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Preparation of W-C-Co Composite Micropowder with Spherical Shaped Particles Using Plasma Technologies

The possibility of obtaining composite micropowders of the W-C-Co system with a spherical particle shape having a submicron/nanoscale internal structure was experimentally confirmed. In the course of work carried out, W-C-Co system nanopowders with the average particle size of approximately 50 nm we...

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Autores principales: Samokhin, Andrey, Alekseev, Nikolay, Astashov, Aleksey, Dorofeev, Aleksey, Fadeev, Andrey, Sinayskiy, Mikhail, Kalashnikov, Yulian
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8348052/
https://www.ncbi.nlm.nih.gov/pubmed/34361452
http://dx.doi.org/10.3390/ma14154258
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author Samokhin, Andrey
Alekseev, Nikolay
Astashov, Aleksey
Dorofeev, Aleksey
Fadeev, Andrey
Sinayskiy, Mikhail
Kalashnikov, Yulian
author_facet Samokhin, Andrey
Alekseev, Nikolay
Astashov, Aleksey
Dorofeev, Aleksey
Fadeev, Andrey
Sinayskiy, Mikhail
Kalashnikov, Yulian
author_sort Samokhin, Andrey
collection PubMed
description The possibility of obtaining composite micropowders of the W-C-Co system with a spherical particle shape having a submicron/nanoscale internal structure was experimentally confirmed. In the course of work carried out, W-C-Co system nanopowders with the average particle size of approximately 50 nm were produced by plasma-chemical synthesis. This method resulted in the uniform distribution of W, Co and C among the nanoparticles of the powder in the nanometer scale range. Dense microgranules with an average size of 40 microns were obtained from the nanopowders by spray drying. The spherical micropowders with an average particle size of 20 microns were received as a result of plasma treatment of 25.36 microns microgranule fraction. The spherical particles obtained in the experiments had a predominantly dense microstructure and had no internal cavities. The influence of plasma treatment process parameters on dispersity, phase, and chemical composition of spherical micropowders and powder particles microstructure has been established.
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spelling pubmed-83480522021-08-08 Preparation of W-C-Co Composite Micropowder with Spherical Shaped Particles Using Plasma Technologies Samokhin, Andrey Alekseev, Nikolay Astashov, Aleksey Dorofeev, Aleksey Fadeev, Andrey Sinayskiy, Mikhail Kalashnikov, Yulian Materials (Basel) Article The possibility of obtaining composite micropowders of the W-C-Co system with a spherical particle shape having a submicron/nanoscale internal structure was experimentally confirmed. In the course of work carried out, W-C-Co system nanopowders with the average particle size of approximately 50 nm were produced by plasma-chemical synthesis. This method resulted in the uniform distribution of W, Co and C among the nanoparticles of the powder in the nanometer scale range. Dense microgranules with an average size of 40 microns were obtained from the nanopowders by spray drying. The spherical micropowders with an average particle size of 20 microns were received as a result of plasma treatment of 25.36 microns microgranule fraction. The spherical particles obtained in the experiments had a predominantly dense microstructure and had no internal cavities. The influence of plasma treatment process parameters on dispersity, phase, and chemical composition of spherical micropowders and powder particles microstructure has been established. MDPI 2021-07-30 /pmc/articles/PMC8348052/ /pubmed/34361452 http://dx.doi.org/10.3390/ma14154258 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Samokhin, Andrey
Alekseev, Nikolay
Astashov, Aleksey
Dorofeev, Aleksey
Fadeev, Andrey
Sinayskiy, Mikhail
Kalashnikov, Yulian
Preparation of W-C-Co Composite Micropowder with Spherical Shaped Particles Using Plasma Technologies
title Preparation of W-C-Co Composite Micropowder with Spherical Shaped Particles Using Plasma Technologies
title_full Preparation of W-C-Co Composite Micropowder with Spherical Shaped Particles Using Plasma Technologies
title_fullStr Preparation of W-C-Co Composite Micropowder with Spherical Shaped Particles Using Plasma Technologies
title_full_unstemmed Preparation of W-C-Co Composite Micropowder with Spherical Shaped Particles Using Plasma Technologies
title_short Preparation of W-C-Co Composite Micropowder with Spherical Shaped Particles Using Plasma Technologies
title_sort preparation of w-c-co composite micropowder with spherical shaped particles using plasma technologies
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8348052/
https://www.ncbi.nlm.nih.gov/pubmed/34361452
http://dx.doi.org/10.3390/ma14154258
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