NORD: NO Relaxation Delay NMR Spectroscopy

The novel concept of NORD (NO relaxation delay) NMR spectroscopy is introduced. The idea is to design concatenated experiments in a way that the magnetization used in the first relaxes toward equilibrium during the second and vice versa, thus saving instrument time. Applications include complete wel...

Descripción completa

Detalles Bibliográficos
Autores principales: Nagy, Tamás Milán, Kövér, Katalin E., Sørensen, Ole W.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: John Wiley and Sons Inc. 2021
Materias:
Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8252012/
https://www.ncbi.nlm.nih.gov/pubmed/33783935
http://dx.doi.org/10.1002/anie.202102487
_version_ 1783717212410871808
author Nagy, Tamás Milán
Kövér, Katalin E.
Sørensen, Ole W.
author_facet Nagy, Tamás Milán
Kövér, Katalin E.
Sørensen, Ole W.
author_sort Nagy, Tamás Milán
collection PubMed
description The novel concept of NORD (NO relaxation delay) NMR spectroscopy is introduced. The idea is to design concatenated experiments in a way that the magnetization used in the first relaxes toward equilibrium during the second and vice versa, thus saving instrument time. Applications include complete well‐resolved (1)H‐(1)H and (1)H‐(13)C one‐bond and long‐range correlation maps of an 80 mM solution of a trisaccharide recorded in less than two minutes and hydrocortisone with extensive spectral overlap.
format Online
Article
Text
id pubmed-8252012
institution National Center for Biotechnology Information
language English
publishDate 2021
publisher John Wiley and Sons Inc.
record_format MEDLINE/PubMed
spelling pubmed-82520122021-07-07 NORD: NO Relaxation Delay NMR Spectroscopy Nagy, Tamás Milán Kövér, Katalin E. Sørensen, Ole W. Angew Chem Int Ed Engl Communications The novel concept of NORD (NO relaxation delay) NMR spectroscopy is introduced. The idea is to design concatenated experiments in a way that the magnetization used in the first relaxes toward equilibrium during the second and vice versa, thus saving instrument time. Applications include complete well‐resolved (1)H‐(1)H and (1)H‐(13)C one‐bond and long‐range correlation maps of an 80 mM solution of a trisaccharide recorded in less than two minutes and hydrocortisone with extensive spectral overlap. John Wiley and Sons Inc. 2021-05-07 2021-06-07 /pmc/articles/PMC8252012/ /pubmed/33783935 http://dx.doi.org/10.1002/anie.202102487 Text en © 2021 The Authors. Angewandte Chemie International Edition published by Wiley-VCH GmbH https://creativecommons.org/licenses/by/4.0/This is an open access article under the terms of the http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited.
spellingShingle Communications
Nagy, Tamás Milán
Kövér, Katalin E.
Sørensen, Ole W.
NORD: NO Relaxation Delay NMR Spectroscopy
title NORD: NO Relaxation Delay NMR Spectroscopy
title_full NORD: NO Relaxation Delay NMR Spectroscopy
title_fullStr NORD: NO Relaxation Delay NMR Spectroscopy
title_full_unstemmed NORD: NO Relaxation Delay NMR Spectroscopy
title_short NORD: NO Relaxation Delay NMR Spectroscopy
title_sort nord: no relaxation delay nmr spectroscopy
topic Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8252012/
https://www.ncbi.nlm.nih.gov/pubmed/33783935
http://dx.doi.org/10.1002/anie.202102487
work_keys_str_mv AT nagytamasmilan nordnorelaxationdelaynmrspectroscopy
AT koverkataline nordnorelaxationdelaynmrspectroscopy
AT sørensenolew nordnorelaxationdelaynmrspectroscopy

Ejemplares similares