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Potent Acrylamide Determination in Food Products Using Ion-Selective Electrode Technique
A potent selective acrylamide liquid sensor based on the reaction of acrylamide with 2-(5-Bromo-2-pyridylazo)-5-[N-n-Propyl-N-(3-Sulfopropyl) amino] aniline reagent is successfully designed. The characteristics slope (52.33 mV/decade), linearity usable range from 1.0 × 10(−7)–1.0 × 10(−1) molar, lim...
Autores principales: | , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2021
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8398482/ https://www.ncbi.nlm.nih.gov/pubmed/34436408 http://dx.doi.org/10.3390/membranes11080645 |
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author | Khalil, Sabry El-Beltagy, Alaa El-Sharnouby, Mohamed |
author_facet | Khalil, Sabry El-Beltagy, Alaa El-Sharnouby, Mohamed |
author_sort | Khalil, Sabry |
collection | PubMed |
description | A potent selective acrylamide liquid sensor based on the reaction of acrylamide with 2-(5-Bromo-2-pyridylazo)-5-[N-n-Propyl-N-(3-Sulfopropyl) amino] aniline reagent is successfully designed. The characteristics slope (52.33 mV/decade), linearity usable range from 1.0 × 10(−7)–1.0 × 10(−1) molar, limit of detection (1.6 × 10(−8)) molar, selectivity attitude to several inorganic cations, amino acids and sugars, time of response (8 s), lifetime (four months), pH effect on the electrode potential and the basic validation parameters were studied. The desirable pH applicable range was 3.0–6.5, and the restraint of the developed sensor is independent on this working pH range. The deployed electrode was effectively applied for rapid inexpensive analysis of acrylamide cations in food products with comparison to high-performance liquid chromatographic method and the results were agreeable with each other. The obtained data by the suggested electrode were treated statistically and compared with the various recently published acrylamide sensors. |
format | Online Article Text |
id | pubmed-8398482 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2021 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-83984822021-08-29 Potent Acrylamide Determination in Food Products Using Ion-Selective Electrode Technique Khalil, Sabry El-Beltagy, Alaa El-Sharnouby, Mohamed Membranes (Basel) Article A potent selective acrylamide liquid sensor based on the reaction of acrylamide with 2-(5-Bromo-2-pyridylazo)-5-[N-n-Propyl-N-(3-Sulfopropyl) amino] aniline reagent is successfully designed. The characteristics slope (52.33 mV/decade), linearity usable range from 1.0 × 10(−7)–1.0 × 10(−1) molar, limit of detection (1.6 × 10(−8)) molar, selectivity attitude to several inorganic cations, amino acids and sugars, time of response (8 s), lifetime (four months), pH effect on the electrode potential and the basic validation parameters were studied. The desirable pH applicable range was 3.0–6.5, and the restraint of the developed sensor is independent on this working pH range. The deployed electrode was effectively applied for rapid inexpensive analysis of acrylamide cations in food products with comparison to high-performance liquid chromatographic method and the results were agreeable with each other. The obtained data by the suggested electrode were treated statistically and compared with the various recently published acrylamide sensors. MDPI 2021-08-23 /pmc/articles/PMC8398482/ /pubmed/34436408 http://dx.doi.org/10.3390/membranes11080645 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Khalil, Sabry El-Beltagy, Alaa El-Sharnouby, Mohamed Potent Acrylamide Determination in Food Products Using Ion-Selective Electrode Technique |
title | Potent Acrylamide Determination in Food Products Using Ion-Selective Electrode Technique |
title_full | Potent Acrylamide Determination in Food Products Using Ion-Selective Electrode Technique |
title_fullStr | Potent Acrylamide Determination in Food Products Using Ion-Selective Electrode Technique |
title_full_unstemmed | Potent Acrylamide Determination in Food Products Using Ion-Selective Electrode Technique |
title_short | Potent Acrylamide Determination in Food Products Using Ion-Selective Electrode Technique |
title_sort | potent acrylamide determination in food products using ion-selective electrode technique |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8398482/ https://www.ncbi.nlm.nih.gov/pubmed/34436408 http://dx.doi.org/10.3390/membranes11080645 |
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