Cargando…

Opuntia spp. Fibre Characterisation to Obtain Sustainable Materials in the Composites Field

Some studies have evaluated the use of Opuntia as reinforcement for polymeric matrices, obtaining good results in energy absorption tests and increasing the tensile elastic modulus. However, no studies focusing on the previous characterisation of the fibres and their treatment to improve compatibili...

Descripción completa

Detalles Bibliográficos
Autores principales: Castellano, Jessica, Marrero, María D., Ortega, Zaida, Romero, Francisco, Benitez, Antonio N., Ventura, Myriam R.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8271437/
https://www.ncbi.nlm.nih.gov/pubmed/34202785
http://dx.doi.org/10.3390/polym13132085
_version_ 1783721002021158912
author Castellano, Jessica
Marrero, María D.
Ortega, Zaida
Romero, Francisco
Benitez, Antonio N.
Ventura, Myriam R.
author_facet Castellano, Jessica
Marrero, María D.
Ortega, Zaida
Romero, Francisco
Benitez, Antonio N.
Ventura, Myriam R.
author_sort Castellano, Jessica
collection PubMed
description Some studies have evaluated the use of Opuntia as reinforcement for polymeric matrices, obtaining good results in energy absorption tests and increasing the tensile elastic modulus. However, no studies focusing on the previous characterisation of the fibres and their treatment to improve compatibility with polymeric matrices have been found. This work analyses the chemical composition of Opuntia maxima (OM) and Opuntia dillenii (OD) cladodes and fibre, studying how different treatments influence it. AOAC 2000 methods were used to determine non-structural components and the Van Soest method was used to estimate structural components. Surface characteristics of the samples were also evaluated by Fourier Transform Infrared Spectroscopy (FTIR). Opuntia fibre presented higher cellulose (50–66%) and lignin (6–14%) content and lower hemicellulose (8–13%) content than Opuntia cladodes (9–14% cellulose, 20–50% hemicellulose, 1–4% lignin). Despite the variability of lignocellulosic materials, OD cladodes treated with water and acetic acid achieved an increase in the structural components. Alkaline fibre treatment removed pectin and hemicellulose from the fibre surface, slightly increasing the cellulose content. Future research should evaluate whether the treated Opuntia fibre can improve the mechanical properties of reinforced polymer.
format Online
Article
Text
id pubmed-8271437
institution National Center for Biotechnology Information
language English
publishDate 2021
publisher MDPI
record_format MEDLINE/PubMed
spelling pubmed-82714372021-07-11 Opuntia spp. Fibre Characterisation to Obtain Sustainable Materials in the Composites Field Castellano, Jessica Marrero, María D. Ortega, Zaida Romero, Francisco Benitez, Antonio N. Ventura, Myriam R. Polymers (Basel) Article Some studies have evaluated the use of Opuntia as reinforcement for polymeric matrices, obtaining good results in energy absorption tests and increasing the tensile elastic modulus. However, no studies focusing on the previous characterisation of the fibres and their treatment to improve compatibility with polymeric matrices have been found. This work analyses the chemical composition of Opuntia maxima (OM) and Opuntia dillenii (OD) cladodes and fibre, studying how different treatments influence it. AOAC 2000 methods were used to determine non-structural components and the Van Soest method was used to estimate structural components. Surface characteristics of the samples were also evaluated by Fourier Transform Infrared Spectroscopy (FTIR). Opuntia fibre presented higher cellulose (50–66%) and lignin (6–14%) content and lower hemicellulose (8–13%) content than Opuntia cladodes (9–14% cellulose, 20–50% hemicellulose, 1–4% lignin). Despite the variability of lignocellulosic materials, OD cladodes treated with water and acetic acid achieved an increase in the structural components. Alkaline fibre treatment removed pectin and hemicellulose from the fibre surface, slightly increasing the cellulose content. Future research should evaluate whether the treated Opuntia fibre can improve the mechanical properties of reinforced polymer. MDPI 2021-06-24 /pmc/articles/PMC8271437/ /pubmed/34202785 http://dx.doi.org/10.3390/polym13132085 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Castellano, Jessica
Marrero, María D.
Ortega, Zaida
Romero, Francisco
Benitez, Antonio N.
Ventura, Myriam R.
Opuntia spp. Fibre Characterisation to Obtain Sustainable Materials in the Composites Field
title Opuntia spp. Fibre Characterisation to Obtain Sustainable Materials in the Composites Field
title_full Opuntia spp. Fibre Characterisation to Obtain Sustainable Materials in the Composites Field
title_fullStr Opuntia spp. Fibre Characterisation to Obtain Sustainable Materials in the Composites Field
title_full_unstemmed Opuntia spp. Fibre Characterisation to Obtain Sustainable Materials in the Composites Field
title_short Opuntia spp. Fibre Characterisation to Obtain Sustainable Materials in the Composites Field
title_sort opuntia spp. fibre characterisation to obtain sustainable materials in the composites field
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8271437/
https://www.ncbi.nlm.nih.gov/pubmed/34202785
http://dx.doi.org/10.3390/polym13132085
work_keys_str_mv AT castellanojessica opuntiasppfibrecharacterisationtoobtainsustainablematerialsinthecompositesfield
AT marreromariad opuntiasppfibrecharacterisationtoobtainsustainablematerialsinthecompositesfield
AT ortegazaida opuntiasppfibrecharacterisationtoobtainsustainablematerialsinthecompositesfield
AT romerofrancisco opuntiasppfibrecharacterisationtoobtainsustainablematerialsinthecompositesfield
AT benitezantonion opuntiasppfibrecharacterisationtoobtainsustainablematerialsinthecompositesfield
AT venturamyriamr opuntiasppfibrecharacterisationtoobtainsustainablematerialsinthecompositesfield