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Fabrication of freestanding Pt nanowires for use as thermal anemometry probes in turbulence measurements

We report a robust fabrication method for patterning freestanding Pt nanowires for use as thermal anemometry probes for small-scale turbulence measurements. Using e-beam lithography, high aspect ratio Pt nanowires (~300 nm width, ~70 µm length, ~100 nm thickness) were patterned on the surface of oxi...

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Autores principales: Le-The, Hai, Küchler, Christian, van den Berg, Albert, Bodenschatz, Eberhard, Lohse, Detlef, Krug, Dominik
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8433353/
https://www.ncbi.nlm.nih.gov/pubmed/34567742
http://dx.doi.org/10.1038/s41378-021-00255-0
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author Le-The, Hai
Küchler, Christian
van den Berg, Albert
Bodenschatz, Eberhard
Lohse, Detlef
Krug, Dominik
author_facet Le-The, Hai
Küchler, Christian
van den Berg, Albert
Bodenschatz, Eberhard
Lohse, Detlef
Krug, Dominik
author_sort Le-The, Hai
collection PubMed
description We report a robust fabrication method for patterning freestanding Pt nanowires for use as thermal anemometry probes for small-scale turbulence measurements. Using e-beam lithography, high aspect ratio Pt nanowires (~300 nm width, ~70 µm length, ~100 nm thickness) were patterned on the surface of oxidized silicon (Si) wafers. Combining wet etching processes with dry etching processes, these Pt nanowires were successfully released, rendering them freestanding between two silicon dioxide (SiO(2)) beams supported on Si cantilevers. Moreover, the unique design of the bridge holding the device allowed gentle release of the device without damaging the Pt nanowires. The total fabrication time was minimized by restricting the use of e-beam lithography to the patterning of the Pt nanowires, while standard photolithography was employed for other parts of the devices. We demonstrate that the fabricated sensors are suitable for turbulence measurements when operated in constant-current mode. A robust calibration between the output voltage and the fluid velocity was established over the velocity range from 0.5 to 5 m s(−1) in a SF(6) atmosphere at a pressure of 2 bar and a temperature of 21 °C. The sensing signal from the nanowires showed negligible drift over a period of several hours. Moreover, we confirmed that the nanowires can withstand high dynamic pressures by testing them in air at room temperature for velocities up to 55 m s(−1).
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spelling pubmed-84333532021-09-24 Fabrication of freestanding Pt nanowires for use as thermal anemometry probes in turbulence measurements Le-The, Hai Küchler, Christian van den Berg, Albert Bodenschatz, Eberhard Lohse, Detlef Krug, Dominik Microsyst Nanoeng Article We report a robust fabrication method for patterning freestanding Pt nanowires for use as thermal anemometry probes for small-scale turbulence measurements. Using e-beam lithography, high aspect ratio Pt nanowires (~300 nm width, ~70 µm length, ~100 nm thickness) were patterned on the surface of oxidized silicon (Si) wafers. Combining wet etching processes with dry etching processes, these Pt nanowires were successfully released, rendering them freestanding between two silicon dioxide (SiO(2)) beams supported on Si cantilevers. Moreover, the unique design of the bridge holding the device allowed gentle release of the device without damaging the Pt nanowires. The total fabrication time was minimized by restricting the use of e-beam lithography to the patterning of the Pt nanowires, while standard photolithography was employed for other parts of the devices. We demonstrate that the fabricated sensors are suitable for turbulence measurements when operated in constant-current mode. A robust calibration between the output voltage and the fluid velocity was established over the velocity range from 0.5 to 5 m s(−1) in a SF(6) atmosphere at a pressure of 2 bar and a temperature of 21 °C. The sensing signal from the nanowires showed negligible drift over a period of several hours. Moreover, we confirmed that the nanowires can withstand high dynamic pressures by testing them in air at room temperature for velocities up to 55 m s(−1). Nature Publishing Group UK 2021-04-02 /pmc/articles/PMC8433353/ /pubmed/34567742 http://dx.doi.org/10.1038/s41378-021-00255-0 Text en © The Author(s) 2021 https://creativecommons.org/licenses/by/4.0/Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) .
spellingShingle Article
Le-The, Hai
Küchler, Christian
van den Berg, Albert
Bodenschatz, Eberhard
Lohse, Detlef
Krug, Dominik
Fabrication of freestanding Pt nanowires for use as thermal anemometry probes in turbulence measurements
title Fabrication of freestanding Pt nanowires for use as thermal anemometry probes in turbulence measurements
title_full Fabrication of freestanding Pt nanowires for use as thermal anemometry probes in turbulence measurements
title_fullStr Fabrication of freestanding Pt nanowires for use as thermal anemometry probes in turbulence measurements
title_full_unstemmed Fabrication of freestanding Pt nanowires for use as thermal anemometry probes in turbulence measurements
title_short Fabrication of freestanding Pt nanowires for use as thermal anemometry probes in turbulence measurements
title_sort fabrication of freestanding pt nanowires for use as thermal anemometry probes in turbulence measurements
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8433353/
https://www.ncbi.nlm.nih.gov/pubmed/34567742
http://dx.doi.org/10.1038/s41378-021-00255-0
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