Cargando…

One‐Pot Synthesis of (11)C‐Labelled Primary Benzamides via Intermediate [(11)C]Aroyl Dimethylaminopyridinium Salts

Electrophilic (11)C‐labelled aroyl dimethylaminopyridinium salts, obtained by carbonylative cross‐coupling of aryl halides with [(11)C]carbon monoxide, were prepared for the first time and shown to be valuable intermediates in the synthesis of primary [(11)C]benzamides. The methodology furnished a s...

Descripción completa

Detalles Bibliográficos
Autores principales:	Ferrat, Mélodie, Dahl, Kenneth, Schou, Magnus
Formato:	Online Artículo Texto
Lenguaje:	English
Publicado:	John Wiley and Sons Inc. 2021
Materias:	Communications
Acceso en línea:	https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8251633/ https://www.ncbi.nlm.nih.gov/pubmed/33885193 http://dx.doi.org/10.1002/chem.202100544

Ejemplares similares

A flexible approach to Pd-catalyzed carbonylations via aroyl dimethylaminopyridinium salts
por: Quesnel, Jeffrey S., et al.
Publicado: (2016)

“In‐loop” carbonylation—A simplified method for carbon‐11 labelling of drugs and radioligands
por: Ferrat, Mélodie, et al.
Publicado: (2020)

Development of a fully automated low‐pressure [(11)C]CO carbonylation apparatus
por: Ferrat, Mélodie, et al.
Publicado: (2020)

Acyl Amidines by Pd-Catalyzed Aminocarbonylation: One-Pot Cyclizations and (11)C Labeling
por: Rydfjord, Jonas, et al.
Publicado: (2022)

New methodologies for the preparation of carbon-11 labeled radiopharmaceuticals
por: Dahl, Kenneth, et al.
Publicado: (2017)

Reactive Palladium–Ligand Complexes for (11)C-Carbonylation at Ambient Pressure: A Breakthrough in Carbon-11 Chemistry
por: Dahl, Kenneth, et al.
Publicado: (2023)

Automated One-pot Radiosynthesis of [(11)C]S-adenosyl Methionine
por: Zoppolo, Florencia, et al.
Publicado: (2017)

Palladium-Mediated Synthesis of [Carbonyl-(11)C]acyl Amidines from Aryl Iodides and Aryl Bromides and Their One-Pot Cyclization to (11)C-Labeled Oxadiazoles
por: Rydfjord, Jonas, et al.
Publicado: (2022)

Rapid one-pot radiosynthesis of [carbonyl-(11)C]formamides from primary amines and [(11)C]CO(2)
por: Luzi, Federico, et al.
Publicado: (2020)

From [(11)C]CO(2) to [(11)C]amides: a rapid one-pot synthesis via the Mitsunobu reaction
por: Bongarzone, S., et al.
Publicado: (2017)

Investigation of the Selectivity of the Palladium-Catalyzed Aroylation and Arylation of Stannyl Glycals with Aroyl Chlorides
por: Shinozuka, Tsuyoshi
Publicado: (2021)

One‐Pot C−H Functionalization of Arenes by Diaryliodonium Salts
por: Reitti, Marcus, et al.
Publicado: (2016)

N-[11-(4-Chlorophenyl)-11,12-dihydrobenzo[c]phenanthridin-6-yl]benzamide
por: Zhang, Min, et al.
Publicado: (2010)

Visible Light-Mediated Direct C–H Aroylation and Alkylation of Heteroarenes
por: Chang, Rui, et al.
Publicado: (2019)

Single molecule aggregation-induced dual and white-light emissive etherified aroyl-S,N-ketene acetals via one-pot synthesis
por: Biesen, Lukas, et al.
Publicado: (2023)

Alkynylated and triazole-linked aroyl-S,N-ketene acetals: one-pot synthesis of solid-state emissive dyes with aggregation-induced enhanced emission characteristics
por: Biesen, Lukas, et al.
Publicado: (2023)

Recoverable Phospha-Michael Additions Catalyzed by a 4-N,N-Dimethylaminopyridinium Saccharinate Salt or a Fluorous Long-Chained Pyridine: Two Types of Reusable Base Catalysts
por: Tessema, Eskedar, et al.
Publicado: (2021)

Aroyl Fluorides as Bifunctional Reagents for Dearomatizing Fluoroaroylation of Benzofurans
por: Yu, Xiaoye, et al.
Publicado: (2022)

A novel (11)C-labeled thymidine analog, [(11)C]AZT, for tumor imaging by positron emission tomography
por: Tahara, Tsuyoshi, et al.
Publicado: (2015)

Low background and high contrast PET imaging of amyloid-β with [(11)C]AZD2995 and [(11)C]AZD2184 in Alzheimer’s disease patients
por: Forsberg, Anton, et al.
Publicado: (2013)

Recent progress in [(11)C]carbon dioxide ([(11)C]CO(2)) and [(11)C]carbon monoxide ([(11)C]CO) chemistry
por: Taddei, Carlotta, et al.
Publicado: (2018)

Synthesis of (11)C‐labeled ubiquinone and ubiquinol via Pd(0)‐mediated rapid C‐[(11)C]methylation using [(11)C]methyl iodide and 39‐demethyl‐39‐(pinacolboryl)ubiquinone
por: Goto, Miki, et al.
Publicado: (2019)

PL-11-an intermediate level language for the PDP-11
por: Jennings, G J
Publicado: (1975)

PL-11: an intermediate level language for the PDP-11
por: Jennings, G J
Publicado: (1975)

Improving the stability of (11)C–labeled L-methionine with ascorbate
por: Woods, Michael, et al.
Publicado: (2017)

A new concept for the production of (11)C-labelled radiotracers
por: Wenz, Jan, et al.
Publicado: (2022)

Base-Promoted One-Pot Synthesis of Pyridine Derivatives via Aromatic Alkyne Annulation Using Benzamides as Nitrogen Source
por: Mehmood, Hina, et al.
Publicado: (2021)

NI-11 PATHOLOGICAL ASSESSMENT IN THE IMPACT OF ONE-SHOT BEVACIZUMAB ON UPTAKE OF (11)C-METHIONINE
por: Beppu, Takaaki, et al.
Publicado: (2019)

Synthesis of (11)C‐labeled Sulfonyl Carbamates through a Multicomponent Reaction Employing Sulfonyl Azides, Alcohols, and [(11)C]CO
por: Stevens, Marc Y., et al.
Publicado: (2016)

Synthesis and evaluation of 2-chloro N-[(S)-{(S)-1-[(11) C]methylpiperidin-2-yl} (phenyl)methyl]3-trifluoromethyl-benzamide ([(11) C]N-methyl-SSR504734) as a PET radioligand for glycine transporter 1
por: Fuchigami, Takeshi, et al.
Publicado: (2012)

N-(4,4′-Dibromo-[1,1′-biphenyl]-2-yl)benzamide
por: Novina, J. Josephine, et al.
Publicado: (2013)

One-Pot Synthesis and Applications of N-Heteroaryl Iodonium Salts
por: Bielawski, Marcin, et al.
Publicado: (2014)

One-Pot Difunctionalization of Aryldiazonium Salts for Synthesis of para-Azophenols
por: Liu, Zhenhua, et al.
Publicado: (2022)

Biodistribution and radiation dosimetry of (11)C-labelled docetaxel in cancer patients
por: van der Veldt, Astrid A. M., et al.
Publicado: (2010)

Copper(I)-Mediated (11)C-Carboxylation of (Hetero)arylstannanes
por: Duffy, Ian R., et al.
Publicado: (2020)

OR02-5 Novel Intermediates Are Catalysed By 11βHSD And CYP17A1 In The C11-oxy Backdoor Pathway Leading To The Production Of 11-ketodihydrotestosterone
por: Swart, Amanda, et al.
Publicado: (2019)

Reactions of an Isolable Dialkylsilylene with Aroyl Chlorides. A New Route to Aroylsilanes
por: Xiao, Xu-Qiong, et al.
Publicado: (2016)

Rapid ‘on-column’ preparation of hydrogen [(11)C]cyanide from [(11)C]methyl iodide via [(11)C]formaldehyde
por: Kikuchi, Tatsuya, et al.
Publicado: (2022)

Exploring C++ 11
por: Lischner, Ray
Publicado: (2014)

Direct Incorporation of [(11)C]CO(2) into Asymmetric [(11)C]Carbonates
por: Haji Dheere, Abdul Karim, et al.
Publicado: (2018)

Cannot write session to /tmp/vufind_sessions/sess_fan8ni88kpmmcq6gbif20m9ucv