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Corrosion Resistance Measurement of 316L Stainless Steel Manufactured by Selective Laser Melting

Selective laser melting (SLM) technology is ushering in a new era of advanced industrial production of metal components. It is of great importance to understand the relationship between the surface features and electrochemical properties of manufactured parts. This work studied the influence of surf...

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Autores principales: Guzmán-Nogales, Rigoberto, Estupiñán-López, Francisco, Gaona-Tiburcio, Citlalli, Lopez-Botello, Omar E., Ramírez-Rodríguez, Juan G., Zambrano-Robledo, Patricia C.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8402199/
https://www.ncbi.nlm.nih.gov/pubmed/34443031
http://dx.doi.org/10.3390/ma14164509
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author Guzmán-Nogales, Rigoberto
Estupiñán-López, Francisco
Gaona-Tiburcio, Citlalli
Lopez-Botello, Omar E.
Ramírez-Rodríguez, Juan G.
Zambrano-Robledo, Patricia C.
author_facet Guzmán-Nogales, Rigoberto
Estupiñán-López, Francisco
Gaona-Tiburcio, Citlalli
Lopez-Botello, Omar E.
Ramírez-Rodríguez, Juan G.
Zambrano-Robledo, Patricia C.
author_sort Guzmán-Nogales, Rigoberto
collection PubMed
description Selective laser melting (SLM) technology is ushering in a new era of advanced industrial production of metal components. It is of great importance to understand the relationship between the surface features and electrochemical properties of manufactured parts. This work studied the influence of surface orientation on the corrosion resistance of 316L stainless-steel (SS) components manufactured with SLM. The corrosion resistance of the samples was measured using linear polarization resistance (LPR) and electromechanical noise (EN) techniques under three different environments, H(2)O, 3.5 wt.% NaCl, and 20% H(2)SO(4), analyzing the horizontal (XY) and vertical (XZ) planes. The microstructure and morphology of the samples were obtained by optical (OM) and scanning electron microscopy (SEM). The obtained microstructure showed the grains growing up from the fusion line to the melt pool center and, via SEM-EDS, the presence of irregular and spherical pores was observed. The highest corrosion rate was identified in the H(2)SO(4) solution in the XZ plane with 2.4 × 10(−2) mm/year and the XY plane with 1.31 × 10(−3) mm/year. The EN technique along with the skewness factor were used to determine the type of corrosion that the material developed. Localized corrosion was observed in the NaCl electrolyte, for the XY and XZ planes (−1.65 and −0.012 skewness factors, respectively), attacking mainly the subgrains of the microstructure and, in some cases, the pores, caused by Cl ions. H(2)O and H(2)SO(4) solutions presented a uniform corrosion mechanism for the two observed orientations. The morphology identified by SEM was correlated with the results obtained from the electrochemical techniques.
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spelling pubmed-84021992021-08-29 Corrosion Resistance Measurement of 316L Stainless Steel Manufactured by Selective Laser Melting Guzmán-Nogales, Rigoberto Estupiñán-López, Francisco Gaona-Tiburcio, Citlalli Lopez-Botello, Omar E. Ramírez-Rodríguez, Juan G. Zambrano-Robledo, Patricia C. Materials (Basel) Article Selective laser melting (SLM) technology is ushering in a new era of advanced industrial production of metal components. It is of great importance to understand the relationship between the surface features and electrochemical properties of manufactured parts. This work studied the influence of surface orientation on the corrosion resistance of 316L stainless-steel (SS) components manufactured with SLM. The corrosion resistance of the samples was measured using linear polarization resistance (LPR) and electromechanical noise (EN) techniques under three different environments, H(2)O, 3.5 wt.% NaCl, and 20% H(2)SO(4), analyzing the horizontal (XY) and vertical (XZ) planes. The microstructure and morphology of the samples were obtained by optical (OM) and scanning electron microscopy (SEM). The obtained microstructure showed the grains growing up from the fusion line to the melt pool center and, via SEM-EDS, the presence of irregular and spherical pores was observed. The highest corrosion rate was identified in the H(2)SO(4) solution in the XZ plane with 2.4 × 10(−2) mm/year and the XY plane with 1.31 × 10(−3) mm/year. The EN technique along with the skewness factor were used to determine the type of corrosion that the material developed. Localized corrosion was observed in the NaCl electrolyte, for the XY and XZ planes (−1.65 and −0.012 skewness factors, respectively), attacking mainly the subgrains of the microstructure and, in some cases, the pores, caused by Cl ions. H(2)O and H(2)SO(4) solutions presented a uniform corrosion mechanism for the two observed orientations. The morphology identified by SEM was correlated with the results obtained from the electrochemical techniques. MDPI 2021-08-11 /pmc/articles/PMC8402199/ /pubmed/34443031 http://dx.doi.org/10.3390/ma14164509 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Guzmán-Nogales, Rigoberto
Estupiñán-López, Francisco
Gaona-Tiburcio, Citlalli
Lopez-Botello, Omar E.
Ramírez-Rodríguez, Juan G.
Zambrano-Robledo, Patricia C.
Corrosion Resistance Measurement of 316L Stainless Steel Manufactured by Selective Laser Melting
title Corrosion Resistance Measurement of 316L Stainless Steel Manufactured by Selective Laser Melting
title_full Corrosion Resistance Measurement of 316L Stainless Steel Manufactured by Selective Laser Melting
title_fullStr Corrosion Resistance Measurement of 316L Stainless Steel Manufactured by Selective Laser Melting
title_full_unstemmed Corrosion Resistance Measurement of 316L Stainless Steel Manufactured by Selective Laser Melting
title_short Corrosion Resistance Measurement of 316L Stainless Steel Manufactured by Selective Laser Melting
title_sort corrosion resistance measurement of 316l stainless steel manufactured by selective laser melting
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8402199/
https://www.ncbi.nlm.nih.gov/pubmed/34443031
http://dx.doi.org/10.3390/ma14164509
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