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Triphenylphosphine Oxide Removal from Reactions: The Role of Solvent and Temperature
[Image: see text] Here, a large-scale feasible, chromatography-free process to purge triphenylphosphine oxide (TPPO) from the crude product of Mitsunobu and Wittig reactions has been developed. Divergence in physicochemical properties like polarity and solubility of TPPO against the product was util...
| Autores principales: | , , , , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
American Chemical Society
2021
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| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8173612/ https://www.ncbi.nlm.nih.gov/pubmed/34095685 http://dx.doi.org/10.1021/acsomega.1c01996 |