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FEBID 3D-Nanoprinting at Low Substrate Temperatures: Pushing the Speed While Keeping the Quality

High-fidelity 3D printing of nanoscale objects is an increasing relevant but challenging task. Among the few fabrication techniques, focused electron beam induced deposition (FEBID) has demonstrated its high potential due to its direct-write character, nanoscale capabilities in 3D space and a very h...

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Autores principales: Hinum-Wagner, Jakob, Kuhness, David, Kothleitner, Gerald, Winkler, Robert, Plank, Harald
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8229455/
https://www.ncbi.nlm.nih.gov/pubmed/34207654
http://dx.doi.org/10.3390/nano11061527
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author Hinum-Wagner, Jakob
Kuhness, David
Kothleitner, Gerald
Winkler, Robert
Plank, Harald
author_facet Hinum-Wagner, Jakob
Kuhness, David
Kothleitner, Gerald
Winkler, Robert
Plank, Harald
author_sort Hinum-Wagner, Jakob
collection PubMed
description High-fidelity 3D printing of nanoscale objects is an increasing relevant but challenging task. Among the few fabrication techniques, focused electron beam induced deposition (FEBID) has demonstrated its high potential due to its direct-write character, nanoscale capabilities in 3D space and a very high design flexibility. A limitation, however, is the low fabrication speed, which often restricts 3D-FEBID for the fabrication of single objects. In this study, we approach that challenge by reducing the substrate temperatures with a homemade Peltier stage and investigate the effects on Pt based 3D deposits in a temperature range of [Formula: see text] The findings reveal a volume growth rate boost up to a factor of [Formula: see text] , while the shape fidelity in 3D space is maintained. From a materials point of view, the internal nanogranular composition is practically unaffected down to [Formula: see text] , followed by a slight grain size increase for even lower temperatures. The study is complemented by a comprehensive discussion about the growth mechanism for a more general picture. The combined findings demonstrate that FEBID on low substrate temperatures is not only much faster, but practically free of drawbacks during high fidelity 3D nanofabrication.
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spelling pubmed-82294552021-06-26 FEBID 3D-Nanoprinting at Low Substrate Temperatures: Pushing the Speed While Keeping the Quality Hinum-Wagner, Jakob Kuhness, David Kothleitner, Gerald Winkler, Robert Plank, Harald Nanomaterials (Basel) Article High-fidelity 3D printing of nanoscale objects is an increasing relevant but challenging task. Among the few fabrication techniques, focused electron beam induced deposition (FEBID) has demonstrated its high potential due to its direct-write character, nanoscale capabilities in 3D space and a very high design flexibility. A limitation, however, is the low fabrication speed, which often restricts 3D-FEBID for the fabrication of single objects. In this study, we approach that challenge by reducing the substrate temperatures with a homemade Peltier stage and investigate the effects on Pt based 3D deposits in a temperature range of [Formula: see text] The findings reveal a volume growth rate boost up to a factor of [Formula: see text] , while the shape fidelity in 3D space is maintained. From a materials point of view, the internal nanogranular composition is practically unaffected down to [Formula: see text] , followed by a slight grain size increase for even lower temperatures. The study is complemented by a comprehensive discussion about the growth mechanism for a more general picture. The combined findings demonstrate that FEBID on low substrate temperatures is not only much faster, but practically free of drawbacks during high fidelity 3D nanofabrication. MDPI 2021-06-09 /pmc/articles/PMC8229455/ /pubmed/34207654 http://dx.doi.org/10.3390/nano11061527 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Hinum-Wagner, Jakob
Kuhness, David
Kothleitner, Gerald
Winkler, Robert
Plank, Harald
FEBID 3D-Nanoprinting at Low Substrate Temperatures: Pushing the Speed While Keeping the Quality
title FEBID 3D-Nanoprinting at Low Substrate Temperatures: Pushing the Speed While Keeping the Quality
title_full FEBID 3D-Nanoprinting at Low Substrate Temperatures: Pushing the Speed While Keeping the Quality
title_fullStr FEBID 3D-Nanoprinting at Low Substrate Temperatures: Pushing the Speed While Keeping the Quality
title_full_unstemmed FEBID 3D-Nanoprinting at Low Substrate Temperatures: Pushing the Speed While Keeping the Quality
title_short FEBID 3D-Nanoprinting at Low Substrate Temperatures: Pushing the Speed While Keeping the Quality
title_sort febid 3d-nanoprinting at low substrate temperatures: pushing the speed while keeping the quality
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8229455/
https://www.ncbi.nlm.nih.gov/pubmed/34207654
http://dx.doi.org/10.3390/nano11061527
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