Cargando…
Which is the best (9)Be carrier for (10)Be/(9)Be accelerator mass spectrometry?
Commercial (9)Be solutions used for chemical preparation of samples for accelerator mass spectrometry contain the cosmogenic long-lived radionuclide (10)Be at elevated but different (10)Be/(9)Be levels. Within a systematic study of recently produced solutions, comparison to published data and new da...
Autores principales: | , , , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Elsevier
2021
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8374718/ https://www.ncbi.nlm.nih.gov/pubmed/34434884 http://dx.doi.org/10.1016/j.mex.2021.101486 |
_version_ | 1783740176675110912 |
---|---|
author | Merchel, Silke Braucher, Régis Lachner, Johannes Rugel, Georg |
author_facet | Merchel, Silke Braucher, Régis Lachner, Johannes Rugel, Georg |
author_sort | Merchel, Silke |
collection | PubMed |
description | Commercial (9)Be solutions used for chemical preparation of samples for accelerator mass spectrometry contain the cosmogenic long-lived radionuclide (10)Be at elevated but different (10)Be/(9)Be levels. Within a systematic study of recently produced solutions, comparison to published data and new data on customised solutions from minerals, we recommend - if no customised solution is available - the (9)Be solutions from Australian Chemical Reagents (ACR) or from LGC. They contain (10)Be/(9)Be at the 3.4 × 10(−15) level, which is still suitable for the majority of Earth science applications, compared to customised solutions at the 10(−16) level for lowest-level studies. Commercial solutions from Scharlab having different lot numbers, i.e. an identification number assigned to a particular lot of material from a single manufacturer, vary in (10)Be/(9)Be by up to a factor of nine. Hence, it seems an advisable strategy to buy a bigger quantity of a single production batch (such as 10 × 100 ml bottles of (9)Be at 1 g l(−1)) and have them tested once at any AMS facility before first use. • The best (9)Be carrier for low-level (10)Be/(9)Be applications is a customised one from minerals like phenakite. • The best (9)Be carriers for medium- and high-level (10)Be/(9)Be applications are currently from Australian Chemical Reagents (ACR) or from LGC. • As (9)Be carriers from Scharlab of different batches (LOT) contain (10)Be/(9)Be at different levels, it is advisable to buy a bigger number of bottles of the same LOT of commercial carriers after being identified to have reasonably low isotope ratios. |
format | Online Article Text |
id | pubmed-8374718 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2021 |
publisher | Elsevier |
record_format | MEDLINE/PubMed |
spelling | pubmed-83747182021-08-24 Which is the best (9)Be carrier for (10)Be/(9)Be accelerator mass spectrometry? Merchel, Silke Braucher, Régis Lachner, Johannes Rugel, Georg MethodsX Method Article Commercial (9)Be solutions used for chemical preparation of samples for accelerator mass spectrometry contain the cosmogenic long-lived radionuclide (10)Be at elevated but different (10)Be/(9)Be levels. Within a systematic study of recently produced solutions, comparison to published data and new data on customised solutions from minerals, we recommend - if no customised solution is available - the (9)Be solutions from Australian Chemical Reagents (ACR) or from LGC. They contain (10)Be/(9)Be at the 3.4 × 10(−15) level, which is still suitable for the majority of Earth science applications, compared to customised solutions at the 10(−16) level for lowest-level studies. Commercial solutions from Scharlab having different lot numbers, i.e. an identification number assigned to a particular lot of material from a single manufacturer, vary in (10)Be/(9)Be by up to a factor of nine. Hence, it seems an advisable strategy to buy a bigger quantity of a single production batch (such as 10 × 100 ml bottles of (9)Be at 1 g l(−1)) and have them tested once at any AMS facility before first use. • The best (9)Be carrier for low-level (10)Be/(9)Be applications is a customised one from minerals like phenakite. • The best (9)Be carriers for medium- and high-level (10)Be/(9)Be applications are currently from Australian Chemical Reagents (ACR) or from LGC. • As (9)Be carriers from Scharlab of different batches (LOT) contain (10)Be/(9)Be at different levels, it is advisable to buy a bigger number of bottles of the same LOT of commercial carriers after being identified to have reasonably low isotope ratios. Elsevier 2021-08-11 /pmc/articles/PMC8374718/ /pubmed/34434884 http://dx.doi.org/10.1016/j.mex.2021.101486 Text en © 2021 The Authors. Published by Elsevier B.V. https://creativecommons.org/licenses/by/4.0/This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Method Article Merchel, Silke Braucher, Régis Lachner, Johannes Rugel, Georg Which is the best (9)Be carrier for (10)Be/(9)Be accelerator mass spectrometry? |
title | Which is the best (9)Be carrier for (10)Be/(9)Be accelerator mass spectrometry? |
title_full | Which is the best (9)Be carrier for (10)Be/(9)Be accelerator mass spectrometry? |
title_fullStr | Which is the best (9)Be carrier for (10)Be/(9)Be accelerator mass spectrometry? |
title_full_unstemmed | Which is the best (9)Be carrier for (10)Be/(9)Be accelerator mass spectrometry? |
title_short | Which is the best (9)Be carrier for (10)Be/(9)Be accelerator mass spectrometry? |
title_sort | which is the best (9)be carrier for (10)be/(9)be accelerator mass spectrometry? |
topic | Method Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8374718/ https://www.ncbi.nlm.nih.gov/pubmed/34434884 http://dx.doi.org/10.1016/j.mex.2021.101486 |
work_keys_str_mv | AT merchelsilke whichisthebest9becarrierfor10be9beacceleratormassspectrometry AT braucherregis whichisthebest9becarrierfor10be9beacceleratormassspectrometry AT lachnerjohannes whichisthebest9becarrierfor10be9beacceleratormassspectrometry AT rugelgeorg whichisthebest9becarrierfor10be9beacceleratormassspectrometry |