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The Curing Kinetics of E-Glass Fiber/Epoxy Resin Prepreg and the Bending Properties of Its Products

The curing kinetics can influence the final macroscopic properties, particularly the three-point bending of the fiber-reinforced composite materials. In this research, the curing kinetics of commercially available glass fiber/epoxy resin prepregs were studied by non-isothermal differential scanning...

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Detalles Bibliográficos
Autores principales: Zhu, Lvtao, Wang, Zhenxing, Rahman, Mahfuz Bin, Shen, Wei, Zhu, Chengyan
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8399898/
https://www.ncbi.nlm.nih.gov/pubmed/34443194
http://dx.doi.org/10.3390/ma14164673
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author Zhu, Lvtao
Wang, Zhenxing
Rahman, Mahfuz Bin
Shen, Wei
Zhu, Chengyan
author_facet Zhu, Lvtao
Wang, Zhenxing
Rahman, Mahfuz Bin
Shen, Wei
Zhu, Chengyan
author_sort Zhu, Lvtao
collection PubMed
description The curing kinetics can influence the final macroscopic properties, particularly the three-point bending of the fiber-reinforced composite materials. In this research, the curing kinetics of commercially available glass fiber/epoxy resin prepregs were studied by non-isothermal differential scanning calorimetry (DSC). The curing kinetic parameters were obtained by fitting and the apparent activation energy E(a) of the prepreg, the pre-exponent factor, and the reaction order value obtained. A phenomenological nth-order curing reaction kinetic model was established according to Kissinger equation and Crane equation. Furthermore, the optimal curing temperature of the prepregs was obtained by the T-β extrapolation method. A vacuum hot pressing technique was applied to prepare composite laminates. The pre-curing, curing, and post-curing temperatures were 116, 130, and 153 °C respectively. In addition, three-point bending was used to test the specimens’ fracture behavior, and the surface morphology was analyzed. The results show that the differences in the mechanical properties of the samples are relatively small, indicating that the process settings are reasonable.
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spelling pubmed-83998982021-08-29 The Curing Kinetics of E-Glass Fiber/Epoxy Resin Prepreg and the Bending Properties of Its Products Zhu, Lvtao Wang, Zhenxing Rahman, Mahfuz Bin Shen, Wei Zhu, Chengyan Materials (Basel) Article The curing kinetics can influence the final macroscopic properties, particularly the three-point bending of the fiber-reinforced composite materials. In this research, the curing kinetics of commercially available glass fiber/epoxy resin prepregs were studied by non-isothermal differential scanning calorimetry (DSC). The curing kinetic parameters were obtained by fitting and the apparent activation energy E(a) of the prepreg, the pre-exponent factor, and the reaction order value obtained. A phenomenological nth-order curing reaction kinetic model was established according to Kissinger equation and Crane equation. Furthermore, the optimal curing temperature of the prepregs was obtained by the T-β extrapolation method. A vacuum hot pressing technique was applied to prepare composite laminates. The pre-curing, curing, and post-curing temperatures were 116, 130, and 153 °C respectively. In addition, three-point bending was used to test the specimens’ fracture behavior, and the surface morphology was analyzed. The results show that the differences in the mechanical properties of the samples are relatively small, indicating that the process settings are reasonable. MDPI 2021-08-19 /pmc/articles/PMC8399898/ /pubmed/34443194 http://dx.doi.org/10.3390/ma14164673 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Zhu, Lvtao
Wang, Zhenxing
Rahman, Mahfuz Bin
Shen, Wei
Zhu, Chengyan
The Curing Kinetics of E-Glass Fiber/Epoxy Resin Prepreg and the Bending Properties of Its Products
title The Curing Kinetics of E-Glass Fiber/Epoxy Resin Prepreg and the Bending Properties of Its Products
title_full The Curing Kinetics of E-Glass Fiber/Epoxy Resin Prepreg and the Bending Properties of Its Products
title_fullStr The Curing Kinetics of E-Glass Fiber/Epoxy Resin Prepreg and the Bending Properties of Its Products
title_full_unstemmed The Curing Kinetics of E-Glass Fiber/Epoxy Resin Prepreg and the Bending Properties of Its Products
title_short The Curing Kinetics of E-Glass Fiber/Epoxy Resin Prepreg and the Bending Properties of Its Products
title_sort curing kinetics of e-glass fiber/epoxy resin prepreg and the bending properties of its products
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8399898/
https://www.ncbi.nlm.nih.gov/pubmed/34443194
http://dx.doi.org/10.3390/ma14164673
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