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Fabrication and characterization of TiO(2) and MWCNT coated electrospinning nanofibers for UV protection properties

This paper aimed to fabricate UV protective nanofibers by the use of specific nanoparticles. The DMF/TiO(2) (Titanium dioxide), DMF/MWCNT (Multi-Walled Carbon Nano Tubes), and DMF/MWCNT+TiO(2) (MWCNT: TiO(2) mass ratio= 1:1) solutions were transferred into a syringe with a stainless steel needle wit...

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Autores principales: Koozekonan, Aysa Ghasemi, Esmaeilpour, Mohammad Reza Monazzam, Kalantary, Saba, Karimi, Ali, Azam, Kamal, Golbabaei, Farideh
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8374361/
https://www.ncbi.nlm.nih.gov/pubmed/34430255
http://dx.doi.org/10.1016/j.mex.2021.101354
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author Koozekonan, Aysa Ghasemi
Esmaeilpour, Mohammad Reza Monazzam
Kalantary, Saba
Karimi, Ali
Azam, Kamal
Golbabaei, Farideh
author_facet Koozekonan, Aysa Ghasemi
Esmaeilpour, Mohammad Reza Monazzam
Kalantary, Saba
Karimi, Ali
Azam, Kamal
Golbabaei, Farideh
author_sort Koozekonan, Aysa Ghasemi
collection PubMed
description This paper aimed to fabricate UV protective nanofibers by the use of specific nanoparticles. The DMF/TiO(2) (Titanium dioxide), DMF/MWCNT (Multi-Walled Carbon Nano Tubes), and DMF/MWCNT+TiO(2) (MWCNT: TiO(2) mass ratio= 1:1) solutions were transferred into a syringe with a stainless steel needle with gauge 21. The electrospinning process was performed for 3 h at the optimized conditions. The surface morphology of nanofibers was characterized by field emission scanning electron microscopy (FESEM). Fourier transform infrared spectroscopy (FTIR) was utilized to characterize functional groups of oxidized MWCNTs and investigate the successful load of nanoparticles at the fiber surface. The UV protection property of nanofibers was investigated by measuring UV rays' transmittance through the composite web. The data of Spectroscopy was used to compute the UV protection factor (UPF). (1) The effect of CNT,TiO(2), and CNT+TiO(2) nanoparticles on ultraviolet protection property was analyzed separately and simultaneously. (2) The different concentrations of nanoparticles, including 1,5,10, & 15 wt%, were used to fabricate UV protective nanocomposites. (3) The electrospinning condition was optimized as a 15 cm distance between the needle tip and collector, 20 KV voltage, 250 RPM drum rotation, and 1.2 ml/h feeding rate to access the best nanofibers.
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spelling pubmed-83743612021-08-23 Fabrication and characterization of TiO(2) and MWCNT coated electrospinning nanofibers for UV protection properties Koozekonan, Aysa Ghasemi Esmaeilpour, Mohammad Reza Monazzam Kalantary, Saba Karimi, Ali Azam, Kamal Golbabaei, Farideh MethodsX Method Article This paper aimed to fabricate UV protective nanofibers by the use of specific nanoparticles. The DMF/TiO(2) (Titanium dioxide), DMF/MWCNT (Multi-Walled Carbon Nano Tubes), and DMF/MWCNT+TiO(2) (MWCNT: TiO(2) mass ratio= 1:1) solutions were transferred into a syringe with a stainless steel needle with gauge 21. The electrospinning process was performed for 3 h at the optimized conditions. The surface morphology of nanofibers was characterized by field emission scanning electron microscopy (FESEM). Fourier transform infrared spectroscopy (FTIR) was utilized to characterize functional groups of oxidized MWCNTs and investigate the successful load of nanoparticles at the fiber surface. The UV protection property of nanofibers was investigated by measuring UV rays' transmittance through the composite web. The data of Spectroscopy was used to compute the UV protection factor (UPF). (1) The effect of CNT,TiO(2), and CNT+TiO(2) nanoparticles on ultraviolet protection property was analyzed separately and simultaneously. (2) The different concentrations of nanoparticles, including 1,5,10, & 15 wt%, were used to fabricate UV protective nanocomposites. (3) The electrospinning condition was optimized as a 15 cm distance between the needle tip and collector, 20 KV voltage, 250 RPM drum rotation, and 1.2 ml/h feeding rate to access the best nanofibers. Elsevier 2021-04-20 /pmc/articles/PMC8374361/ /pubmed/34430255 http://dx.doi.org/10.1016/j.mex.2021.101354 Text en © 2021 The Authors. Published by Elsevier B.V. https://creativecommons.org/licenses/by-nc-nd/4.0/This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
spellingShingle Method Article
Koozekonan, Aysa Ghasemi
Esmaeilpour, Mohammad Reza Monazzam
Kalantary, Saba
Karimi, Ali
Azam, Kamal
Golbabaei, Farideh
Fabrication and characterization of TiO(2) and MWCNT coated electrospinning nanofibers for UV protection properties
title Fabrication and characterization of TiO(2) and MWCNT coated electrospinning nanofibers for UV protection properties
title_full Fabrication and characterization of TiO(2) and MWCNT coated electrospinning nanofibers for UV protection properties
title_fullStr Fabrication and characterization of TiO(2) and MWCNT coated electrospinning nanofibers for UV protection properties
title_full_unstemmed Fabrication and characterization of TiO(2) and MWCNT coated electrospinning nanofibers for UV protection properties
title_short Fabrication and characterization of TiO(2) and MWCNT coated electrospinning nanofibers for UV protection properties
title_sort fabrication and characterization of tio(2) and mwcnt coated electrospinning nanofibers for uv protection properties
topic Method Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8374361/
https://www.ncbi.nlm.nih.gov/pubmed/34430255
http://dx.doi.org/10.1016/j.mex.2021.101354
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