Cargando…

Separation of the inelastic and elastic scattering in time-of-flight mode on the pinhole small-angle neutron scattering diffractometer K­WS-2

To study and control the incoherent inelastic background in small-angle neutron scattering, which makes a significant contribution to the detected scattering from hydrocarbon systems, the KWS-2 small-angle neutron scattering diffractometer operated by the Jülich Centre for Neutron Science (JCNS) at...

Descripción completa

Detalles Bibliográficos
Autores principales: Balacescu, Livia, Brandl, Georg, Radulescu, Aurel
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8366428/
https://www.ncbi.nlm.nih.gov/pubmed/34429724
http://dx.doi.org/10.1107/S1600576721006610
_version_ 1783738885539364864
author Balacescu, Livia
Brandl, Georg
Radulescu, Aurel
author_facet Balacescu, Livia
Brandl, Georg
Radulescu, Aurel
author_sort Balacescu, Livia
collection PubMed
description To study and control the incoherent inelastic background in small-angle neutron scattering, which makes a significant contribution to the detected scattering from hydrocarbon systems, the KWS-2 small-angle neutron scattering diffractometer operated by the Jülich Centre for Neutron Science (JCNS) at Heinz-Maier Leibnitz Zentrum (MLZ), Garching, Germany, was equipped with a secondary single-disc chopper that is placed in front of the sample stage. This makes it possible to record in time-of-flight mode the scattered neutrons in the high-Q regime of the instrument (i.e. short incoming wavelengths and detection distances) and to discard the inelastic component from the measured data. Examples of measurements on different materials routinely used as standard samples, sample containers and solvents in the experiments at KWS-2 are presented. When only the elastic region of the spectrum is used in the data-reduction procedure, a decrease of up to two times in the incoherent background of the experimentally measured scattering cross section may be obtained. The proof of principle is demonstrated on a solution of bovine serum albumin in D(2)O.
format Online
Article
Text
id pubmed-8366428
institution National Center for Biotechnology Information
language English
publishDate 2021
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-83664282021-08-23 Separation of the inelastic and elastic scattering in time-of-flight mode on the pinhole small-angle neutron scattering diffractometer K­WS-2 Balacescu, Livia Brandl, Georg Radulescu, Aurel J Appl Crystallogr Research Papers To study and control the incoherent inelastic background in small-angle neutron scattering, which makes a significant contribution to the detected scattering from hydrocarbon systems, the KWS-2 small-angle neutron scattering diffractometer operated by the Jülich Centre for Neutron Science (JCNS) at Heinz-Maier Leibnitz Zentrum (MLZ), Garching, Germany, was equipped with a secondary single-disc chopper that is placed in front of the sample stage. This makes it possible to record in time-of-flight mode the scattered neutrons in the high-Q regime of the instrument (i.e. short incoming wavelengths and detection distances) and to discard the inelastic component from the measured data. Examples of measurements on different materials routinely used as standard samples, sample containers and solvents in the experiments at KWS-2 are presented. When only the elastic region of the spectrum is used in the data-reduction procedure, a decrease of up to two times in the incoherent background of the experimentally measured scattering cross section may be obtained. The proof of principle is demonstrated on a solution of bovine serum albumin in D(2)O. International Union of Crystallography 2021-07-30 /pmc/articles/PMC8366428/ /pubmed/34429724 http://dx.doi.org/10.1107/S1600576721006610 Text en © Livia Balacescu et al. 2021 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Papers
Balacescu, Livia
Brandl, Georg
Radulescu, Aurel
Separation of the inelastic and elastic scattering in time-of-flight mode on the pinhole small-angle neutron scattering diffractometer K­WS-2
title Separation of the inelastic and elastic scattering in time-of-flight mode on the pinhole small-angle neutron scattering diffractometer K­WS-2
title_full Separation of the inelastic and elastic scattering in time-of-flight mode on the pinhole small-angle neutron scattering diffractometer K­WS-2
title_fullStr Separation of the inelastic and elastic scattering in time-of-flight mode on the pinhole small-angle neutron scattering diffractometer K­WS-2
title_full_unstemmed Separation of the inelastic and elastic scattering in time-of-flight mode on the pinhole small-angle neutron scattering diffractometer K­WS-2
title_short Separation of the inelastic and elastic scattering in time-of-flight mode on the pinhole small-angle neutron scattering diffractometer K­WS-2
title_sort separation of the inelastic and elastic scattering in time-of-flight mode on the pinhole small-angle neutron scattering diffractometer k­ws-2
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8366428/
https://www.ncbi.nlm.nih.gov/pubmed/34429724
http://dx.doi.org/10.1107/S1600576721006610
work_keys_str_mv AT balacesculivia separationoftheinelasticandelasticscatteringintimeofflightmodeonthepinholesmallangleneutronscatteringdiffractometerkws2
AT brandlgeorg separationoftheinelasticandelasticscatteringintimeofflightmodeonthepinholesmallangleneutronscatteringdiffractometerkws2
AT radulescuaurel separationoftheinelasticandelasticscatteringintimeofflightmodeonthepinholesmallangleneutronscatteringdiffractometerkws2