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Potent Acrylamide Determination in Food Products Using Ion-Selective Electrode Technique

A potent selective acrylamide liquid sensor based on the reaction of acrylamide with 2-(5-Bromo-2-pyridylazo)-5-[N-n-Propyl-N-(3-Sulfopropyl) amino] aniline reagent is successfully designed. The characteristics slope (52.33 mV/decade), linearity usable range from 1.0 × 10(−7)–1.0 × 10(−1) molar, lim...

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Autores principales: Khalil, Sabry, El-Beltagy, Alaa, El-Sharnouby, Mohamed
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8398482/
https://www.ncbi.nlm.nih.gov/pubmed/34436408
http://dx.doi.org/10.3390/membranes11080645
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author Khalil, Sabry
El-Beltagy, Alaa
El-Sharnouby, Mohamed
author_facet Khalil, Sabry
El-Beltagy, Alaa
El-Sharnouby, Mohamed
author_sort Khalil, Sabry
collection PubMed
description A potent selective acrylamide liquid sensor based on the reaction of acrylamide with 2-(5-Bromo-2-pyridylazo)-5-[N-n-Propyl-N-(3-Sulfopropyl) amino] aniline reagent is successfully designed. The characteristics slope (52.33 mV/decade), linearity usable range from 1.0 × 10(−7)–1.0 × 10(−1) molar, limit of detection (1.6 × 10(−8)) molar, selectivity attitude to several inorganic cations, amino acids and sugars, time of response (8 s), lifetime (four months), pH effect on the electrode potential and the basic validation parameters were studied. The desirable pH applicable range was 3.0–6.5, and the restraint of the developed sensor is independent on this working pH range. The deployed electrode was effectively applied for rapid inexpensive analysis of acrylamide cations in food products with comparison to high-performance liquid chromatographic method and the results were agreeable with each other. The obtained data by the suggested electrode were treated statistically and compared with the various recently published acrylamide sensors.
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spelling pubmed-83984822021-08-29 Potent Acrylamide Determination in Food Products Using Ion-Selective Electrode Technique Khalil, Sabry El-Beltagy, Alaa El-Sharnouby, Mohamed Membranes (Basel) Article A potent selective acrylamide liquid sensor based on the reaction of acrylamide with 2-(5-Bromo-2-pyridylazo)-5-[N-n-Propyl-N-(3-Sulfopropyl) amino] aniline reagent is successfully designed. The characteristics slope (52.33 mV/decade), linearity usable range from 1.0 × 10(−7)–1.0 × 10(−1) molar, limit of detection (1.6 × 10(−8)) molar, selectivity attitude to several inorganic cations, amino acids and sugars, time of response (8 s), lifetime (four months), pH effect on the electrode potential and the basic validation parameters were studied. The desirable pH applicable range was 3.0–6.5, and the restraint of the developed sensor is independent on this working pH range. The deployed electrode was effectively applied for rapid inexpensive analysis of acrylamide cations in food products with comparison to high-performance liquid chromatographic method and the results were agreeable with each other. The obtained data by the suggested electrode were treated statistically and compared with the various recently published acrylamide sensors. MDPI 2021-08-23 /pmc/articles/PMC8398482/ /pubmed/34436408 http://dx.doi.org/10.3390/membranes11080645 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Khalil, Sabry
El-Beltagy, Alaa
El-Sharnouby, Mohamed
Potent Acrylamide Determination in Food Products Using Ion-Selective Electrode Technique
title Potent Acrylamide Determination in Food Products Using Ion-Selective Electrode Technique
title_full Potent Acrylamide Determination in Food Products Using Ion-Selective Electrode Technique
title_fullStr Potent Acrylamide Determination in Food Products Using Ion-Selective Electrode Technique
title_full_unstemmed Potent Acrylamide Determination in Food Products Using Ion-Selective Electrode Technique
title_short Potent Acrylamide Determination in Food Products Using Ion-Selective Electrode Technique
title_sort potent acrylamide determination in food products using ion-selective electrode technique
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8398482/
https://www.ncbi.nlm.nih.gov/pubmed/34436408
http://dx.doi.org/10.3390/membranes11080645
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