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Π-GISANS: probing lateral structures with a fan shaped beam

We have performed grazing incidence neutron small angle scattering using a fan shaped incident beam focused along one dimension. This allows significantly reduced counting times for measurements of lateral correlations parallel to an interface or in a thin film where limited depth resolution is requ...

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Detalles Bibliográficos
Autores principales: Vorobiev, Alexei, Paracini, Nicolò, Cárdenas, Marité, Wolff, Max
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8423805/
https://www.ncbi.nlm.nih.gov/pubmed/34493764
http://dx.doi.org/10.1038/s41598-021-97112-x
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author Vorobiev, Alexei
Paracini, Nicolò
Cárdenas, Marité
Wolff, Max
author_facet Vorobiev, Alexei
Paracini, Nicolò
Cárdenas, Marité
Wolff, Max
author_sort Vorobiev, Alexei
collection PubMed
description We have performed grazing incidence neutron small angle scattering using a fan shaped incident beam focused along one dimension. This allows significantly reduced counting times for measurements of lateral correlations parallel to an interface or in a thin film where limited depth resolution is required. We resolve the structure factor of iron inclusions in aluminium oxide and show that the ordering of silica particles deposited on a silicon substrate depends on their size. We report hexagonal packing for 50 nm but not for 200 nm silica spheres deposited by a modified Langmuir-Schaefer method on a silicon substrate. For the 200 nm particles we extract the particles shape from the form factor. Moreover, we report dense packing of the particles spread on a free water surface. We name this method π-GISANS to highlight that it differs from GISANS as it gives lateral information while averaging the in-depth structure.
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spelling pubmed-84238052021-09-09 Π-GISANS: probing lateral structures with a fan shaped beam Vorobiev, Alexei Paracini, Nicolò Cárdenas, Marité Wolff, Max Sci Rep Article We have performed grazing incidence neutron small angle scattering using a fan shaped incident beam focused along one dimension. This allows significantly reduced counting times for measurements of lateral correlations parallel to an interface or in a thin film where limited depth resolution is required. We resolve the structure factor of iron inclusions in aluminium oxide and show that the ordering of silica particles deposited on a silicon substrate depends on their size. We report hexagonal packing for 50 nm but not for 200 nm silica spheres deposited by a modified Langmuir-Schaefer method on a silicon substrate. For the 200 nm particles we extract the particles shape from the form factor. Moreover, we report dense packing of the particles spread on a free water surface. We name this method π-GISANS to highlight that it differs from GISANS as it gives lateral information while averaging the in-depth structure. Nature Publishing Group UK 2021-09-07 /pmc/articles/PMC8423805/ /pubmed/34493764 http://dx.doi.org/10.1038/s41598-021-97112-x Text en © The Author(s) 2021 https://creativecommons.org/licenses/by/4.0/Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) .
spellingShingle Article
Vorobiev, Alexei
Paracini, Nicolò
Cárdenas, Marité
Wolff, Max
Π-GISANS: probing lateral structures with a fan shaped beam
title Π-GISANS: probing lateral structures with a fan shaped beam
title_full Π-GISANS: probing lateral structures with a fan shaped beam
title_fullStr Π-GISANS: probing lateral structures with a fan shaped beam
title_full_unstemmed Π-GISANS: probing lateral structures with a fan shaped beam
title_short Π-GISANS: probing lateral structures with a fan shaped beam
title_sort π-gisans: probing lateral structures with a fan shaped beam
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8423805/
https://www.ncbi.nlm.nih.gov/pubmed/34493764
http://dx.doi.org/10.1038/s41598-021-97112-x
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