical tests and Push-to-Pull devices was proposed. For tensile tests, dog-bone shaped lamellae 280–330 nm thick and ~ 2.5 µm long were used as objects of study. The lamellae were manufactured using the focused ion beam technology from the metal–diamond interface of diamond-containing composite material with a single-phase binder made of Fe–Co–Ni alloy. The experimentally determined bonding strength was 110 MPa. Nature Publishing Group UK 2021-05-21 /pmc/articles/PMC8139953/ /pubmed/34021180 http://dx.doi.org/10.1038/s41598-021-89536-2 Text en © The Author(s) 2021 https://creativecommons.org/licenses/by/4.0/Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) .
spellingShingle Article
Loginov, P. A.
Sidorenko, D. A.
Orekhov, A. S.
Levashov, E. A.
A novel method for in situ TEM measurements of adhesion at the diamond–metal interface
title A novel method for in situ TEM measurements of adhesion at the diamond–metal interface
title_full A novel method for in situ TEM measurements of adhesion at the diamond–metal interface
title_fullStr A novel method for in situ TEM measurements of adhesion at the diamond–metal interface
title_full_unstemmed A novel method for in situ TEM measurements of adhesion at the diamond–metal interface
title_short A novel method for in situ TEM measurements of adhesion at the diamond–metal interface
title_sort novel method for in situ tem measurements of adhesion at the diamond–metal interface
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8139953/
https://www.ncbi.nlm.nih.gov/pubmed/34021180
http://dx.doi.org/10.1038/s41598-021-89536-2
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