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Void Content Minimization in Vacuum Infusion (VI) via Effective Degassing

This paper addresses the major concern which component porosity represents in Vacuum Infusion (VI) manufacturing due to resin gelation at pressures close to absolute vacuum. Degassing is a fundamental step to minimize or even avoid resin outgassing and enhance dissolution of voids created during pre...

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Detalles Bibliográficos
Autores principales: Juan, Jaime, Silva, Arlindo, Tornero, Jose Antonio, Gámez, Jose, Salán, Nuria
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8433843/
https://www.ncbi.nlm.nih.gov/pubmed/34502916
http://dx.doi.org/10.3390/polym13172876
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author Juan, Jaime
Silva, Arlindo
Tornero, Jose Antonio
Gámez, Jose
Salán, Nuria
author_facet Juan, Jaime
Silva, Arlindo
Tornero, Jose Antonio
Gámez, Jose
Salán, Nuria
author_sort Juan, Jaime
collection PubMed
description This paper addresses the major concern which component porosity represents in Vacuum Infusion (VI) manufacturing due to resin gelation at pressures close to absolute vacuum. Degassing is a fundamental step to minimize or even avoid resin outgassing and enhance dissolution of voids created during preform impregnation. The efficacy of different degassing procedures based on vacuum degassing, and assisted by adding a nucleation medium, High Speed (HS) resin stirring and/or later pressurization during different time intervals have been analyzed in terms of final void content is studied. Through a rigorous and careful design of the manufacturing process, outgassing effects on final void content were isolated from the rest of porosity causes and specimens with two clearly identifiable regions in terms of porosity were manufactured to facilitate its analysis. Maximum void content was kept under 4% and porous area size was reduced by 72% with respect to conventional vacuum degassing when resin was stirred at HS; therefore, highlighting the importance of enhancing bubble formation during degassing.
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spelling pubmed-84338432021-09-12 Void Content Minimization in Vacuum Infusion (VI) via Effective Degassing Juan, Jaime Silva, Arlindo Tornero, Jose Antonio Gámez, Jose Salán, Nuria Polymers (Basel) Article This paper addresses the major concern which component porosity represents in Vacuum Infusion (VI) manufacturing due to resin gelation at pressures close to absolute vacuum. Degassing is a fundamental step to minimize or even avoid resin outgassing and enhance dissolution of voids created during preform impregnation. The efficacy of different degassing procedures based on vacuum degassing, and assisted by adding a nucleation medium, High Speed (HS) resin stirring and/or later pressurization during different time intervals have been analyzed in terms of final void content is studied. Through a rigorous and careful design of the manufacturing process, outgassing effects on final void content were isolated from the rest of porosity causes and specimens with two clearly identifiable regions in terms of porosity were manufactured to facilitate its analysis. Maximum void content was kept under 4% and porous area size was reduced by 72% with respect to conventional vacuum degassing when resin was stirred at HS; therefore, highlighting the importance of enhancing bubble formation during degassing. MDPI 2021-08-27 /pmc/articles/PMC8433843/ /pubmed/34502916 http://dx.doi.org/10.3390/polym13172876 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Juan, Jaime
Silva, Arlindo
Tornero, Jose Antonio
Gámez, Jose
Salán, Nuria
Void Content Minimization in Vacuum Infusion (VI) via Effective Degassing
title Void Content Minimization in Vacuum Infusion (VI) via Effective Degassing
title_full Void Content Minimization in Vacuum Infusion (VI) via Effective Degassing
title_fullStr Void Content Minimization in Vacuum Infusion (VI) via Effective Degassing
title_full_unstemmed Void Content Minimization in Vacuum Infusion (VI) via Effective Degassing
title_short Void Content Minimization in Vacuum Infusion (VI) via Effective Degassing
title_sort void content minimization in vacuum infusion (vi) via effective degassing
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8433843/
https://www.ncbi.nlm.nih.gov/pubmed/34502916
http://dx.doi.org/10.3390/polym13172876
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