NORD: NO Relaxation Delay NMR Spectroscopy

The novel concept of NORD (NO relaxation delay) NMR spectroscopy is introduced. The idea is to design concatenated experiments in a way that the magnetization used in the first relaxes toward equilibrium during the second and vice versa, thus saving instrument time. Applications include complete wel...

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Detalles Bibliográficos
Autores principales: Nagy, Tamás Milán, Kövér, Katalin E., Sørensen, Ole W.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: John Wiley and Sons Inc. 2021
Materias:
Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8252012/
https://www.ncbi.nlm.nih.gov/pubmed/33783935
http://dx.doi.org/10.1002/anie.202102487
Descripción
Sumario:The novel concept of NORD (NO relaxation delay) NMR spectroscopy is introduced. The idea is to design concatenated experiments in a way that the magnetization used in the first relaxes toward equilibrium during the second and vice versa, thus saving instrument time. Applications include complete well‐resolved (1)H‐(1)H and (1)H‐(13)C one‐bond and long‐range correlation maps of an 80 mM solution of a trisaccharide recorded in less than two minutes and hydrocortisone with extensive spectral overlap.

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