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Efficient Adsorption of Deoxynivalenol by Porous Carbon Prepared from Soybean Dreg

A novel porous carbon adsorbent for the removal of deoxynivalenol was prepared from soybean dreg (SD). The new material was characterized by scanning electron microscopy equipped with energy dispersive X-ray spectroscopy (SEM-EDS), transmission electron microscopy (TEM), Brunauer–Emmett–Teller (BET)...

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Autores principales: Ying, Zhiwei, Zhao, Di, Li, He, Liu, Xinqi, Zhang, Jian
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8310275/
https://www.ncbi.nlm.nih.gov/pubmed/34357972
http://dx.doi.org/10.3390/toxins13070500
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author Ying, Zhiwei
Zhao, Di
Li, He
Liu, Xinqi
Zhang, Jian
author_facet Ying, Zhiwei
Zhao, Di
Li, He
Liu, Xinqi
Zhang, Jian
author_sort Ying, Zhiwei
collection PubMed
description A novel porous carbon adsorbent for the removal of deoxynivalenol was prepared from soybean dreg (SD). The new material was characterized by scanning electron microscopy equipped with energy dispersive X-ray spectroscopy (SEM-EDS), transmission electron microscopy (TEM), Brunauer–Emmett–Teller (BET) analysis, N(2) adsorption/desorption measurement techniques, X-ray diffraction (XRD), Raman spectroscopy, Fourier transform infrared (FTIR) spectroscopy and X-ray photoelectron spectroscopy (XPS). The specific surface area of the SDB-6-KOH was found to be 3655.95 m(2) g(−1), the pore volume was 1.936 cm(3) g(−1) and the average pore size was 2.125 nm. The high specific surface area and effective functional groups of the carbon material promoted the adsorption of deoxynivalenol. By comparing the adsorption effect of SDB-6-X prepared with different activators (X: KOH, K(2)CO(3), KHCO(3)), SDB-6-KOH had the highest adsorption capacity. The maximum adsorption capacity of SDB-6-KOH to deoxynivalenol was 52.9877 µg mg(−1), and the removal efficiency reached 88.31% at 318 K. The adsorption kinetic and isotherm data were suitable for pseudo-second-order and Langmuir equations, and the results of this study show that the novel carbon material has excellent adsorptive ability and, thus, offers effective practical application potential for the removal of deoxynivalenol.
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spelling pubmed-83102752021-07-25 Efficient Adsorption of Deoxynivalenol by Porous Carbon Prepared from Soybean Dreg Ying, Zhiwei Zhao, Di Li, He Liu, Xinqi Zhang, Jian Toxins (Basel) Article A novel porous carbon adsorbent for the removal of deoxynivalenol was prepared from soybean dreg (SD). The new material was characterized by scanning electron microscopy equipped with energy dispersive X-ray spectroscopy (SEM-EDS), transmission electron microscopy (TEM), Brunauer–Emmett–Teller (BET) analysis, N(2) adsorption/desorption measurement techniques, X-ray diffraction (XRD), Raman spectroscopy, Fourier transform infrared (FTIR) spectroscopy and X-ray photoelectron spectroscopy (XPS). The specific surface area of the SDB-6-KOH was found to be 3655.95 m(2) g(−1), the pore volume was 1.936 cm(3) g(−1) and the average pore size was 2.125 nm. The high specific surface area and effective functional groups of the carbon material promoted the adsorption of deoxynivalenol. By comparing the adsorption effect of SDB-6-X prepared with different activators (X: KOH, K(2)CO(3), KHCO(3)), SDB-6-KOH had the highest adsorption capacity. The maximum adsorption capacity of SDB-6-KOH to deoxynivalenol was 52.9877 µg mg(−1), and the removal efficiency reached 88.31% at 318 K. The adsorption kinetic and isotherm data were suitable for pseudo-second-order and Langmuir equations, and the results of this study show that the novel carbon material has excellent adsorptive ability and, thus, offers effective practical application potential for the removal of deoxynivalenol. MDPI 2021-07-18 /pmc/articles/PMC8310275/ /pubmed/34357972 http://dx.doi.org/10.3390/toxins13070500 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Ying, Zhiwei
Zhao, Di
Li, He
Liu, Xinqi
Zhang, Jian
Efficient Adsorption of Deoxynivalenol by Porous Carbon Prepared from Soybean Dreg
title Efficient Adsorption of Deoxynivalenol by Porous Carbon Prepared from Soybean Dreg
title_full Efficient Adsorption of Deoxynivalenol by Porous Carbon Prepared from Soybean Dreg
title_fullStr Efficient Adsorption of Deoxynivalenol by Porous Carbon Prepared from Soybean Dreg
title_full_unstemmed Efficient Adsorption of Deoxynivalenol by Porous Carbon Prepared from Soybean Dreg
title_short Efficient Adsorption of Deoxynivalenol by Porous Carbon Prepared from Soybean Dreg
title_sort efficient adsorption of deoxynivalenol by porous carbon prepared from soybean dreg
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8310275/
https://www.ncbi.nlm.nih.gov/pubmed/34357972
http://dx.doi.org/10.3390/toxins13070500
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