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Ultrafast 2D (1)H–(1)H NMR spectroscopy of DNP-hyperpolarised substrates for the analysis of mixtures
We show that TOCSY and multiple-quantum (MQ) 2D NMR spectra can be obtained for mixtures of substrates hyperpolarised by dissolution dynamic nuclear polarisation (D-DNP). This is achieved by combining optimised transfer settings for D-DNP, with ultrafast 2D NMR experiments based on spatiotemporal en...
Autores principales: | , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
The Royal Society of Chemistry
2021
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8477446/ https://www.ncbi.nlm.nih.gov/pubmed/34291258 http://dx.doi.org/10.1039/d1cc03079e |