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Ni/Al-Hybrid Cellular Foams: An Interface Study by Combination of 3D-Phase Morphology Imaging, Microbeam Fracture Mechanics and In Situ Synchrotron Stress Analysis
Nickel(Ni)/aluminium(Al) hybrid foams are Al base foams coated with Ni by electrodeposition. Hybrid foams offer an enhanced energy absorption capacity. To ensure a good adhering Ni coating, necessary for a shear resistant interface, the influence of a chemical pre-treatment of the base foam was inve...
Autores principales: | , , , , , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2021
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8269473/ https://www.ncbi.nlm.nih.gov/pubmed/34206514 http://dx.doi.org/10.3390/ma14133473 |
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author | Luksch, Jutta Jung, Anne Pauly, Christoph Derr, Ralf Gruenewald, Patrick Laub, Marc Klaus, Manuela Genzel, Christoph Motz, Christian Mücklich, Frank Schaefer, Florian |
author_facet | Luksch, Jutta Jung, Anne Pauly, Christoph Derr, Ralf Gruenewald, Patrick Laub, Marc Klaus, Manuela Genzel, Christoph Motz, Christian Mücklich, Frank Schaefer, Florian |
author_sort | Luksch, Jutta |
collection | PubMed |
description | Nickel(Ni)/aluminium(Al) hybrid foams are Al base foams coated with Ni by electrodeposition. Hybrid foams offer an enhanced energy absorption capacity. To ensure a good adhering Ni coating, necessary for a shear resistant interface, the influence of a chemical pre-treatment of the base foam was investigated by a combination of an interface morphology analysis by focused ion beam (FIB) tomography and in situ mechanical testing. The critical energy for interfacial decohesion from these microbending fracture tests in the scanning electron microscope (SEM) were contrasted to and the results validated by depth-resolved measurements of the evolving stresses in the Ni coating during three-point bending tests at the energy-dispersive diffraction (EDDI) beamline at the synchrotron BESSY II. Such a multi-method assessment of the interface decohesion resistance with respect to the interface morphology provides a reliable investigation strategy for further improvement of the interface morphology. |
format | Online Article Text |
id | pubmed-8269473 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2021 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-82694732021-07-10 Ni/Al-Hybrid Cellular Foams: An Interface Study by Combination of 3D-Phase Morphology Imaging, Microbeam Fracture Mechanics and In Situ Synchrotron Stress Analysis Luksch, Jutta Jung, Anne Pauly, Christoph Derr, Ralf Gruenewald, Patrick Laub, Marc Klaus, Manuela Genzel, Christoph Motz, Christian Mücklich, Frank Schaefer, Florian Materials (Basel) Article Nickel(Ni)/aluminium(Al) hybrid foams are Al base foams coated with Ni by electrodeposition. Hybrid foams offer an enhanced energy absorption capacity. To ensure a good adhering Ni coating, necessary for a shear resistant interface, the influence of a chemical pre-treatment of the base foam was investigated by a combination of an interface morphology analysis by focused ion beam (FIB) tomography and in situ mechanical testing. The critical energy for interfacial decohesion from these microbending fracture tests in the scanning electron microscope (SEM) were contrasted to and the results validated by depth-resolved measurements of the evolving stresses in the Ni coating during three-point bending tests at the energy-dispersive diffraction (EDDI) beamline at the synchrotron BESSY II. Such a multi-method assessment of the interface decohesion resistance with respect to the interface morphology provides a reliable investigation strategy for further improvement of the interface morphology. MDPI 2021-06-22 /pmc/articles/PMC8269473/ /pubmed/34206514 http://dx.doi.org/10.3390/ma14133473 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Luksch, Jutta Jung, Anne Pauly, Christoph Derr, Ralf Gruenewald, Patrick Laub, Marc Klaus, Manuela Genzel, Christoph Motz, Christian Mücklich, Frank Schaefer, Florian Ni/Al-Hybrid Cellular Foams: An Interface Study by Combination of 3D-Phase Morphology Imaging, Microbeam Fracture Mechanics and In Situ Synchrotron Stress Analysis |
title | Ni/Al-Hybrid Cellular Foams: An Interface Study by Combination of 3D-Phase Morphology Imaging, Microbeam Fracture Mechanics and In Situ Synchrotron Stress Analysis |
title_full | Ni/Al-Hybrid Cellular Foams: An Interface Study by Combination of 3D-Phase Morphology Imaging, Microbeam Fracture Mechanics and In Situ Synchrotron Stress Analysis |
title_fullStr | Ni/Al-Hybrid Cellular Foams: An Interface Study by Combination of 3D-Phase Morphology Imaging, Microbeam Fracture Mechanics and In Situ Synchrotron Stress Analysis |
title_full_unstemmed | Ni/Al-Hybrid Cellular Foams: An Interface Study by Combination of 3D-Phase Morphology Imaging, Microbeam Fracture Mechanics and In Situ Synchrotron Stress Analysis |
title_short | Ni/Al-Hybrid Cellular Foams: An Interface Study by Combination of 3D-Phase Morphology Imaging, Microbeam Fracture Mechanics and In Situ Synchrotron Stress Analysis |
title_sort | ni/al-hybrid cellular foams: an interface study by combination of 3d-phase morphology imaging, microbeam fracture mechanics and in situ synchrotron stress analysis |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8269473/ https://www.ncbi.nlm.nih.gov/pubmed/34206514 http://dx.doi.org/10.3390/ma14133473 |
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