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Integration Technology for Wafer-Level LiNbO(3) Single-Crystal Thin Film on Silicon by Polyimide Adhesive Bonding and Chemical Mechanical Polishing

An integration technology for wafer-level LiNbO(3) single-crystal thin film on Si has been achieved. The optimized spin-coating speed of PI (polyimide) adhesive is 3500 rad/min. According to Fourier infrared analysis of the chemical state of the film baked under different conditions, a high-quality...

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Detalles Bibliográficos
Autores principales: Geng, Wenping, Yang, Xiangyu, Xue, Gang, Xu, Wenhao, Bi, Kaixi, Mei, Linyu, Zhang, Le, Hou, Xiaojuan, Chou, Xiujian
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8537918/
https://www.ncbi.nlm.nih.gov/pubmed/34685009
http://dx.doi.org/10.3390/nano11102554
Descripción
Sumario:An integration technology for wafer-level LiNbO(3) single-crystal thin film on Si has been achieved. The optimized spin-coating speed of PI (polyimide) adhesive is 3500 rad/min. According to Fourier infrared analysis of the chemical state of the film baked under different conditions, a high-quality PI film that can be used for wafer-level bonding is obtained. A high bonding strength of 11.38 MPa is obtained by a tensile machine. The bonding interface is uniform, completed and non-porous. After the PI adhesive bonding process, the LiNbO(3) single-crystal was lapped by chemical mechanical polishing. The thickness of the 100 mm diameter LiNbO(3) can be decreased from 500 to 10 μm without generating serious cracks. A defect-free and tight bonding interface was confirmed by scanning electron microscopy. X-ray diffraction results show that the prepared LiNbO(3) single-crystal thin film has a highly crystalline quality. Heterogeneous integration of LiNbO(3) single-crystal thin film on Si is of great significance to the fabrication of MEMS devices for in-situ measurement of space-sensing signals.